甲下的

The acetalization and ketalization of various aldehydes and ketones with glycerol by using KHSO4 as catalyst were studied. Effect of reaction time, mole ratio of reactants and amount of catalyst on yield of acetals were investigated.

研究了在KHSO4催化下，丙三醇与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正辛醛、二苯甲酮、苯甲醛等十余种醛的缩合反应。

The acetalization and ketalization of various aldehydes and ketones with glycols using FeCl3 as catalyst were studied. The effects of reaction time, mole ratio of reactants and amount of catalyst on the yield of acetals were investigated.

研究了在FeCl3催化下，乙二醇与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正辛醛、二苯甲酮、苯甲醛等十余种醛的缩合反应。

Conclution: Diester aconitum alkaloid can be changed to monoester aconitum and aconine alkaloids. Under the controled condition benzoylaconine is a major hydrolysis products.

双酯型的乌头碱可水解转化为单酯型乌头碱和乌头原碱；在控制条件下，苯甲酰乌头原碱为主要水解产物。

Amination reaction was carried out at temperature of 90℃ to 150℃ for 2h to 10h and then ashless dispersant of polyisobutylene succinimide would be obtained after dehydration with the operations of vacuum distillation and filtration.

结果发现，实验在N_2保护下进行，BPO／PIB质量比为0.035，MA／PIB摩尔比为1.3，反应温度为150℃，反应时间为12h，搅拌速率为250rpm，引发剂过氧化苯甲酰以丁酮为溶剂分六次，时间间隔为30分钟，均量地加入反应器时，烃化反应物聚异丁烯的转化率最高。

Under this reaction condition, the yield of N-Phenyl benzamide was enhanced to 81.5%.

在此反应条件下，苯甲酰苯胺的收率达到了81.5%。

The 6- cyano-1, 1 (1, 3- dioxypropylidene)-7-(carbomethoxyl group- methyl - 5- oxo-Delt6 (8)- tetrahydrochysene indolizine and haloethane reacts with each other for ethylization with existence of alkali and organic solution with or without phase transversion catalyst, and produces mentioned product.

本发明在相转移催化剂或无相转移催化剂存在下，6-氰基-1，1-(1，3-亚丙二氧基)-7-(甲氧羰基-甲基-5-氧代-Δ6(8)-四氢中氮茚类化合物与卤代乙烷在碱和有机溶剂的存在下进行乙基化反应即得6-氰基-1，1-(1，3-亚丙二氧基)-7-1′-(烷氧羰基-丙基-5-氧代-Δ6(8)-四氢中氮茚类化合物。

The degree of eosinophil infiltration was determined by Chromotrope 2R histochemical method in the corresponding tissue. The number of EOS of blood was counted in each group. Result: There were more significant differences between either two groups about the level of tissue-bound IgE and the degree of eosinophil infiltration.

结果：(1)鼻息肉病、鼻息肉、正常下鼻甲黏膜三组组织中IgE的表达水平不同，两两比较差别均有统计学意义(P.01)；且其水平分别与鼻息肉及鼻息肉病组织中EOS浸润数呈正相关(P.01)。

A series of complex EuTb(subscript 1-x)3Dipy were synthesized in anhydrous alcohol with dibenzoyl methane and 2, 2-dipyridyl.

合成了稀土（Eu(上标 3+)和Tb(上标 3+)）与二苯甲酰甲烷、2，2'-联吡啶的一系列稀土配合物EuTb(下标 1-x)3Dipy。

The copolycondensation type polyamic acid was synthesized by using 3,3', 4,4'-Benzophenonetetracarboxylic dianhydride as the dianhydride monomer, 4,4'-Diamino diphenylmethane and 4,4'-Oxydianiline as the diamine monomer under microwave irradiation in Dimethylformamide.

在微波辐射条件下，采用3，3'，4，4'-二苯酮四羧酸二酐、4，4'-二氨基二苯甲烷和4，4'-二氨基二苯醚为单体，N，N'-二甲基甲酰胺为溶剂，低温合成一种共缩聚聚酰亚胺的前驱体聚酰胺酸，化学亚胺化脱水环化生成BTDA型共缩聚聚酰亚胺。

The research aimed to establish a FIPIX method for the determination of fipronil and acephate in 36% emulsifiable concentrate.

［目的］建立在同一液相色谱条件下测定混刹中氟虫腈和乙酰甲胺磷含量的方法。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。