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琥珀酰

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Self-assembled nanomicelles of N -cholesterol succinyl O -carboxymethyl chitosan were prepared by probe sonication method. The amphiphilic property and the critical micelle concentration of CCMC were determined by fluorescence probe technique; the morphology and the size of CCMC self-assembled nanomicelles were analyzed by transmission electron microscopy and the dynamic laser light scattering.

以 N -胆甾醇琥珀酰基- O -羧甲基壳聚糖(CCMC,胆甾醇基取代度6.9%)为原料,在水溶液中通过探头超声处理制备其自组装凝胶纳米胶束,采用稳态荧光探针法考察临界胶束浓度,并通过透射电镜和动态激光散射仪检测胶束的形态大小。

A method for separation and determination of amino acids using pre column derivatization with 6 aminoquinoline N hydroxysuccinimido carbamate AccQ.

对Waters公司采用 6 氨基喹啉 N 羟基琥珀酰亚胺基氨基甲酸酯柱前衍生化测定氨基酸的方法进行了改进。

MethodAmoxicillin were coupled with bovine serumalbuminand oval buminby using N-hydroxysuccini mide actived ester method to prepare the i mmune antigen AMX-BSA and detection antigen AMX-OVA.The adult rabbits were immunized with AMX-BSAto obtainthe polyclonal antibody with high titer.

方法采用N-羟基琥珀酰亚胺活性酯法将阿莫西林分别与牛血清白蛋白、卵清蛋白偶联,制备免疫抗原AMX-BSA和检测抗原AMX-OVA,用AMX-BSA免疫成年兔以获得高效价的多克隆抗体。

Based on the principle of Hunter reagant,N-Hydroxysuccinimide functional group was introduced into polymer carrier to synthesize a couple of olefine acids" and styrene" copolymer-NHS-esters.

利用Hunter试剂的原理,将N-羟基琥珀酰亚胺酯功能基团引入高分子载体上,合成了几种烯酸与苯乙烯聚合物的NHS酯。

Cold crystallization process of N-(1-naphthyl) succinimide below glass transition temperature was monitored by differential scanning calorimetry and X-ray diffraction.

采用x射线粉末衍射和差示扫描量热分析方法,跟踪研究了N-(1-萘基)琥珀酰亚胺的液氮淬冷样品在室温(25℃)即在玻璃化转变温度以下的冷结晶行为。

In order to improve the stability and mechanical properties in moist state,the gelatin nanofibrous membranes were chemically crosslinked by 1-ethyl-3-dimethyl-aminopropyl carbo-diimide hydrochloride and N-hydroxyl succinimide.

采用1-乙基-(3-二甲基氨基丙基)碳二亚胺和N-羟基琥珀酰亚胺对明胶纳米纤维膜材料进行化学交联处理,改善了材料的耐水性、热稳定性和力学抗拉性能。

The antibody was chemically conjugated onto the microspheres through the reaction between primary amino groups and the succinimide ester groups due to their high reactivity.

琥珀酰亚胺酯基由于其与生物分子上的伯氨基具有高反应活性,条件温和,反应速度快,是一种很好的固定生物分子的功能基。

The 3,4-disubstituted succinimide substructure-containing natural products andindolizidine alkaloids, tropane alkaloids are widespread in nature. Most of themexhibit important bioactivities.

含有3,4-二取代琥珀酰亚胺结构的天然产物以及吲哚里西啶生物碱、托品烷类生物碱广泛分布于自然界中,它们大多具有重要的生物活性。

The determination of amino acids in blood clam antianaemia oral liquid using HPLC-AccQ-Tag method is reported. The oral liquid reacted with 6-aminoquinolyl-N-hydroxysuccini-mdyl carbamate. Then, the corresponding derivatives were analyzed with an HPLC. The chromatographic conditions were AccQ-TagTM C18 column for amino acids analysis (3.9mm×15cm); mobile phase of program elution sodium acetate solution(pH5.02), acetonitrile, Milli-Q water. The amino acids'AQC deriatives were detected at 248nm with a UV-detector. Eighteen kinds of amino acids were completely determined in 35 minutes.

以6-氨基喹啉-N-羟基琥珀酰亚胺基氨基甲酸酯为衍生剂,与毛蚶抗贫血口服液中的氨基酸柱前定量衍生,用WatersHPLC仪,AccQ-TagTM专用C18柱(3.9mm×15cm),以140mmol·L-1的醋酸钠溶液(pH5.02)为溶剂A,乙腈为溶剂B,超纯水为溶剂C,进行梯度洗脱,检测波长为248nm,35min测试完毕。

Methods The amino acids in the injections were pretreated with 6-aminoquinolyl-N-hydroxysuccinimdyl separately and their derivatives were analyzed on Waters 2695 HPLC using AccQ-Tag column. Gradient eluents consisted of sodium acetate solution (pH 4.95), acetonitrile and water. The Detection wavelength was 248 nm and column temperature 37℃.

采用AccQ-Tag法,以6-氨基喹啉-N-羟基琥珀酰亚胺基甲酸酯为衍生试剂,与复方氨基酸注射液(18AA-V)中17种氨基酸柱前衍生,用Waters 2695 HPLC仪器,AccQ-Tag柱,以醋酸钠(pH 4.95)缓冲液为流动相A,乙腈为流动相B,水为流动相C进行梯度洗脱,检测波长为248 nm,柱温为37℃,进样量为5μL。

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