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The catalytic transformation pathway can change to decrease the yield of hydrogen and yield methyl-contained sulfides such as methyl mercaptan, dimethyl sulfide and dimethyl disulfide, but overlarge concentration of methanol would holdback the transformation of isobutyl mercaptan. The transformation of isobutyl mercaptan was favorable if the volume ratio of methanol and benzene was 0.2.The addition of methanol assume certain effect on the catalytic cracking of di-n-butyl sulfide in solvent benzene but without changing the cracking reaction mechanism of di-n-butyl sulfide.

甲醇也可以使异丁硫醇的催化转化路径发生改变降低硫化氢的产率,生成甲硫醇、甲硫醚及二甲基二硫化物等含甲基硫化物,但甲醇的浓度过高会抑制异丁硫醇的转化,在反应体系中当甲醇的体积占到溶剂苯体积的20%时对异丁硫醇的转化较为有利;甲醇的添加对丁硫醚在溶剂苯中的催化裂化有一定影响,但没有改变丁硫醚的裂解反应历程。

This thiosemicarbazide was treated under the catalysis of glacier acetic acid,mercuric acetate giving 2 benzyl 5 phenylamino 1,3,4 thiodiazole and 2 benzyl 5 phenylamino 1,3,4 oxadiazole respectively.

然后分别将其在冰醋酸、醋酸汞存在下关环,制得 2 苯甲基 5 苯胺基 1,3 ,4 噻二唑与 2 苯甲基 5 苯胺基 1,3 ,4 口恶二唑

The graft copolymerization of acryalmide and methyl acrylacyl oxyethyl trimethyl ammonium chloride onto chitosan under microwave radiation was studied. The effect of synthesis conditions on graft ratio and graft efficiency, on the strengthening efficacy of the product for wheat straw pulp was studied.

摘 要:研究了用微波辐射的方法进行壳聚糖和丙烯酰胺及甲基丙烯酰氧乙基三甲基氯化铵的接枝共聚反应,讨论了反应条件与产物的接枝效果对麦草浆的增强作用的影响。

To obtain a flocculant which could effectively remove dyes from dyeing wastewater , the amphoteric polymer was prepared by copolymerization of acrylamide, acrylic acid, cationic monomer and dmethyldiallylammonium chloride or acryloyl oxyethyl trimethyl ammonium chloride.

为制备一种对染色废水有显著脱色效果的絮凝剂,采用溶液聚合法,将两种阳离子单体二甲基二烯丙基氯化铵和丙烯酰氧乙基三甲基氯化铵分别与丙烯酰胺,丙烯酸共聚,合成了两性聚合物。

Five chalcones were synthesized via the aldol condensation reaction of acetophenone or parasubstituted acetophenones with 1-phenyl-3-methyl-5-phenoxyl-pyrazol-4-aldehyde, which reacted with two kinds of hydrazine in glacial acetic acid under refluxing to give a series of bipyrazoline derivatives. In this synthetic course, glacial acetic acid is not only a solvent, but also a catalyzer.

以1-苯基-3-甲基-5-苯氧基-吡唑-4-甲醛为原料,与苯乙酮发生羟醛缩合,生成相应的查尔酮,再在冰醋酸中与不同的肼反应,高产率的合成出10种新的5位含1-苯基-3-甲基-5-苯氧基-吡唑基的吡唑啉类衍生物。

Methods:2-Hydroxy-4-methyl-3-nitropyridine was reacted with phosphorous pentachloride to give 2-chloro-4-methyl-3-nitropyridine.

以4-甲基-3-硝基-2-羟基吡啶为起始原料,与五氯化磷进行卤代反应制得4-甲基-3-硝基-2-氯吡啶。

Our study show that 9, 11-Octadecadienoic acid, methyl ester is the highest content of organic acid ester components in non-hydrocarbon fraction, higher content of 6-Octadecenoic acid, methyl ester reflects mainly terristrial source input, higher content of pentadecane acid, 14-methyl, methyl ester or Heptadeeanoic acid, 16-methyl, methyl ester shows mainly aquatic source input.

原油和岩石抽提物非烃中有机酸酯类化合物的有机地球化学研究报道很少,系统研究发现非烃有机酸酯中9,11-十八二烯酸甲酯含量最高,而次高峰的丰度可用作生源判识,陆源母质输入多的样品次高峰为6-十八单烯酸甲酯,水生母质供给多者次高峰为14-甲基十五烷酸甲酯或16-甲基十七烷酸甲酯。

In solid phase process, the polyiodides, which include triiodide, pentaiodide, heptaiodide, nonaiodide and undecaiodide tetra-n-butyl ammonium iodide, tetrabutyl ammonium bromide and tetramethyl ammonium iodide poly-compounds, were synthesized by the low-heat solid phase reaction between iodine and tetra-n-butyl ammonium iodide, tetrabutyl ammonium bromide or tetramethyl ammonium iodide; In complexation process, solution polyiodides were synthesized by complexing action of different agents; In resinifying process, triiodide, pentaiodide, heptaiodide resinic polyiodides were synthesized by ion-exchange when the strong basicity styrene anion exchange resin, potassium iodide and iodine were used as raw materials.

固相法是用正四丁基碘化铵、四丁基溴化铵或四甲基碘化铵分别与碘作用,通过低热固相反应,合成出碘三、碘五、碘七、碘九和碘十一形式的正四丁基碘化铵、四丁基溴化铵或四甲基碘化铵的系列高聚碘化合物;在络合法合成溶液高聚碘的实验中,选用几种络合剂通过络合作用首次合成了溶液高聚碘;树脂法合成高聚碘的实验是采用强碱性苯乙烯系阴离子交换树脂、碘化钾和碘为原料,通过离子交换,合成了碘三、碘五和碘七形式的树脂高聚碘。

Ethyl alcohol, 3-methyl-4-oxo- pentanoic acid, acetic acid butyl ester, 2-methyl-butanoic acid ethyl ester, diethyl phthalate,-2,4-Decadienal were the same volatiles d from the 10 cultivars.

其中共有组6种,为乙醇、3-甲基-4-羰基戊酸、乙酸丁酯、2-甲基丁酸乙酯、邻苯二甲酸二乙酯、-2,4-癸二烯醛。

A new method for the synthesis of 1 methyl 3 propyl pyrazol e 5 carboxlic acid from 2 pentanone and diethyl oxalate is reported.

以 2 -戊酮和草酸二乙酯为起始原料,经缩合、与甲基肼环合、水解等三个步骤合成了 1 -甲基-3-丙基吡唑-5 -羧酸。

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