用合成法合成

Cyclopentenopyridine(3) in yield of 65% was synthesized from acrolein ,cyclopentanone and NH3 by heterogeneous catalysis reaction through a fixed bed reactor.

以丙烯醛和环戊酮为原料，用固定床多相催化法合成了2，3-环戊烯并吡啶，收率65%，含量高于50%。

A molecularly imprinted solid phase extractant, particularly for the recognition of diphenylguanidine was prepared using diphenylguanidine as the template and bulk polymerization.

以二苯胍为模板分子，用本体聚合法合成了对二苯胍具有良好识别能力的分子印迹固相萃取剂。

A series of Zn Al hydrotalcite like compounds was synthesized by co precipitation method.

用非均相共沉淀法合成了系列Zn Al类水滑石样品，研究发现Al/摩尔比在 0 3 1～ 0 5 2范围内可得到纯类水滑石相。

Hybrid mesoporous molecular sieve materials with hexagonal mesoporous structure and covalent bonded polyoxometalates were synthesized based on tetraethoxysilane anti lacunary polyoxometalate, SiW11, via sol-gel method in the presence of triblock copolymers P123 as the structure-directing agent. The influences of molar ratio of inorganic precursors and aging temperature on the structure and the loadings of SiW11 in the hybrid materials were investigated. Some reaction details in the synthesis were revealed.

用嵌段共聚物P123为模板剂，正硅酸乙酯和缺位结构的多金属氧酸盐SiW11为无机前驱体，由溶胶－凝胶法合成了具有六方结构和SiW11共价键联的介孔分子筛杂化材料SiW11/SBA-15，着重考察了无机前驱的配比和老化温度对杂化材料结构及SiW11负载量的影响。

Results In Vero cell system,under lucifugal and illumination conditions,fullerene C60 has direct virucidal activity and infection block effect,but it does not has any multiplication inhibition action to HSV-1F strain.

以逆相蒸馏法合成了富勒烯脂质体，用药物对病毒所致细胞病变的抑制实验以及病毒的空斑减数实验，观察C60脂质体对HSV-1F株的直接杀灭、感染阻断及增殖抑制作用。

Whenthey reacted with organolithium reagents,α-trifluoromethylketimines can be prepared.

用N-三氟乙酰基氨基膦盐和锂试剂作用后，〓锅法合成了α—三氟甲基酮亚胺。

Deoxybenzoin(3) was prepareded by using the resorcinol and substituted phenylacetic as starting meterials in microwave-mediated.Then the compound(3) was reacted with acetic anhydride to produce(4).The compound(4) was hydrolyzed to convert compound(5) in the acid-mediated. The compound(5) was reacted with the 1,2-dibromo-ethane and 1,3-dibromo-propane in refluxed condition with acetone as solvent to give(6) or(7),respectively.Lastly,the title compounds were synthesized by refluxing(6) or(7) with 2-methyl-benzimidazole and potassium carbonate in acetone solution.

以取代苯乙酸和间苯二酚为起始原料，用微波辐射法合成脱氧安息香(3)，(3)与乙酸酐缩合生成2-甲基-7-乙酰氧基异黄酮(4)，(4)在酸性条件下水解生成相应的异黄酮(5)，化合物(5)分别与1，2-二溴乙烷和1，3-二溴丙烷反应生成(6)和(7)，化合物(6)和(7)再分别与2-甲基苯并咪唑偶合生成目标化合物。

In this dissertation , Physical and chemical properties of raw material was studied first, then sodium model-modification of it was researched. Next, preparation of FILM in traditional process using montmorillonite after model-modification was in research. After that, we studied the preparation of PILM in hydrothermal process using montmorillonite without being model-modified. Finally, products in experiments were characterized and Analyzed by XRD, IR, DTA.

根据目前国内外的发展现状，针对存在的问题，本课题做了以下几个方面的研究：首先对采用的基质材料的物化性进行了研究；然后研究了其钠化改型的工艺方法；接下来研究钠化后的蒙脱石用常规工艺合成PILM；在此基础上提出并研究了水热法制备PILM和其柱化剂的新工艺；最后对制备的试样通过XRD、IR、DTA等进行了分析和表征。

Calcium humic acid resin is synthesized by one step gel method. With the column filled with the resin made,the column poiser kept at pH 5～6, and with 0.01 mol/L HCl as an eluent, Ca 2+, Mg 2+ can be separated quantitatively.

利用一步凝胶法合成了钙型腐植酸树脂，用自制树脂装柱，控制柱平衡液的pH为5～6并以0.01mol／LHCl为洗脱液，使Ca2＋、Mg2＋离子与其它12种离子定量分离。

The high-purity propionyl chloride was synthesized using propanoic acid and triphosgene as raw materials.

以丙酸和三光气为原料，用三光气法合成了纯度较高的丙酰氯。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失