玻璃化

A novel trifunctional fluorinated epoxy compound was synthesized, which was cured with one alicyclic anhydride and two aromatic diamines, respectively.

固化后的含氟三官能团环氧树脂表现出高玻璃化转变温度、低介电常数、低热膨胀系数、低吸水率等特点。

Department of Scientific History and Archaeometry; Graduate University of Chinese Academy of Sciences; Beijing 100049;4.Institute of Archaeology; Chinese Academy of Social Sciences; Beijing 100710; China;The fabrication technologies in terms of phase composition,structure,firing temperature,porosity,density and water permeability of ceramic water pipes and contrastive ceramic tilesexcavated from Anyang Yin Ruins of Shang dynasty were studied by X-ray fluorescence,X-ray diffraction and dilatometer,respectively.It was found that the contents of CaO,K2O,MgO and P2O5 in CWP were relatively higher than those in contrastive CT.The difference was further confirmed by the mass ratio of flux...

采用X射线荧光、X射线衍射、热膨胀等分析手段对比研究了安阳商代陶水管的制作工艺，发现陶水管化学成分中各类熔剂的质量分数均略高于对比陶片中熔剂的质量分数，CaO、K2O、MgO等助熔剂与A l2O3的质量比进一步证实该现象，而这种差异性则外在地表现为陶水管的气孔度低于对比陶片以及陶水管热膨胀曲线中出现玻璃化现象，该结果表明陶水管原料应为一种易熔粘土，或者在沉淀粘土中人为地掺和了草木灰类掺和料，这有利于陶水管烧制与成型，有助于熔剂在熔融状态下，较好地进入陶水管中的空隙，使陶水管变得更加致密，一定程度上有利于防止陶水管的渗水，显示出陶水管制作工艺的特殊性。

Methods: Human mature oocytes were cryopreserved using cryoleaf. Resuscitated oocytes were administered by intracytoplasmic sperm injection, embryo transplantation or cultured to blastulation, observing the fertilization and developmental capacity of oocytes.

运用cryoleaf进行人类成熟卵母细胞玻璃化冷冻保存，复苏后行胞浆内单精子注射-胚胎移植或培养至囊胚形成，观察复苏后卵母细胞受精及发育能力。

Methods: MII, GV and IVM-MII were vitrified. After thawed, they underwent in vitro maturation, in vitro fertilization, embryo cultivation or fixed for immunofluorescence. The rates of survival, maturation, fertilization, blastulation and cytoskeleton with normal configuration were calculated.

玻璃化冷冻生殖泡期卵、成熟中期卵及体外成熟卵，解冻复苏后，分别作体外成熟、体外受精、胚胎培养或固定作免疫荧光标记，统计复苏率、成熟率、受精率、囊胚率、细胞骨架正常率。

Methods: mⅱ,gv and ivm-mⅱ were vitrified. after thawed, they underwent in vitro maturation, in vitro fertilization,embryo cultivation or fixed for immunofluorescence. the rates of survival, maturation, fertilization, blastulation and cytoskeleton with normal configuration were calculated.

玻璃化冷冻生殖泡期卵、成熟中期卵及体外成熟卵ivm-mⅱ），解冻复苏后，分别作体外成熟、体外受精、胚胎培养或固定作免疫荧光标记，统计复苏率、成熟率、受精率、囊胚率、细胞骨架正常率。

Compared with homo-polymimdes and copolymimdes,PAIs can evidently improve mechanical properties while maintaining excellent solubility,high Tg and thermal stability of fluorenyl cardo polyimides.

与均聚PI，共聚PI相比，PAI在维持芴基Cardo型PI优异的溶解性，高的玻璃化转变温度及热稳定性的同时，明显改善力学性能。

Preparation and Application of water-borne curing agent from cashew nut shell liquid ;2. The dispersion was then modified with cashew nut shell liquid containing hydroxyl groups.

采用含有—OH的脱羧腰果壳液对其改性后，复合膜玻璃化温度上升、硬度提高，耐水性进一步改善。

In order to explore the relationship between structure and properties of hydroxyalkyl cellulose ether nitrate, molecular structures of nitrate ester of hydroxylethyl cellulose ether, nitrate ester of hydroxylpropyl cellulose and nitrate ester of cellulose glycerol ether with molar substitution of 1 were simulated by using Synthia module of Materials Studio, and their performances of nitrogen content, glass transition temperature and Young's modulus were predicted.

为探索羟烷基纤维素醚硝酸酯的结构与性能关系，借助Materials Studio软件中的Synthia模块模拟了摩尔取代度为1的羟乙基纤维素醚硝酸酯、羟丙基纤维素醚硝酸酯和二羟丙氧纤维素醚硝酸酯的结构，并预测了它们的含氮量、玻璃化转变温度和杨氏模量。

When the PEMA and PVC were in their glass transition region,the number of their characteristic absorption peaks increased.

结果表明，在玻璃化转变区域材料的吸声系数较高，PEMA和PVC均具有特征吸收频率。

In this paper, three kinds of hydroxyl component are prepared for two-component waterborne polyurethane paint, that is, acrylic dispersion, acrylic emulsion and silicone-modified acrylic emulsion. The influence of the composites of these dispersion and emulsions on polymerization process, viscosity, particle size and coagulum are investigated, infrared spectroscopy , inductance coupling plasma , transmission electron microscopy and thermogravimetric analysis are used to characterized their structure, composite, morphology and thermal stability, respectively.

本论文制备了三种用于水性双组分聚氨酯涂料的含羟基组分，即丙烯酸分散体、丙烯酸乳液和有机硅改性丙烯酸乳液，研究了这些分散体和乳液在制备过程中聚合物的羟值、酸值、玻璃化温度、乳化剂、反应温度等对聚合转化率、凝聚物含量、聚合物粘度和粒径的影响，用红外光谱、热重分析、透射电镜和感应偶合等离子技术表征了其结构、组成、形态和热稳定性。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。