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Effect of adding rosin into raw lacquer on the film properties was studied.

研究了松香改性对生漆漆膜性能的影响。

Urushiol 40-80%, gum and nitrogen 6-14%, water 14-40%.

一般生漆中约含有漆酚40~80%,树胶质和含氮物6~14%,水分14~40%。

Urushiol compositions of Chinese lacquer samples from 60 single trees were determined by GC. Film properties including surface drying time, luster value, shock strength, adhesion and flexibility were tested according to standard methods for coating.

本文作者用气相色谱法测定了约60个单株生漆样品的漆酚组成;同时用涂料标准方法测定了这些样品的漆膜的表干时间、光泽值、冲击强度、附着力、柔韧性等。

The structures and configurations of other components weredetermined too.The results show that the structure of components ofChinese lacquer urushiol are the same as components of Japaneselacquer. In this work,2D-heteronuclear relayed coherence transferspectroscopy plays an important role in determining molecularskeleton carbon linkage.

研究结果表明,中国生漆漆酚中含量最大并起关键作用的两双键共轭的三烯漆酚的结构与构型与日本漆中的该组分完全相同,即都有末端甲基的3—十五碳烯烃(8′Z,11′E,13′Z)邻苯二酚,而没有末端双键的存在,其它几个漆酚主要组分的结构也与日本漆酚对应组分基本相同。

In China,natural lacquer has been studied for a long time.Because to separate natural homologous is very difficult,it is almostimpossible to obtain a great deal of pure sample.So the structure ofmain constitute of Chinese lacquer urushiol has not an identicalresult due to the incomplete structural data. The urushiol diacetate derived from urushiol have beensuccessfully separated using centrifugal rotational TLC withpreparative silica get thin layer coated silver nitrate.

天然漆的研究,在我国有较长的历史,漆酚组分及结构做过一些工作,但由于天然同系物之间分离的困难,不易大量得到纯的样品,只能通过零星结构数据推断结构,致使中国生漆漆酚主要组分的结构没有一致的认识与确切的结论。

The acetated and hydrogenated urushiol dimer has been separated,and studied by hetero-J resolved 2D-NMR,homo- and heteronuclearchemical shift correlation 2D-NMR and long-range coupled chemicalshift correlation 2D-NMR.The results show that the urushiol dimerare most diphenyl and alkyl phenyl ether structures.Furthermore,IR and MS data also has conformed this structures.

本文将酶催化预聚后的生漆,催化加氢后,乙酰酯化,再进行离心旋转薄层层析,分离得到二聚体主要组分,用异核J分辨谱,同核化学位移相关,异核化学位移相关,远程偶合异核化学位移相关等2D—NMR技术,全面研究了其结构,得到了联苯型和烷基芳醚型聚合结构的结论。

Wooding F B P%Northcote D H The fine structure of the mature resin canals in Pinus pinca 10.1016/S0022-5320(65)80072-7 J Ultrastructure Research , 1963,null

赵桂仿%胡正海漆树乳汁道分泌细胞的超微结构及其与生漆产生关系的研究植物学报, 1990,1

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