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A method combining HPLC, a post-column derivation device and a fluorescent detector was used to determine residues of ten carbamate pesticides (aldicarb sulfoxide, aldicarb sulfone, oxamyl, methomyl, 3-hydroxy carbofuran, aldicarb, propaxur, carbofuran, carbaryl and methiocarb) in 68 vegetable and 32 soil samples under four different cultivation systems (traditional kailyard, open field vegetable base, green house and paddy) were collected from a certain city in South Jiangsu.

本研究采用高效液相色谱-柱后衍生-荧光检测法分析了苏南某市4种不同种植方式下(传统菜地、露天蔬菜基地、大棚蔬菜基地和水稻田)68个蔬菜样品和32个土壤样品中10种N-甲基氨基甲酸酯类农药(涕灭威、涕灭威砜、涕灭威亚砜、杀线威、灭多威、残杀威、克百威、3-羟基克百威、甲萘威和灭虫威)的残留量,结果表明在蔬菜中检出的氨基甲酸酯农药残留水平多处于0.2~23μgkg^-1,土壤中为0.1~10μgkg^-1;土壤中3-羟基克百威和灭虫威全部检出,其最高检测浓度分别为10μgkg^-1和1.64μgkg^-1,其他农药仅有少数检出。

Venous blood was drawn from 35 old hypertension patients when blood pressure was nomial and abnormal, respectively. Epinephrine. norepinephine, endothelins, angiotensin Ⅱ and calcitonin-gene-related peptide were determined by radio-immunity. The above five cytokines were also determined in 33 old healthy people. The cytokines levels were compared between the normal and abnormal blond pressure in hypertension patients and also between the old hypertension patients and healthy persons. The correlation between blood pressure and cytokines were analyzed.

35例老年EH患者,血压正常时和血压波动时各抽取静脉血一次,放射免疫法检测肾上腺素、去甲肾上腺素、内皮素、血管紧张素Ⅱ和降钙素基因相关肽水平,同时检测33例健康老年人群各因子水平,比较EH患者血压波动前后各因子水平的差异和血压正常范围时两组人群各因子水平差异,分析不同状态下血压和各因子水平之间的相关性。

MAIN OUTCOME MEASURES: The morphology of BMSCs was observed by the inverted phase contrast microscope. Expression of BMSC surface antigens was detected by flow cytometer. Osteogenous potential was assessed by alkaline phosphatase staining. Adipogenic potential was evaluated by Oil red O staining. Chondrogenic potential was assessed by toluidine blue staining.

主要观察指标:倒置相差显微镜下观察骨髓间充质干细胞的生长状态,流式细胞仪检测细胞表面标志物的表达,采用碱性磷酸酶染色鉴定成骨能力,以油红O染色鉴定成脂能力,以甲苯胺蓝染色鉴定成软骨能力。

RESULTS: HE stained cells were fusiform-shaped with pseudopodia, round or oval nucleus. The cytoplasm was blue after stained with the toluidine blue. The immunohistochemical test revealed that there existed positive expression of type Ⅰ collagen in the cells. In the presence of 10% calf serum, IGF-Ⅰ significantly improved cell proliferative activity in a dose-dependent manner within effective dose range.

结果:苏木精-伊红染色细胞多为梭形,有伪足伸出,细胞核为圆形或椭圆形;甲苯胺蓝染色,胞浆为深蓝色;免疫细胞学方法检测表明纤维环细胞有Ⅰ型胶原表达;在体积分数为0.1的血清条件下,胰岛素样生长因子Ⅰ能提高细胞的增殖活性,并且在有效浓度范围内呈剂量效应关系。

The different enzyme protecting agent had effected on the liquid alkaline protease under the dissimilar condition. Taking the living rate of enzyme as the target, we obtained one high effective alkaline protease stabilizing agent formula through orthogonal experiments as following: 5 mmolL^(-1) Ca(superscript 2+), 15mgmL^(-1) trimethylene glycol-single methyl ether, 0.015% 4-formyl phenyl-boron dihydroxide, 1% glycerine.

在此基础上,进行L13(3^7)正交实验,以相对酶活率为指标,考察了不同酶活性保护剂在不同条件下对液体碱性蛋白酶活力的影响,筛选到一种优质高效的碱性蛋白酶稳定剂配方为:5mmolL^(-1) Ca(上标 2+),15mgmL^(-1)丙二醇-单甲醚,0.015% 4-甲酰苯基硼酸,1%甘油。

Objective: To observe the effect of septoplasty and partial turbinectomy on the peak flow of nose, and to evaluate the value of the peak flow of nose in the diagnosis of the nasal chronic diseases.

目的:观察鼻中隔矫正术和下鼻甲部分切除术对峰值鼻呼吸流量的影响,以确定峰值鼻呼吸流量在慢性鼻病中的诊断价值。

The vasomotion was induced by noradrenaline in vivo, then the changes of vasomotion after injecting SI and Na-monomethyl-L-arginine (L-NMMA, a NO synthase inhibitor) were measured respectively on a TV monitor using a TV camera mounted on the microscope, and the influence of L-NMMA on effect of SI was also observed.

在活体情况下运用去甲肾上腺素(noradrenaline,NA)血管运动诱导法诱导出血管运动,分别观察静脉注射N^G-单甲基-L-精氨酸(NG_monomethyl.L-arginine,L-NMMA)、SI后血管运动的变化及应用一氧化氮合酶抑制剂L-NMMA对SI作用的影响,摄录结果于监视器上用暂停功能测量。

Yet lately the attitude of the German superstars at the club has been less than reciprocal. When Bayern lost 3-2 at Wolfsburg in the Bundersliga last September, Oliver Kahn took time out from making some costly goalkeeping errors to lambast Hargreaves.

然而近来,俱乐部德国超级球星们的态度开始产生了变化,去年9月当拜仁在德甲联赛客场3:2输给沃尔夫斯堡时后,奥利弗卡恩抛下自己所犯的重大失误,将矛头指向乖小孩哈格里夫斯。

Currently, a great deal of Santa Claus want be a foucs group for immunization, it not only for next mothly those child with run at the nose will set on his leg, but also they all have a big bellt.

目前,美国很多圣诞老人都想优先接种甲流疫苗,这不只是因为下个月那些流着鼻涕的小孩会坐在他们腿上,这还与他们圆鼓鼓的肚子有关。

The optimal operation condition of Friedel-Crafts acylation for product Ⅰ was determined by orthogonal experiment: 0.02mol N-ethyl- carbazol, n Benzoyl chloride/n N-ethyl- carbazol=1.2, n AlCl3/n N-ethyl- carbazol=1.2 , at 25 oC for 3.5h. The yield was 94.6%.

通过正交设计实验,探讨了产物Ⅰ的Friedel-Crafts 酰化的最佳反应条件:N-乙基咔唑为0.02mol时,反应物苯甲酰氯与N-乙基咔唑摩尔配比为1.2。,催化剂AlCl3与N-乙基咔唑摩尔配比为1.2, 25℃下反应3.5h,产率可达94.6%。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。