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ConclusionThe main components of essential oils are 2,4-bis(1,1-dimethylethyl) phenol (4.4%), tetradecanoic acid (6.96%), n-hexadecanoic acid (7.69%), 9,12-cctadecadienoic acid (6.37%), hexadecanoic acid-2-hydroxy-1- ethyl ester (4.79%) and octadecanoic acid-2-hydroxy-1- ethyl ester (4.77%), respectively.

结论阿给炭挥发油的主要成分为2,4-二树丁基苯酚(4.4%)、十四酸(6.96%)、n-十六酸(7.69%)、-9,12-十八碳二烯酸(6.37%)、软脂酸-2-羟基-1-羟甲基乙酯(4.79%)、硬脂酸-2-羟基-1-羟甲基乙酯(4.77%)。

The technological conditions with methylacrylic acid and hexadecanol as raw-material and the synthesis of hexadecyl methylacrylate by direct-esterification are studied.

研究了以α-甲基丙烯酸和十六醇为原料采用直接酯化法合成α-甲基丙烯酸十六酯的工艺条件。

Dihydrojasmone was synthesized from2-hexyl-5-methyl-1,2-oxaborolane,prepared frommethyl vinyl ketone and hexene,via the homologationwith 〓 followed by PCC oxidation and intra-molecular condensation.In stead of the oxidation ofthe C-B bond of 1,2-oxaborolane,fluoride inducedhalogenation of 2-alkoxy-1,2-oxaborolane was found togive 3-halopropanol.

硼氢化甲基乙烯基酮和已烯得到的2-已基-5-甲基-1,2-氧硼杂环戊烷与〓反应,再经PCC氧化,分子内缩合得到二氢茉莉酮。1,2-氧硼杂环戊烷的C-B键除氧化断裂之外,也能够在〓或KF作用下卤化断裂成碳卤键。

The alternative method of O-demethylation,methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

方法在以蒂巴因为原料,经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中,分别采用甲磺酸/DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

By the hydrolyzation of MePhSiCl_2 and Me_2SiCl_2, polymethylphenylsilicone rubber can be obtained.

同时对比了甲基苯基硅橡胶和二甲基二苯基硅橡胶耐辐照性能的好坏。

Based on the principle of ester hydrolyzation to ether in alkali condition, the process for preparation of dimethyl sulfide from sodium methyl sulfate residue was investigated.

根据酯在碱性条件下水解反应生成醚的原理,研究了以甲基硫酸钠废渣为原料制备二甲基硫醚的方法。

The light and thermal stability of methyl orange anion-pillared hydrotalcite was enhanced to a considerable extent, comparing with that of methyl orange.

该超分子结构材料不仅保持了甲基橙本身的颜色,而且与甲基橙相比,其耐光性和耐热性均有大幅度的提高。

Investigation of major metabolic pathways of SFZ-47 in animals The metabolites of SFZ-47 in rabbit urine following oral administration were separated and detected with HPLC and LC-MS methods. On the basis of the chromatographic behavior and mass spectra of the metabolites as well as biotransformation pathways of drugs with the partial structure of SFZ-47, the hydroxylic derivative 4-(3H-1, 2- dihydro-1-pyrrolizinone-2-methylamino benzyl alcohol and the carboxylic derivative 4-(3H-1, 2-dihydro-1-pyrrolizinone-2-methylamino benzoic acid of SFZ-47 were proposed as two potential metabolites and were synthesized.

在动物体内主要代谢途径的确定用HPLC和LC-MS对家兔口服SFZ-47后尿中的代谢物进行了分离、检测,根据代谢产物的色谱和质谱行为以及与SFZ-47有类似结构部分的其它药物的代谢途径,推测其羟基衍生物[4-(3H-1,2-二氢-1-吡咯里嗪酮-2-甲基胺基)苯甲醇]与羧基衍生物[4-(3H-1,2-二氢-1-吡咯里嗪酮-2-甲基胺基)苯甲酸]是两种可能的代谢产物,遂用化学方法合成了这两种衍生物。

In the synthesis of canthaxanthin by selective catalylitic oxidating of βcarotene,CO2 was used as acidifying or alkalizing agent,which controlled reacting system acidity and protected polyene.,producing less by-products and increasing catalylitic oxidation selectivity.In the addition reaction of isoprene with hypochloric acid,1-chloro-2-methyl-3-buten-2-ol and l-chloro-2-methyl-3-buten-4-ol were made by controlling of the acidity with carbon dioxide i...

CO2作为酸碱调节剂和惰性气体,在β-胡萝卜素催化氧化合成角黄素反应中,可以控制反应体系酸性,保护原料中的双键,减少副反应发生,提高催化氧化反应的选择性;异戊二烯氯醇化生成1-氯-2-甲基-3-丁烯-2-醇和1-氯-2-甲基-3-丁唏-4-醇反应中,CO2代替有机酸作酸碱调节剂,控制次氯酸的生成速度,达到调控反应的目的,反应条件温和,不副产固体。

Aniline-BP was used as CTC system to initiate the polymerization ofMMA under UV irradiation, PMMA prepolymer with aromatic imino endgroup was prepared.

以苯胺-BP为CTC体系,在紫外光辐射下,引发甲基丙烯酸甲酯聚合,得到了含有芳亚胺端基的聚甲基丙烯酸甲酯预聚物。

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我的第一篇文章为屏幕力量杂志,在对这天是Jackie Chan 正式杂志,是香港actioner Gen X 警察的DVD 回顾,担任主角Nicholas Tse 和丹尼尔吴。

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他的唇使吃草了 hirs,现在你将要做什麼?

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