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Our company supply raw materials and related intermediates as follows: Second dibutyryl cAMP calcium, voriconazole, terbinafine, vecuronium amines, cAMP, thiamphenicol, a chlorophenol hydrochloride esters, card network sodium phosphate tilmicosin, foscarnet, lornoxicam, Tilmicosin, Cephalosporium aspirin acid, ceftiofur hydrochloride, ceftiofur sodium, Ozagrel, ondansetron hydrochloride ketones, hydroxyurea, ticarcillin sodium, telmisartan, esmolol hydrochloride, hydrochloric acid Daguan Nikkomycin, adefovir dipivoxil, buflomedil hydrochloride, granisetron hydrochloride, warfarin sodium,-methyl gabexate acid, nicergoline, pantoprazole sodium,·, tegafur, cefepime hydrochloride, vecuronium bromide, hydrochloric acid meclofenoxate, sertraline hydrochloride, Cefonicid amine salt, aztreonam, ticarcillin, cefdinir, cefodizime sodium, sodium ferulate, colloidal pectin secretion, 2,3 - cyclopentene and pyridine, Piperacillin acid, cefetamet US-acid, hydrochloride Cefmenoxime ,3-TZ, 2 - deoxy-D-glucose, two-amidine urea benzene, sodium Cefonicid, Cefonicid intermediates, ester Cefamandole sodium, Cefalotin acid, intermediates cefpirome, cefepime sulphate, cefepime intermediate nucleus of cefepime, cefpirome nucleus, Cefamandole sodium, ceftriaxone new active ester, oxaliplatin, cyclophosphamide vary gland amines, polyene match him.

我公司供应的原料药及相关中间体为:二丁酰环磷腺苷钙、伏立康唑、盐酸特比萘芬、维库溴胺、环磷腺苷、甲砜霉素、盐酸甲氯酚酯、卡络磺钠、磷酸替米考星、膦甲酸钠、氯诺昔康、替米考星、头孢匹胺酸、头孢噻呋盐酸盐、头孢噻呋钠、奥扎格雷、盐酸恩丹西酮、羟基脲、替卡西林钠、替米沙坦、盐酸艾司洛尔、盐酸大观霉素、阿德福韦酯、盐酸丁咯地尔、盐酸格拉司琼、华法林钠、甲磺酸加贝酯、尼麦角林、泮托拉唑钠、普拉洛芬、替加氟、盐酸头孢吡肟、维库溴铵、盐酸甲氯芬酯、盐酸舍曲林、头孢尼西胺盐、氨曲南、替卡西林、头孢地尼、头孢地嗪钠、阿魏酸钠、胶体果胶泌、2,3-环戊烯并吡啶、哌拉西林酸、头孢他美酸、头孢甲肟盐酸盐、3-TZ、2-脱氧-D-葡萄糖、双脒苯脲、头孢尼西钠、头孢尼西中间体、头孢孟多酯钠、头孢噻吩酸、头孢匹罗中间体、头孢吡肟硫酸盐、头孢吡肟中间体、头孢吡肟母核、头孢匹罗母核、头孢孟多钠、头孢曲松新型活性酯、奥沙利铂、异环磷腺胺,多烯他赛。

The factors affect on the degree of substitution of product, yield and apparent viscosity, such as the mol rates of EPTAC with -NH2, reaction temperature, reaction time and the content of water in system have been discussed in detail. FTIR spectrometer and UV spectrometer are used to characterize the structure of the derivative and it is proved that substitution reaction mainly occurs on the -N element .The particle size and morphology of chitosan and quantemary ammonium salt of chitosan are analysised by comparing photos of their scanning electron microscope. The degree of substitution of HACC is determined by acid -base conductometric titration. An error in current formula of DS has pointed out and a correct formula has presented.On the base of experience of above experiment, the reaction conditions of HACC were systematically investigated through orthogonal design, and then the best conditions are found. Water-solubility and dependence of pH are studied.

壳聚糖和环氧丙基三甲基氯化铵在异相条件下发生反应,通过单因素实验,制备了一系列不同性能的壳聚糖季铵盐,本文首次详细讨论了反应条件(反应摩尔比、反应时间、反应温度、水含量)对产率及产物性能的影响;用红外光谱和核磁共振对结构进行表征分析时,发现季铵盐阳离子基以N位上取代为主;通过电镜图片对壳聚糖和季铵盐衍生物外观形貌进行对比,采用酸碱电导滴定法测定产物的取代度,并对常用取代度公式做了修正。

A bis-imdazoline corrosion inhibitor JUC was synthesized by reacting with divinyl three amine,and its quaternary ammonium JUCI was also synthesized for corrosion inhibition in acids.

以己二酸、二乙烯三胺为原料合成了双环咪唑啉缓蚀剂JUC,并对其季铵化后得到了适于酸化用的双环咪唑啉季铵盐缓蚀剂JUCI;采用静态挂片失重法对合成的缓蚀剂在酸化条件下的缓蚀性能及与非离子表面活性剂SA-1复配后的缓蚀性能进行了评价研究。

The reaction conditions of synthesizingcyclohexyl acetate catalyzed with ammonium ferric sulfate dodecahydrate NH4Fe(SO42.12H2Oare studied .The yield of cyclohexyl acetate can reach 87.2% under mole ratio of aceticacid,cyclohexyl alcohol and ammonium ferric sulfate is 1∶0.44∶0.02,cyclohexane as solvent ,refluxing and segregating water for 60min.

