用合成法合成

METHODS The structures of compound I, extracted from Clausena lansium Skeels, and synthesized compound III were determined by single crystal X-ray diffraction analysis. The stereo-structures of compound II and IV were also built up through Tripos force field based on crystal structures of compound I and III. RESULTS The molecular formula and molecular weight were found to be C18H17O2N and 279.34 respectively.

方法用单晶X-射线衍射分析法测定了从植物黄皮提取物中分离得到的化合物I和采用合成方法得到的化合物III的晶体结构，并用分子力学计算方法分别模建化合物II和IV的立体结构。

Aortas were harvested for assessment of vasomotor function by isometric force recordings.

血管内皮一氧化氮合成脢及p47phox 的蛋白质表现则用西方墨点法记录。

Next , Blue organic light-emitting material Liq is synthesized, purified with chemical and physical methods. The pureness of Liq is inspected with liquid chromatogram and element analytical methods. Then the structure token of Liq is carried out by X-ray diffraction, IR spectra, UV absorption spectra, cyclic voltammeter and fluorescence spectra, fluorescence spectrum.

结合实验条件，合成了蓝色有机发光材料Liq，对其进行了化学和物理提纯，用液相色谱及元素分析法进行了纯度检测，并用X-射线衍射、红外吸收光谱、紫外—可见吸收光谱、循环伏安曲线、及荧光光谱等测试手段对Liq进行了结构表征。

The structure of the directingagent by method of Xray diffraction was examined.

用X－射线衍射法对用于NaA合成的导向剂结构进行了研究。

The super microporous tin-doped zirconium oxides were successfully synthesized by sol-gel method using zirconyl chloride as Zr source, tin chloride as Sn source and cetyltrimethylammonium bromide as template under hydrothermal or refluxing conditions.

以二氯氧锆和四氯化锡为金属源，十六烷基三甲基溴化铵为模板剂，用溶胶-凝胶法在水热或回流条件下成功合成出了锡掺杂的超微孔二氧化锆材料。

Objective To determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of Edaravone, by gas chromatography.

摘要］ 目的：用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量。

Part 7 is the conclusion of this paper.The main research in this paper includes:1 The 22 mixed ligand complexes were synthesized in which bipyridine-, phenanthroline 5-nitrophenanthroline , phenanthroline- 5,6-dikentone and biquinoline are the first ligand and chlorine ion phenylalanine, tyosine asparagic radical 2.6-diaminocaproic radical tryptophan , histidine malonate(mal2-) benzyl malonate (bmal2-) phenethtyl malonate (pmal2-) are the second ligand.

本文具体研究内容包括四部分：一、合成了以联吡啶、邻菲啰啉、5—硝基邻菲啰啉、邻菲啰啉-5，6-二酮、联喹啉为第一配体，以Cl~-、苯丙氨酸根、酪氨酸根、天冬氨酸根asp~(2-、赖氨酸根、色氨酸根、组氨酸根、丙二酸根mal~(2-、苄基丙二酸根bmal~(2-和苯乙基丙二酸根pmal~(2-为第二配体的共22个混配配合物，制备了其中6个混配配合物和1个单配体配合物单晶，用X-射线单晶衍射法测定了晶体结构。

The known titanoheterocyclic compound〓 was synthesized in high yield by a new route involving an oxidative addition reaction of "titanocene"with benzil, and its structure was first confirmed by a single crystal X-ray diffraction method.

首次由&二茂钛&与二苯乙二酮的氧化加成反应，高产率地合成了一个已知的高价钛杂环化合物〓，并首次用X-射线衍射法测得该化合物的单晶分子结构。

In this thesis, a reductive amination was used to prepare compound 16 with the boronic acid moiety. The moiety can provide covalent interaction with sugars.

本论文中，合成化合物16，是将化合物15与2-甲醯苯硼酸用还原胺化法而得到；其含有硼酸部分，可以与醣类分子以共价键键结。

The dissertation is focused on the research of organic supramolecular self-assembly and molecule folding. It consists of four parts. In the first part, three new model molecules for investigating intramolecular coaggregation behavior have been designed and synthesized. Fluorescence studies reveal that intramolecular coaggregation of these molecules take place with the increase of the solvent polarity because of hydrophobic-lipophilic interaction .

本论文主要对有机超分子自组装和分子折叠做了一些研究，共分四个部分：第一部分中，我们设计并合成了一个新的研究分子内自簇集的模型，用荧光光谱法对该模型进行了研究，研究表明，在促簇能力较强的溶剂体系中，这一类模型分子可在疏水亲脂作用的驱动下发生分子内自簇集而形成卷曲的构象。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失