甲基

The results indicate that [(L 1) 2SnEt 2] can selectively bind to the N 1 atom of the base and the phosphate oxygen atom of AMP and may further destroy the helical structure of DNA, while the dimethyltin compound of 1,3 dimethyl 4 acetyl 5 pyrazolone [(L 1) 2SnMe 2] merely binds to the the phosphate oxygen atom of AMP and causes the contraction of DNA helical structure.

结论3 二甲基 4 乙酰基 5 吡唑酮的二乙基锡配合物(L1 ) 2 SnEt2 可与AMP 的碱基N1 和磷酸根氧原子螯合并可能会破坏DNA 的双股螺旋结构；而二甲基锡配合物(L1 ) 2 SnMe2 易与单核苷酸的磷酸氧结合，难以与单核苷酸的碱基氮原子稳定结合且只引起DNA 双股螺旋的收缩

Two novel pyrazolone derivatives 2-ethylamino-6H-5-(1-phenyl-3-methyl/phenyl-5-pyrazolone-4-ylene)-1,3,4-thiadiazine (PMCP-ETSC/DPCP-ETSC) containing NNS six-membered heterocycles were synthesized by the condensation reaction of 1-phenyl-3-methyl/phenyl-4-chloroacetyl-pyrazolone-5 with 4-ethyithiosemicarbazide. The title compounds were characterized by elemental analysis, IR, 1H NMR, 13C NMR and single-crystal X-ray diffraction.

利用1-苯基－3-甲基／苯基－4-氯乙酰基－吡唑啉酮－5与4-乙基氨基硫脲发生缩合反应，生成了2个新的双杂环化合物2-乙氨基－6H-5-（1-苯基－3-甲基／苯基－5-吡唑啉酮－4-基）－1，3，4-噻二嗪(PMCP-ETSC/DPCP-ETSC)，并对其进行元素分析、红外光谱、核磁共振表征和晶体结构分析。

In order to search for the new pyrazolyl-heterocycles lead compounds, eight pyrazolyl- were synthesized from 3-ethyl-1-methyl- 4-substituted-5-pyrazolecarboxylic acid chloride and nitrogen heterocyclic rings such as 3-methyl-5-pyrazolone, 1H-3-ethyl-5-pyrazole ester, etc.

为了寻求新的含吡唑双杂环先导化合物，用 4 取代 1 甲基 3 乙基 5 吡唑甲酰氯与 3 甲基 5 吡唑酮、3 乙基 5 吡唑甲酸乙酯等含氮杂环反应得到了 8个新的含吡唑环的双杂环类化合物。

Methyl - 2- pyridyl） merhylenerhodanine ; Gold.

5－（3－甲基－2－吡啶）；亚甲基若丹宁；金；光度法

Secondly,UV spectrophotometry was adopted to research the combination action on SM_2 and SIZ with MAA and 4-Vp.The combination action of functional monomer with template molecules were produced in the results. Then,the prediction imprinting principle of SM_2 and SIZ were given. The diagrams of infrared spectrum were analysed in MAA and 4-Vp and IMPs of SM_2. It was discoved that the absorbability peak of C=C function group in the IMPs were turn to be very low ,but the function group of carboxylic acid and pyridyl in the IMPs were no evidence change, and the condition was created in the molecular recognition of MIPs. Thermal Analysis was adopted to research IMPs ,in which ,a better thermal stability and its decompose temperature were showed in the results.

