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Polyborosilazane, a precursor to SiBNC ceramic, was synthesized via cocondensation approach using methyldichlorosilane (MeHSiCl2), boron trichloride (BCl3) and hexamethydisilazane as starting materials. SiBNC ceramics were obtained by pyrolysing the as-synthesized PBSZ in N2 or NH3/N2 atmospheres.

甲基氢二氯硅烷、三氯化硼、六甲基二硅氮烷为起始原料,采用共缩合原理合成了聚硼硅氮烷先驱体,将PBSZ分别在N2和NH3/N2气氛中高温热解得到SiBNC陶瓷。

A novel hydroxyl terminated aminosilicone oil was synthesized using octamethylcyclo tetrasiloxane (D4) and the hydrolysis product of γ-piperazinepropylmethyldimethoxysilane (HD-110) as raw material and potassium hydrate as catalyst.

以八甲基环四硅氧烷(D4)、γ-哌嗪基丙基甲基二甲氧基硅烷(HD-110)水解物为原料,在氢氧化钾催化下,制备了羟基封端的新型氨基硅油。

Mn oxidates dimethyl sulfoxide to dimethyl sulfone (DMSO2) at pH=6.0 of Tris-HCl buffer solution, Mn could react with dimethyl sulfone to form an ion association complex, so that the system's scattering intensity of RLS is enhanced.

在pH=6.0的Tris-HCl缓冲溶液中,锰氧化二甲基亚砜成为二甲基砜(DMSO2),生成的Mn(上标 2+)与DMSO2结合形成离子缔合物,使体系的共振光散射急聚增强。

Second,α,β-unsaturated nitriles were synthesized by three kinds of methods., all the reactions of N-methylhydroxylamine, O-methylhydroxylamine, N-benzylhydroxylamine and O-benzylhydroxylamine withα,β-unsaturated nitriles were carried out, under different temperatures and different solvents. But no desired products were found, though some catalysis were also added.

在不同温度、不同溶剂的条件下,用所合成的α,β-不饱和腈与N-甲基羟胺、N-苄基羟胺、O-甲基羟胺和O-苄基羟胺分别进行反应,没有得到期望的产物,尝试加入了一些催化剂,也没有得到产物。

We regard horsetail pine weight turpentine as materail, because the chemistry characteristic of its constitutions is different,they can be effectively separated,and synthesize the series perfumes product, Such asω- AML,ω- HML,isolongifolene,β-carypophyllene alcohol,cyclo-oxy-carypophyllene,α-santaleneol.

本文以马尾松重质松节油为原料,利用其组分各自的化学特性不同,对其进行了有效分离,在分离的同时合成系列香料产品,主要有:ω-乙酰氧甲基长叶烯、ω-羟甲基长叶烯、异长叶烯、甲酸长叶酯、β-石竹烯醇、环氧石竹烯、a-檀香烯醇等。

The central 5, 5'-disubstituted bipyridine units of each ligand coordinate theNi or Fe ion, while all the terminal 6-monosubstituted bipyridine units of the ligands keep free of coordination, as the result trinuclear triple-stranded helicate 〓 can not form. This is considered to be caused by the steric hindrance of the methylene substituents α to the chelating nitrogens of the terminal bipyridine units and the strain caused by linkage mode.

配体L〓与Ag作用得到〓,两个配体链相互缠绕着两个Ag离子周围形成双股螺旋结构并以头尾式排列(见图3),由于配体中位于配位N原子α或β位的末端甲基或次甲基取代基的空间位阻阻碍了头对头式异构体的形成,也正是由于配体头尾式排列而使Ag双股螺旋得以形成,这一结果表明该螺旋体的组装过程中自发地采取了空间阻碍尽可能小的那个构型。

They are hydrogen peroxide, ammonium persulfate, sodium persulfate, chlorinated polypropylene, chloridized EVA, garox mek, carbon dioxide, hydrogen, sodium carboxymethyl cellulose, carboxymethyl amylum sodium, feed additive, auric salt and silver salt series, tin salt series, tin dichloride, silver nitrate, fireworks raw materials, spheroid form nickel hydroxide, refined sulfuric acid, battery sulfuric acid, ultramicro fine powder, compound fertilizer, 40% multiple sulfur suspending agent, 40% sulfur-tricyclazole suspending agent, 40% sulfur-multiple-trideflocculant, 20% pemiro-dichlor suspending agent, high panniculus adiposus and so on.

主要产品有:过氧化氢、过硫酸铵、过硫酸钠、氯化聚丙烯、氯化EVA 、过氧化甲乙酮、二氧化碳、氢气、羧甲基纤维素钠、羧甲基淀粉钠、饲料添加剂、金、银盐系列、锡盐系列、氯化亚锡、硝酸银、烟花原料、球形氢氧化镍、精制硫酸、电池硫酸、超微细粉体、复合肥、40%多硫悬浮剂、40%硫·三环唑悬浮剂、40%硫·多·三悬浮剂、20%吡嘧·二氯悬浮剂、高脂膜等10个系列百多个品种、规格产品。

The study investigats the mass transport and hydrolysis behavior for poly in various concentrations of methanol/ tin chloride (SnCl2·2H2O) cosolvent between 40℃ to 60℃. Furthermore, by using the successfully manufactured poly/ tin dioxide nano composites, the mechanical, optical and thermal properties are investigated.

中文摘要本研究系探讨在不同质传温度(40℃~60℃)下,聚甲基丙烯酸甲酯於不同浓度之氯化锡/甲醇潜溶剂(0g/100g、3g/100g、5g/100g、7g/100g及9g/100g)中的质传及水解行为,并利用成功制得之聚甲基丙烯酸甲酯/二氧化锡奈米复合材料,进一步探讨奈米复合材料之光学性质、机械性质及热性质。

We then used a selection process incorporating microarrays and/or real-time PCR analysis of tissue samples to further test marker candidates for maximum methylation in CRC tissue and minimum amplification in tissues from both healthy individuals and patients with other diseases.

然后,我们进行进一步的实验,就是利用芯片技术和荧光定量PCR方法发现候选标志物,这种标志物最大可能性的在结直肠癌组织的发生甲基化,而最小可能的在健康人和其他疾病时发生甲基化。

Washing oil distillate from coal tar is rich in such valuable organic chemical materials as quinoline,α-methyl-naphthalene,β-methyl-naphthalene, diphenyl, indole, acenaphthene, fluorene, etc.

煤焦油洗油馏分中富含喹啉、α-甲基萘、β-甲基萘、联苯、吲哚、苊、芴等宝贵的基本有机化工原料,介绍了这些组分的分离提取及其在精细化工中的应用,煤焦油的深加工对资源综合利用及精细化工的发展具有重要意义。

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Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地,使人们普遍认识到发展不能以牺牲农业为代价。

Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。