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In this paper, 2,2-dimethylolbutyraldehyde was synthesized through the acetal reaction of formaldehyde and butyraldehyde, using silicotungstic acid as catalyst.

通过实验研究了硅钨酸对此羟醛缩合反应的催化效果,研究探讨了硅钨酸对此缩醛反应的催化反应活性,以及催化剂的的用量,反应物配比,反应时间等因素对反应产品收率的影响,确定了最佳催化条件。

The effects of mole ratio of reactants,reaction time and catalyst dosage on the yield of n-octylaldehyde 1,2-propylene glycol acetal were examined.

考察了醛醇摩尔比、反应时间、催化剂用量及其重复使用等因素对反应的影响,优化了反应条件。

The effects of reaction time and acetic anhydride/anhydroglucose unit molar ratio on the DS of starch acetates were investigated.

考察了反应时间和酰化试剂用量对酰化程度的影响。

The synthesis of methyl benzoate was carried out from acetophenone and dimethyl carbonate in the presence of solid acid and base catalysts.

以固体酸碱为催化剂,研究了碳酸二甲酯与苯乙酮合成苯甲酸甲酯的反应,考察了反应温度、反应时间、催化剂用量和原料摩尔配比等因素对反应结果的影响。

Therefore,a lower temperature(50℃)and a higher catalyst dosage were adopted in acetylation of high-grade bamboo pulp.

因而我们选择了乙酰化反应采用较低的温度(50℃)相对较高的催化剂用量3%。

In this paper, acetylsalicylic acid, cyclohexanone Preparation of micro-content of the experimental design, in different reaction conditions were carried out under analysis to optimize the improvements and chemical experiments on the basis of conventional experimental and micro-experimental comparison, being The experimental results consistent with the premise, fully reflects the micro-chemistry experiments to save time, save the amount of reagents, as well as many advantages such as reducing environmental pollution.

本文阐述了乙酰水杨酸、环己酮微型化制备实验的设计内容,在不同反应条件下进行了对照分析,从而进行优化改进,并就基础化学实验中常规实验与微型实验进行比较,在得到一致的实验结果的前提下,充分体现了微型化学实验节省时间、节省试剂用量、以及减少环境污染等诸多优点。

Decided relatively the craft condition of beautiful: IA occupies total monomer rub Er mark is 22%, 6.67% what cross ammonium sulphate dosage to be total monomer quality, reaction temperature ℃ of 80 ℃~85, acrylic acid and the drop that cross ammonium sulphate add time to be 2.5 H, heat preservation time is 3.5 H, total reaction time is 6 H.

确定了较佳的工艺条件:IA占总单体的摩尔分数为22%,过硫酸铵用量为总单体质量的6.67%,反应温度80℃~85℃,丙烯酸和过硫酸铵的滴加时间为2.5 h,保温时间为3.5 h,总反应时间为6 h。

The effect of ratio of hydroxyl acid, amount of catalyst and reaction time to the yield of sioamyl propionate were investigated.

探讨了醇酸物质的量比、催化剂用量、反应时间对丙酸异戊酯产品收率的影响。

The result of experiment indicates that the inversion ratio of acid is 89%, product accords with standard of our country, also catalyst can be used repeatedly, which doesn't pollute environment.

结果表明,催化剂用量为醋酸的40%,酸醇摩尔比为1:1.1,反应时间为1.5h,酸的转化率达89%,产品符合国家标准要求,并且催化剂可重复使用,对环境无污染。

The influences of reactiontemperature, leaching time, dosage of nitric acid and the ratio of solid to liquid wereinvestigated.

在银的浸出实验中,通过单因素条件研究了反应温度、时间、硝酸用量和固液比对浸出率的影响,确定了浸出银的最佳工艺。

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