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The reaction rates between VC/PMI and VC/N-cyclohexyl maleimide are compared, and the later is more rapid than the former.

并对VC/N-环己基马来酰亚胺和VC/PMI两个体系进行了比较。

In order to further understand combining characteristic of cyclohexyl methylphosphonofluoridate and isopropyl methylphosphonofluoridate and contribute more scientific data for its medical protection, the potency of inhibition of acetylcholinesterase activity induced by GF, GF+GB and the effects of reactivation by oximes pyramidoxime monohydrate(HI-6) and pyridine-2-aldoxime methylchloride(2-PAM-Cl) in rat brain were investigated with DTNB microanalysis in this study.

为进一步了解甲氟膦酸环己酯与甲氟膦酸异丙酯的联合特性,为制订医学防护措施提供更多的理论依据,用微量DTNB法对GF,GB和GF与GB混合对大鼠脑乙酰胆碱酯酶的抑制及肟类重活化剂酰胺磷定(HI-6)和氯磷定(2-PAM-Cl)的重活化作用进行了研究。

To establish a method for determination of cyclopentadiene,dimethylformamide and N-methylpyrrolidone simultaneously in isoprene by GC.

用毛细色谱法建立异戊二烯中各组分定性分析方法及环戊二烯,N-甲基吡咯烷酮,N,N-二甲基甲酰胺的测定方法。

The fluorinated polyamides could be dissolved in strong aprotic solvents and some low boiling point solvents, such as cyclopentanone, to form homogenously solution with solid content higher than 20%.

这一系列聚酰胺材料在极性溶剂或低沸点溶剂如环戊酮中都具有较好的溶解性,可以获得固含量高达20%以上的均相溶液,并在较的低温下固化成膜。

Methods The target compounds were synthesized from cyclopentanone via Stork reaction, Mannich reaction and selective reduction.

方法以环戊酮为起始原料,通过Stork烯胺反应、Mannich反应、选择性还原制备目标化合物;以二甲苯致小鼠耳肿胀模型测试目标化合物的抗炎活性。

When acetone oxime was used as substrates, lower conversion and selectivity were obtained. For cyclopentanone oxime as the substrate, the Beckmann fragmentation was observed.

对于丙酮肟和环戊酮肟,前者重排得到N-甲基乙酰胺的选择性低,后者则不发生Beckmann重排。

Synthesis of Antidote of N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane BI Hong-mei, ZHANG Jin-yan, LIANG Ying, SHEN Yong (College of Arts and Sciences Heilongjiang August First Reclamation University, Daqing 163319, Heilongjiang, China) Abstract: N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane was synthesized by one pot method with isopropanolamine, cyclopentanone and dichloroacetyl chloride. The optimum reaction conditions obtained are as follows:the proportion in moles of the above materials is 1∶1∶1.2, reaction solvent is toluene, reaction temperature is -15 to -10 ℃,reaction time is 3 h, under the optimum condition, the yield of the compound is 50.0%.

除草剂解毒剂N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷的合成毕洪梅,张金艳,梁英,沈勇(黑龙江八一农垦大学文理学院,黑龙江大庆 163319)摘要:以33%的氢氧化钠水溶液为缚酸剂,异丙醇胺、环戊酮和二氯乙酰氯为原料,采用&一锅法&合成了N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷,采用正交实验法得到最佳反应条件:反应原料摩尔比为1∶1∶1.2,苯作溶剂,反应的温度为-15 ℃~-10 ℃,搅拌时间为3 h,产率达到50.0%。

However, alkylating agents, such as cyclophosphamide, and the topoisomerase II inhibitors, doxorubicin and epirubicin, are associated with two types of cytogenetically distinct leukemias after adjuvant chemotherapy.

然而,烷化剂如环磷酰胺、拓扑异构酶II抑制剂、阿霉素、表阿霉素都与辅助化疗后的两种细胞遗传学不同的白血病的发生相关。

Our research focused on the synthesis of heterocyclic compounds through the reaction between the dihalogen compounds and amides or carbamates.

我们小组首次进行了二卤代化合物和酰胺或氨基酸酯之间偶联反应的研究,以期发展构筑氮杂环化合物的新方法。

TFC could remarkably inhibit the ear edema induced by dimethylbenzene in mice at the dose of 125,250,500mg.kg~(-1), the swelling of rats hind paws induced by carrageenan and primary inflammatory reaction in AA rats at the dose of 84,168,336 mg.kg~(-1) and reduce the weight of granuloma induced by cotton in rats at the dose of 84,168,336mg.kg~(-1), respectively.

TFC的免疫调节作用体外研究发现,TFC0.005,0.05,0.5,5,50 mg·L~(-1可明显提高环磷酰胺(cyclophosphamid,Cy)诱导免疫功能低下小鼠的脾淋巴细胞增殖反应,而对正常小鼠的脾淋巴细胞增殖无明显作用。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。