用合成法合成

Since the production of carbon nanotubes synthesized by arc-discharge method contains impurities such as carbon nano-particles, amorphism carbon and graphite fragment, several purification methods were used to purify carbon nanotubes. It is found that with oxidation method in air, we can easily get purified carbon nanotubes.

由于用电弧放电法合成出来的纳米碳管产物中除了有纳米碳管外，还含有一些纳米石墨颗粒、无定形碳和石墨碎片等，因此本文对用电弧放电法合成出的纳米碳管进行了多种方法、探索性的提纯研究，实验结果发现，利用大气氧化法对纳米碳管进行提纯效果好，设备简单，是一种方便实用的方法。

In this paper different concentrations of iron boride powders were put into the iron - based metal catalyst to get different kinds of boron-doped diamonds with high thermal stability under high temperature and high pressure conditions.

本文在铁基触媒的基础上加入不同含量的硼铁粉，用静压法合成了含硼金刚石。

A series of novel dendrons with 1,3,5-triazine structure were synthesized by convergent strategy using cyanuric chloride, p-hydroxyazobenzene,β-naphthol, 1-hydroxyanthraquinone, 3,5-dihydroxybenzyl. They were the first generation p-phenyl-azo-phenyloxy-terminated dendron G1.0, the first generation naphthyloxy-terminated dendron G1.0, the first generation naphthyloxy-terminated and 1-anthraquinonoxy-cored dendron G, and the second generation naphthyloxy-terminated dendron G2.0.

以对羟基偶氮苯、β-萘酚为端基，三聚氯氰、3，5-二羟基苄醇为支化单体，1-羟基蒽醌为核心，用收敛法合成了一系列新型结构的含均三嗪环的树枝块：第一代端基为偶氮苯的树枝块G1.0、端基为萘氧基的树枝块G1.0、端基为萘氧基、中心为蒽醌的树枝块G、第二代端基为萘氧基的树枝块G2.0。

Domestic enterprises still adopt direct synthetic method to produce methyl chloride silane. In recent years, great progress has been made.

我国有机硅单体的研究开发起步较晚，多数企业仍延用直接法合成甲基氯硅烷，以及小型流化床反应装置。

In solid phase process, the polyiodides, which include triiodide, pentaiodide, heptaiodide, nonaiodide and undecaiodide tetra-n-butyl ammonium iodide, tetrabutyl ammonium bromide and tetramethyl ammonium iodide poly-compounds, were synthesized by the low-heat solid phase reaction between iodine and tetra-n-butyl ammonium iodide, tetrabutyl ammonium bromide or tetramethyl ammonium iodide; In complexation process, solution polyiodides were synthesized by complexing action of different agents; In resinifying process, triiodide, pentaiodide, heptaiodide resinic polyiodides were synthesized by ion-exchange when the strong basicity styrene anion exchange resin, potassium iodide and iodine were used as raw materials.

固相法是用正四丁基碘化铵、四丁基溴化铵或四甲基碘化铵分别与碘作用，通过低热固相反应，合成出碘三、碘五、碘七、碘九和碘十一形式的正四丁基碘化铵、四丁基溴化铵或四甲基碘化铵的系列高聚碘化合物；在络合法合成溶液高聚碘的实验中，选用几种络合剂通过络合作用首次合成了溶液高聚碘；树脂法合成高聚碘的实验是采用强碱性苯乙烯系阴离子交换树脂、碘化钾和碘为原料，通过离子交换，合成了碘三、碘五和碘七形式的树脂高聚碘。

The paper introduced three processes to prepare isochroman from β-phenethyl alcohol and polyformaldehyde:HCl catalysis,AlCl_3 catalysis and toluene-p-sulfonic acid catalysis,and discussed its reaction mechanism,using toluene-p-sulfonic acid catalysis method to prepare isochroman ,the yield is 46%,purity is 96%.

用β-苯乙醇和多聚甲醛为原料，进行了HC l催化法，三氯化铝催化法和对甲苯磺酸催化法的合成路线的实验，并对其反应机理进行了探讨，应用对甲苯磺酸催化法合成异色满的合成路线，得率46%，纯度96%。

In this article,the tripeptide RGD is synthesized by the method of liquid synthesis .

采用液相合成法合成了RGD 三肽并对其进行了生物活性检测，证实用液相合成的 RGD 短肽具有促进材料与内皮细胞粘附的生物活性。

Respectively, glutamic acid derivatized β-CD has been synthesized with epoxy chloropropane as the intermediate, a water-insoluble yellow liquid was got after the acetylating of the by using acetic anhydride, which was used as a novel gas chromatographic CSP; A water-soluble β-CD polymer cross-linked with epoxy chloropropane has been synthesized, and the derivatives of β-CD polymer were synthesized by its alkylating and acetylating. The different β-CD derivatives were coated on silica capillary columns by dynamic method, the chromatographic properties and retention behaviors of the fused silica capillary columns were studied, the results showed that the β-CD derivatives had good stereoselectivity and separation results to some compounds, especially to various positional isomers and enantiomers.

本文还分别以环氧氯丙烷为中间体，合成了七{2，6-二-O-[3-(1，3-二羟基丙氨酸)]}-β-环糊精，再用醋酸酐将其乙酰化，得到了一种淡黄色粘稠液体，合成了一种新型的环糊精衍生物；以环氧氯丙烷作交联剂合成了一种水溶性的β-环糊精聚合物，再将其烷基化和酰基化，合成了β-环糊精聚合物的不同衍生物，用动态法将不同类型的β-环糊精衍生物涂渍在石英毛细管柱上，通过对所制备柱柱性能的测试和对一系列化合物的分离和保留行为的研究，结果表明所合成的β-环糊精衍生物对各类化合物，特别是对位置异构体和对映异构体具有较好的分离效果，显示了很强的立体选择性。

And the morphologies of lead tungstate crystal were different when different surfactants of polygycol 200 and cetyltrimethyl ammonium bromide were added in the experiments.

以钨酸钠和醋酸铅为原料，分别加以表面活性剂聚乙二醇200和十六烷基三甲苯溴化铵，用沉淀法合成出钨酸铅纳米晶和菱形微晶。

Lithium manganese oxide doped by lithium and nickel was prepared by liquid method.

用液相合成法合成出掺锂、镍的锂锰氧化物。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失