甲下的

Under the conditions without air, oxygen may adsorb on the I-modified surface of electrolytic silver.

在甲醇和氧共吸附的情况下，表面可以检测到甲氧基和甲酸根。

Methods This title compound was prepared using the O-phenylene diamine and the anisaldehyde as the raw material,methanol as the solvent,and the phosphoric acid makes the oxidant.

方法本课题以邻苯二胺和对甲氧基苯甲醛为原料，在甲醇为溶剂，磷酸为催化剂的酸性条件下，一步反应制得2-(4-甲氧基苯基)苯并咪唑。

Meanwhile, cyanosis of lips, purplish tongue, varicose sublingual vein, flaccidity of lower extremities, hemianesthesia, headache, blackish eyelids, dispiritedness, tongue with ecchymosis, dysphasia, blackish complexion, squamous and dry skin, pain on the paralytic limbs, dermorrhagia, and distension of stomach and abdomen are more influential symptoms and signs.

同时，在相关的临床症状和体征的多元线性逐步回归分析中发现，唇色紫暗、舌质紫暗、舌脉曲张、下肢肌力减弱、偏身麻木、头痛，睑下青黑、精神萎靡、舌有瘀斑、言謇失语、面色晦暗、肌肤甲错、瘫肢疼痛不移、肌肤青紫/有瘀斑及脘腹胀满对脑梗塞血瘀证诊断的影响较大；将单因素分析有显著性意义的症状、体征变量，代入贝叶斯逐步判别分析，结果发现唇色紫暗、舌脉曲张、爪甲紫暗、偏身麻木、舌质紫暗、言謇失语、睑下青黑、头痛、瘫肢温度降低、下肢肌力下降等对血瘀证的诊断能力较强，而且在随后的交互检验中也显示了较好的稳定性。

In our paper,1-hexylcarbamoyl-5-fluorouracils and1-cyclohexyl-carbamoyl-5-fluorouracils were prepared through 5-fluorouracil reacting with hexyl isocyanate or cyclohexyl isocyanate by using dimethylaminopyridine as the catalyst.

以5-氟尿嘧啶(5-FU)、正己基异氰酸酯和环己基异氰酸酯为原料，在N，N-二甲氨基吡啶的催化下，通过N-脲化反应制成1-己基氨基甲酰基-5-氟尿嘧啶及1-环己基氨基甲酰基-5-氟尿嘧啶。

Part III, 12-benzyl dehydroabietyl thioisocyanate was synthesized from methyl 12-benzyl dehydroabietic acid, by hydrolysis, chloride, Curtius reaction to give isocyanate which was hydr- olysied to amine under acidic condition, and with the method of CS2 at last, the maximal excitat- ion wavelength was bathochromic shifted 14nm compared to DDHA-NCS.

第三部分，从12-苯甲酰基脱氢松香酸甲酯出发，经过水解，酰氯化、Curtius reaction得到异氰酸酯，在酸性条件下水解成胺，最后由二硫化碳法得到一种新的荧光衍生试剂12-苯甲酰基脱氢松香酸异硫氰酸甲酯，与DDHA-NCS相比，最大激发波长红移了14nm。

Study on removal rate of methyl mercaptan and ethanethiol by bio-trickling filter;2. The deodorizing effect of tea functional ingredients on methyl mercaptan (CH3SH) was studied in this investigation.

就茶叶功能成份对主要恶臭成分甲硫醇的去除效果进行了研究，结果表明：绿茶水提取物，儿茶素，EGCG对甲硫醇的去除效果不明显，而茶黄素则表现出较强的活性；在pH10的碱性条件下，1mg含量为40%的茶黄素对甲硫醇的最大去除量为0。

In the presence of alkalinity and tetraethyl ammonium bromide, 2,4-dihydroxy benzophenone reacts with allyl glycidyl ether to form an ethylenic derivative of benzophenone, 2-hydroxy-4-(β-hydroxy-γ-allyloxy) propyloxy benzophenone, which can further undergo hydrosilylation with polyhydromethylsiloxane.

在相转移催化剂四乙基溴化按作用下，利用2，4-二羟基二苯甲酮与烯丙基缩水甘油醚在碱性水溶液中的开环加成反应，合成了中间体4-丙氧基－2-羟基二苯甲酮，将其进一步与聚甲基氢硅氧烷进行硅氢化加成反应。

Furoin was synthesized from furol with VB1 as the catalyst,which was then reacted with acetyl chloride, lauroyl chloride ,benzoyl chloride,α-furoyl chloride and 3-α-furyl acryloyl chloride,respectively;corresponding monoester compounds of furoin were synthesized in THF in the presence of sodium hydroxide under reflux.

以糠醛为基础原料，经维生素B1催化合成糠偶姻，再由糠偶姻分别和乙酰氯、月桂酰氯、苯甲酰氯、α-呋喃甲酰氯和3-α-呋喃烯丙酰氯反应，在NaOH/无水THF体系中，于水浴回流条件下合成了相对应的糠偶姻单酯类化合物。

Four novel methoxycarbonylindole-3-carboxaldehyde phenylhydrazone s were synthesized by the condensation reaction between methoxycarbonylindole-3-carboxaldehyde and phenylhydrazine in acidic condition.

甲氧羰基吲哚-3-甲醛与苯肼在酸性条件下通过缩合反应合成了4个未见文献报道的新化合物甲氧羰基吲哚-3-甲醛苯腙，其结构经1HNMR，IR和MS确证。

Four novel methoxycarbonylindole-3-carboxaldehyde phenylhydrazones were synthesized by the condensation reaction between methoxycarbonylindole-3-carboxaldehyde and phenylhydrazine in acidic condition.

甲氧羰基吲哚-3-甲醛与苯肼在酸性条件下通过缩合反应合成了4个未见文献报道的新化合物甲氧羰基吲哚-3-甲醛苯腙，其结构经1HNMR，IR和MS确证。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。