研究了NH4Fe(SO4)2.12H2O催化合成乙酸环己酯的反应条件,当乙酸、环己醇和硫酸铁铵的摩尔比为1∶0.44∶0.02,以环己烷为溶剂,回流分水60min,乙酸环己酯收率达87.2%,在相同反应条件下,合成了甲酸环己酯(收率为68.5%)、丙酸环己酯(收率为59.4%)和丁酸环己酯(收率为21.6%)。

Professional sales companies operating bromide products: sodium bromide, sodium bromide, potassium bromide, potassium bromate, Tetrabromobisphenol A, Deca-BDE, ten PBDEs, DBDPE, hexabromodiphenyl Central dodecane, dibromo neopentyl glycol, neopentyl bromide three alcohols, three bromine phenol, octabromodiphenyl ether, brominated polystyrene, bromide, calcium bromide, dibromo succinic acid, dibromo-D ene glycol, bromide surfactants series: Dodecyl trimethyl ammonium bromide, tetradecyl trimethyl ammonium bromide, cetyltrimethyl ammonium bromide, octadecyl trimethyl ammonium bromide dodecyl trimethyl ammonium chloride, tetradecyl trimethyl ammonium chloride, cetyl trimethyl ammonium chloride, octadecyl trimethyl ammonium chloride, tetrabutyl ammonium bromide wholesale sales: dimethylolpropionic acid, DL-malic acid, isophthalic acid PIA, glycolic acid, adipic acid.

公司专业经营销售溴化物系列产品:溴化钠、溴酸钠、溴化钾、溴酸钾、四溴双酚A、十溴二苯醚、十溴联苯醚、十溴二苯乙烷、六溴环十二烷、二溴新戊二醇、三溴新戊醇、三溴苯酚、八溴醚、溴化聚苯乙烯、溴化铵、溴化钙、二溴丁二酸、二溴丁烯二醇、溴化表面活性剂系列:十二烷基三甲基溴化铵、十四烷基三甲基溴化铵、十六烷基三甲基溴化铵、十八烷基三甲基溴化铵、十二烷基三甲基氯化铵、十四烷基三甲基氯化铵、十六烷基三甲基氯化铵、十八烷基三甲基氯化铵、四丁基溴化铵批发销售:二羟甲基丙酸、DL-苹果酸、间苯二甲酸 PIA、羟基乙酸、己二酸。

The enhancement of the reaction activity is attributed to the phasetransfer capability of the built-in quaternary ammonium and pyridinium salts of theMn catalyst.

分子内季铵盐和吡啶盐具有相转移能力,对于取代色烯不对称环氧化的作用与外加的吡啶盐和卤化铵的作用相似,使Mn催化剂催化取代色烯环氧化反应的活性明显提高。

The enhancement of the reaction activity is attributed to the phasetransfer capability of the built-in quaternary ammonium and pyridinium salts of theMn catalyst. The effect of the internal quaternary ammonium and/or pyridiniumsalt on the epoxidation of substituted chromenes is similar to that of the externalpyridinium salts and ammonium halides.

分子内季铵盐和吡啶盐具有相转移能力,对于取代色烯不对称环氧化的作用与外加的吡啶盐和卤化铵的作用相似,使Mn催化剂催化取代色烯环氧化反应的活性明显提高。

The selected process consists of several steps as follows. Firstly, ammonifying the oily mixture of PXA pyrolysis by ammonia or aqueous ammonia, then adding the organic solvent to extra

实验结果表明,合适的分离提纯工艺为:先将裂解产物用氨水氨化、有机溶剂萃取,然后用硫酸酸化11-CUA铵盐水溶液、再将粗品11-CUA于合适介质中结晶,得到高纯度11-CUA晶体;优化工艺条件为:氨化pH值8.0~10.0、温度25-35℃,甲苯为萃取剂,酸化pH值1.5~2.0、温度55-60℃,环己烷为结晶介质,粗品11-CUA在环己烷中溶解温度50~55℃、与环己烷初始质量比4:100、结晶前沉降分层时间10min、结晶温度20℃。

This thesis included three parts:(1)The study of the complexation and threaded structures based on the benzo-21-crown-7/secondary dialkylammonium salt recognition motif;(2)Secondary dialkylammonium salt can thread through the cavity of pyrido-21-crown-7 to form the threaded structures;(3)The study of the size of macrocycle rings which can complex with secondary dialkylammonium salts.

本论文主要开展了以下三方面內容的研究:(1)基于苯并21-冠-7(B21C7)的主体冠醚和二级铵盐客体化合物的络合以及互穿结构研究;(2)客体二级铵盐穿过吡啶-21-冠-7(P21C7)的空腔形成准轮烷及轮烷互穿结构的研究;(3)对关于络合二级铵盐的冠醚环的尺寸大小做了探讨。

The diagnostic vibrational modes of these complexes were predicted and assigned. Bond length, total atomic charge, frontier molecualr obital energy, molecular obital coefficience, and Mullicken Bonding Population demonstrated that electron transfer should have happened from benzene to ammonium, and therefor the charge-transfer complex should be formed.

通过复合物中的键长、原子净电荷、分子轨道能量和系数、Mullicken成键布居等量子化学参数的分析得出了铵和苯环碳原子发生作用而形成电荷转移复合物,铵和苯之间的作用包含s-π相互作用的结论。

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