甲基

The result of immobilization showed that hydrophile membranes were more advantageous than hydrophobe ones to act as immobilization carrier. Crosslinking organophosphorus hydrolase by glutaraldehyde on polyethersulfone membrane is a simple and practical immobilization method. An appropriate amount of bovine serum albumin and crosslinker is necessary to get a good result of immobilization. In the biodegradation of methyl-parathion through enzyme membrane reactor, the effect of immobilized enzyme amount, flow rate of peristaltic pump, pH of the feed, and the methyl-parathion concentration on biodegradation rate was studied. It was shown that the biodegradation rate increased with immobilized enzyme amount and substrate concentration. Biodegradation rate didn't increase when the folw rate of the peristaltic pump was larger than 7 ml/min.

然后，研究固定化酶降解甲基对硫磷，从不同材料的膜载体固定有机磷水解酶的比较中，发现亲水膜比疏水膜适合作固定化酶载体；在此基础上，将有机磷水解酶固定在聚醚砜微滤膜上，并制成酶膜生物反应器，用于降解甲基对硫磷；戊二醛化学交联法固定时，酶液与10%牛血清白蛋白溶液的比例在3：1~2：1，与交联剂的比例在7：2~7：4范围内，固定化效果较好，并发现牛血清白蛋白和膜载体有降低酶活损失的作用；将固定化的酶膜装于酶膜反应器降解甲基对硫磷，实验结果表明：反应器的降解速率与固定化酶量呈正比，也随底物浓度的增加而加快，当流速低时，降解速率随流速增大而加快，到7ml/min以上时，降解速率不随流速脑黾佣洌到獾淖畹团ǘ任？

Fixation of direct dyes with silica gel ;2. Taking advantage of proof salt and high hydrophilic property of the silica gel and the carboxymethyl cellulose inarch polysalt of the super water-absorbent resin recombination,this paper made use of the water-absorbent composite form the inorganic polymer, sequentially advanced water-absorbent velocity and capacity of polymer water-absorbent resin in the brine.

利用具有良好耐盐和高亲水性能的硅凝胶与羧甲基纤维素接枝聚丙烯酸盐的高吸水树脂进行复合，制备出无机高分子的硅凝胶-羧甲基纤维素接枝聚丙烯酸盐耐盐高吸水复合材料，从而提高了高分子吸水树脂在盐水中的吸收能力及吸收速度，研究了复合材料的吸盐水性能，通过扫描电子显微镜观察了复合材料表面的微观结构，初步探讨了硅凝胶-羧甲基纤维素接枝聚丙烯酸盐耐盐高吸水复合材料的吸盐水机理。

Xinquan HuTwo new chiral backbones R-- and S--2-amino-2"-hydroxy-4,4",6,6"-tetra methyl-1,1"-biphenyl were synthesized via nitration, diazotation/iodination, Ulhnann coupling, selective reduction, diazotation/hydrolysis, hydrogenation and resolution from 2,4-dimethyl-aniline in seven steps.

以2，4-二甲基苯胺为起始原料，经过硝化反应、重氮化碘代反应、Ullmann缩合反应、选择性双硝基单还原反应、重氮化水解反应、催化氢化反应和拆分，首次合成了--2-氨基-2'-羟基-4，4'，6，6'-四甲基-1，1'-联苯和--2-氨基-2'-羟基-4，4'，6，6'-四甲基-1，1'-联苯两个对映体。

Racemic backbones 2-amino-2'-hydroxy-6,6'-dimethyl-l,l'-biphenyl la and 2-amino-2'-hydroxy-4,4',6,6'-tetramethyl-l,1'-biphenyl 1b were synthesized from o-methylaniline and 2,4-dimethylaniline via nitration, diazotation/iodination, Ullmann coupling, selective reduction, diazotation/hydrolysis and hydrogenation.

从邻甲苯胺及2，4-二甲基苯胺出发，经过硝化，重氮化-碘代，偶联，单还原，重氮化-水解及还原反应合成了消旋体骨架2-氨基-2'-羟基-6，6'-二甲基-1，1'-联苯1a和2-氨基-2'-羟基-4，4'，6，6'-四甲基-1，1'-联苯1b。

A mild and convenient method for the synthesis of 4(3)-substituted 3(4)-nitro-1H-pyrroles and 3-substituted 4-methyl-2-tosyl-1H-pyrroles from nitroolefins and tosylmethyl isocyanide in ionic liquid 1-butyl-3- methylimidazolium bromide was developed.

本文以离子液体－溴化1-丁基-3-甲基咪唑为溶剂，采用对甲苯磺酰基甲基异腈与硝基烯反应生成4(3)-取代-3(4)-硝基-1-氢吡咯或3-取代-4-甲基-2-对甲苯磺酰基-1-氢吡咯。

A HPLC method has been developed for the simultaneous determination of 4-methylbenzy- lalcohol,p-tolualdehyde,4-caboxybenzaldehyde,benzoic acid,p-toluie acid,terephthalic acid,o- phthalic acid and isophthalic acid in the residue from purification of terephthalic acid.

其残渣中含有再利用价值很高的中间产物：4一甲基苯甲醇(4一MBA)，对甲基苯甲醛(P一tolual-dehyde)，4一竣基苯甲醛(4一CBA)，苯甲酸，对甲基苯甲酸，对苯二甲酸，邻苯二甲酸，间苯二甲酸等。

The increase in the methylene resonance signal intensity which reflects the alterations in membrane lipids and accordingly in the biophysical and biochemical characteristics of cell membrane during apoptosis was found to be closely associated with nuclear changes as detected by DNA laddering assay and the TUNEL procedure.

在用烟酰胺处理的烟草细胞中，亚甲基信号强度的增加与DNA Ladder几乎同时出现，随诱导时间的延长，亚甲基信号强度也逐渐增大，在24 h亚甲基信号强度增加约2倍。

To avoid the low yield in direct hydrosilylation addition of allyamine, 1, 1, 1, 3, 3, 3-hexamethyldisilazane is used to protect the amino groups, and the protective groups are removed easily after hydrosilylation addition, then the high yield of ladderlike copolymethyl-aminpropylsilsesquioxane was obtained.

为了克服将烯丙基胺直接与聚氢基甲基倍半硅氧烷进行硅氢加成反应接枝效率低的缺点，探索用六甲基二硅氮烷对烯丙基胺预保护，硅氢加成反应后再脱保护，从而以较高产率制备了含胺丙基、甲基的反应性梯形共聚倍半硅氧烷。

The photodegradation of methylic orange under UV light irradiation in aforementioned photocatalyst were studied.

通过对甲基橙光催化的研究表明：在同样条件下，TiO2-PEG400颗粒的甲基橙光降解效果明显优于其他颗粒，甲基橙光降解率最高达到97。

A "benign"/adult form of methylmalonic acidemia is associated with increased, albeit mild, urinary excretion of methylmalonate secondary to impaired activity of the enzyme methylmalonyl-CoA mutase; individuals seem stable but may have acute metabolic decompensation.

一种&良性&／成年人的甲基丙二酸血症是由于甲基丙二酰辅酶A变位酶酶活力受损引起的，伴随着逐渐增加的，虽然是慢性地，尿排泄甲基丙二酸盐；患者病情看似稳定但是可能会出现急性的代谢失代偿。

Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在，所有的孩子都要在综合学校继续学习，所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地，使人们普遍认识到发展不能以牺牲农业为代价。