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Cinnabarinus at 150 mg/L.The influences on bioactivity of substituted pyrazole and pyrimidine were discussed respectively: pyrazoles substituted with phenyls at 3 position had higher activity than thiophen and compounds with R_1=methyl had higher activity than that with R_1= hydrogen, pyrimidines substituted with methyl at 2 (R_3) and 5 (R_3) position and phenyl at 6 position were most active.

本论文对吡唑及嘧啶取代基对活性的影响分别进行了讨论,可知:吡唑3位为取代苯基的化合物杀菌活性优于取代噻吩的,吡唑4位(R_1)为甲基的杀菌活性高于R_1为氢的活性;嘧啶的2位(R_3)为甲基,5位(R_1)为甲基,6位为无取代基的苯基时活性最好。

Methacryloyloxydecyl-2-thiouracil-5-carboxylate was synthesized from the reaction of thiouracil with diethyl ethoxymethylene malonate and ω-hydroxy-decyl-methacrylate.

以硫脲、乙氧基次甲基丙二酸二乙酯和甲基丙烯酸ω-羟癸酯为主要原料合成了一种新的粘接性单体10-甲基丙烯酰氧癸基-2-硫脲嘧啶-5-羧酸酯。

In this paper, 2,6-dimethyl-1,4-phenylene oxidel was modified by trimethyl chlorosilane and triphenyl chlorosilane, and a serfes of silyl-substituted PPO were synthesized.

讨论了聚2,6-二甲基-1,4-苯撑氧与三甲基氯硅烷和三苯基氯硅烷的反应,合成了一系列取代含量不同的三甲基硅取代PPO和三苯基硅取代PPO。

Veratrum aldehyde synthesis of many drugs intermediates, methyl aldehyde method for raw materials in Champlain, after dimethyl sulfate methylation available to 20% sodium hydroxide as the solvent, 10-11 in the PH value of the under the conditions of synthesis; microwave irradiation is the use of microwave radiation heating to replace the traditional approach to synthesis of a product of methylation reactions, this method does not require solvents, and less by-products, but still need to use 15% sodium hydroxide to adjust pH.

藜芦醛是许多药物合成的中间体,甲基化法以香兰醛为原料,经过硫酸二甲酯甲基化可得,以20%氢氧化钠为溶剂,在PH值为10-11的条件下合成;微波辐射法是利用微波辐射代替传统加热方式进行甲基化反应合成产物,这种方法不需要溶剂,并且副产物少,但仍需要用15%氢氧化钠来调节酸碱度。

This paper details an efficient method for a one-step transformation of the trityl ether to the acetonide. Treatment of trityl ether with a mixture of trifluoroacetic acid, 2,2-dimethoxy propane and camphorsulfonic acid as catalyst in dichloromethane through detritylation followed by acetonization gave the acetonide in high yield.

介绍了一种新的高效的由三苯甲基醚直接生成丙酮化合物的方法,也就是使三氟乙酸条件下脱三苯甲基的反应和生成丙酮化合物的反应在一个反应瓶中同时进行,使脱三苯甲基作用后生成的醇继续反应得到高产率的丙酮化合物。

Hrough copolymerization of styrene with few quantity of methacrylic acid, maleic anhydrate or 4-vinyl pyridine respectively and of butyl methacrylate with maleic anhydrate, the functional groups carboxyl, simple anhydride and pyridyl have been introduced respectively to the chain of PS or PBma.

通过苯乙烯与少量的甲基丙烯酸、马来酸酐或4—乙烯基吡啶的共聚及甲基丙烯酸正丁酯与马来酸酐的共聚,可在聚苯乙烯及聚甲基丙烯酸丁酯链上分别引入功能基因羧基、酸酐基和吡啶基对共聚物进行了红外光谱、酸碱滴定、元素分析、玻璃化转变温度、粘度及紫外光谱的测定。

After the carboxymethylation,the solubility of pachyman in the water was significantly increased,its β-D-glucan characteristic absorption peak at 890 cm-1 became weak obviously,and its methylene vibration absorption peak and CO antisymmetrical stretch vibration absorption peak appeared at 1 333 and 1 606 cm-1 respectively,which indicated that the carboxymethylation succeeded.The analysis of AFM results showed that CMP molecules existed in different morphology under different solution conditions,and that the concentration,ionic strength and solvent physical chemistry characteristics of polysaccharide solution had effects on the CMP chains conformation and the action mode between different molecular chains.The phenomena were considered to be related to hydrogen bond association and intramolecular and intermolecular electrostatic interactions of CMP.