其次，本文利用紫外分光光度法研究磺胺二甲嘧啶和磺胺异噁唑与甲基丙烯酸或4-乙烯基吡啶的结合作用，结果表明，溶液中的功能单体与模板分子之间产生了结合作用，并预测磺胺二甲嘧啶和磺胺异噁唑印迹机理；分别分析了功能单体甲基丙烯酸、4-乙烯基吡啶、磺胺二甲嘧啶和磺胺异噁唑分子印迹聚合物的红外谱图，经过对比发现制得的印迹聚合物中C=C双键峰很小，并且功能键羧酸键和吡啶氮没有明显变化，这为聚合物特异识别特性创造了条件；利用综合热分析仪，对分子印迹聚合物进行综合热分析，结果表明分子印迹聚合物具有较好的热稳定性，分解温度也较高。

On the basis of these principles and requirements,in this paper,a new modifier has been synthesized from pyromellitic dianhydride and thiosemicarbazide by the nucleophilic addition of anhydride,the cyclization of acyl thiosemicarbazide in alkaline solution,and the N-hydroxymethylation of the triazole-thione.

本文根据这一思路，以均苯四甲酸二酐和氨基硫脲为起始原料，通过酸酐的亲核加成反应、酰氨基硫脲的碱性环化反应、三唑硫酮环的N-羟甲基化反应合成出了一种新的N-羟甲基三唑硫酮酸改性剂。

The preparation process for methacrolein and methyl methacrylate by oxidation method was studied in a fixed-bed reactor and a slurry reactor respectively with raffinate C4 fractions by-product of ethylene plant as raw materials.

以乙烯装置副产的抽余C4馏分为原料，分别在固定床反应器和浆态床反应器上考察了甲基丙烯醛和甲基丙烯酸甲酯的氧化法制备工艺。

The result showed that the dosage of 5000 IJs/plant was the best one among the 8 dosages, the average of injured legume (3.l%) with BPS was significant lower than that of 40% isofenphos-methyl solution (9.0%) and than that of tap water (53.2%). The rate of grub decrease (95.7%) and the dry weight of peanut (5941.5 kg/ha) with BPS were significant different (P.05) to that of with 40% isofenphos-methyl solution (82.7%, 303.8 kg). The application of BPS was better with irrigation than with spray. At the dosage of 5000 IJs/plant, the combination of BPS and Rhabditis sp.(4500:500) did not show conflictive, coordinate or synergistic effect to grub control.

结果显示：在8个处理剂量中，以5000 IJs/穴的剂量田间效果最好，花生荚果受害率(3.1 %)显著低于40 %甲基异柳磷对照的(9.0 %)和清水对照的荚果受害率(53.2 %)，蟒螬减退率(95.7%)和平均产量(5941.5 kg/hm^2)也与40%甲基异柳磷对照的(82.7%， 303.8 kg)有显著差异(P.05)；灌施效果显著好于喷施；在5000 IJs/穴的剂量下，混合喷施BPs线虫和小杆线虫(4500：500)，未表现出相克、协同或加性效应。

It is well known that isorhamnetin is used in clinic to cure coronary artery diseases, rhamnetin is used as a fine anti-inflammatory, and these medicines are just such methylated products.

本课题通过对槲皮素甲基化的研究，力求得到五个不同位置的甲基化反应产物。

Use D4 or DMC,vinyl di-blocking agent,ringy vinyl,hexamethyl-disiloxane as raw materials,tetramethyl hydroxyl ammonium as catalyst,we synthesized a vinyl silicone oil.

以D4，乙烯基双封头，乙烯基环体，六甲基二硅氧烷等为原料，四甲基氢氧化铵为催化剂合成了摩尔质量和乙烯基含量不同的乙烯基硅油；以高含氢硅油，含氢双封头，D4合成实验所需的含氢硅油；以白碳黑为填料通过密炼等工序制备了医用高透明液体注射硅橡胶。

My first article for Screen Power Magazine, which is to this day is the official magazine of Jackie Chan, was a DVD review of the Hong Kong actioner Gen-X Cops, starring Nicholas Tse and Daniel Wu.

我的第一篇文章为屏幕力量杂志，在对这天是Jackie Chan 正式杂志，是香港actioner Gen X 警察的DVD 回顾，担任主角Nicholas Tse 和丹尼尔吴。

His lips grazed hirs, Now what are you going to do?

他的唇使吃草了 hirs，现在你将要做什麼？