结果表明:经过羧甲基修饰,茯苓多糖在水中的溶解性显著增加,890 cm-1 处的β-D-葡聚糖特征吸收峰明显减弱,1 333 cm-1 处出现次甲基振动吸收峰,1 606 cm-1 处出现〖JG(〗C〖ZJLX,Y〗O〖JG)〗非对称伸缩振动吸收峰,表明羧甲基化成功;原子力显微镜分析表明:在不同溶液条件下,CMP分子以不同形态存在,多糖溶液的浓度、离子强度及溶剂的物化特性均能对CMP的分子链构象及链间相互作用形式产生影响,推测可能与CMP分子内、分子间的氢键缔合及静电作用有关,CMP分子与云母基底间的吸附及静电作用也会对CMP的分子链构象及图像质量产生影响。

Water,butylene glycol,glycerin,glyceryl polymethacrylate,triethanolamine,carbomer,ppg-26-bueth-26,chondrus crispus,peg-40 hydrogenated castor oil,phenoxyethanol,imidazolidinyl urea,propylene glycol,benzophenone-4,retinyl palmitate,citrus aurantiudulcisoil,phospholipids,methylparaben,tocopheryl acetate,c12-23 alkyl lactate,disodium EDTA,centella asiatica extract,iris germanica root extract,pentadecalactone,aloe barbadensis leaf juice,mimosa tenuiflora bark extract,sodium hyaluronate,menthol,biosaccharide gum-1,citrus aurantium amara oil,propylparaben,methylchloroisothiazolinone,sodium benzoate,potassium sorbate,citric acid,calcium sorbate,methylisothiazolinone,butylparaben,ethylparaben,yellow 5(CI 19140),limonene,linalool

水,丁二醇,甘油,甘油聚甲基丙烯酸酯,三乙醇胺,卡波姆,PPG-26-丁醇聚醚-26,鹿角菜胶,PEG-40 氢化蓖麻油,苯氧乙醇,尿素醛,丙二醇,二苯酮-4,维他命A酯,甜橙油,磷脂质,羟苯甲酯,醋酸盐维他命E,C12-13 烷醇乳酸酯,乙二胺四乙基二钠,雷公根萃取,鸢尾花根萃取,环十五内酯,吉拉索芦荟叶汁,含羞草萃取,透明质酸钠,薄荷脑,多醣物质,苦橙油,羟苯丙酯,甲基氯异塞唑晽酮,苯甲酸钠,山梨酸钾,柠檬酸,山梨酸钙,甲基异噻唑啉酮,羟苯丁酯,羟苯乙酯,柠檬黄,柠檬精油,沈香醇水:几乎所有护肤品成分第一位都是水。丁二醇:保湿剂及溶剂,质地温和

Lower mercury methylation was expected in these two reservoirs.With the development of reservoir,it is possible that the methylmercury concentrations will increase due to autochthonous and extraneous organic materials,and methylmercury may be released due to thermal stratification.But this was not confirmed.

通过研究发现目前库区环境汞的甲基化率低,但随着水库生态系统的不断演化,内源和外源营养物的输入及水体在温度分层其间自身甲基汞的形成,导致水体甲基汞含量的逐渐增加,但仍需进一步的研究证实。

However, analysis of DNA methylation level indicated that the total DNA methylation levels were not significantly different between diploid and autotetraploid. Autotriploid showed a trend of low DNA methylation level. It implied that the alterations of DNA methylation levels were not linear with the autopolyploidy level in watermelon.

有趣地是,二倍体与四倍体西瓜相比DNA甲基化水准却未发生大规模的调整,而三倍体西瓜显示出较为明显的低DNA甲基化水准趋势,表明西瓜同源多倍化过程中其基因组DNA甲基化水准变化与其倍性不成线性关系。

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Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在,所有的孩子都要在综合学校继续学习,所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地,使人们普遍认识到发展不能以牺牲农业为代价。

Detailed Intrinsic Reaction Coordination calculations were carried out to guarantee the optimized transition-state structures being connected to the related tautomers.

同时,做了详尽的内禀反应坐标计算,以保证所得到的过渡态连接相应的始末异构体。