环胺

Both hexanitrohexaazatricyclododecanedione and hexanitrohexaazatricyclotetradecanedifuroxan are the typical representatives of fused ring-nitroamine. 4, l0-Dinitro-2, 6, 8, 12-tetraoxadiazatetrocyclo [5.5.0.0^(5.9). 0^(3.11)] dodecane is the typical representative of cage nitroamine.

六硝基六氮杂三环十二烷二酮和六硝基六氮杂三环十四烷并双氧化呋咱是稠环硝胺化合物中的典型代表；4， 10-二硝基－2， 6， 8， 12-四氧杂－4， 10-二氮杂异伍兹烷是笼形硝胺化合物中的典型代表。

The binding capacities of the water-soluble chitosan and its derivatives to taurocholate and glycocholate as bile salts were investigated in vitro.

修饰后的壳聚糖结合胆酸盐的能力增强，说明引入更多的胺基或铵基有利于对胆酸盐的结合，胺基上烷基与胆酸盐的甾环之间也应当产生疏水相互作用；同样我们在体外也研究了水溶性壳聚糖及其衍生物对硬脂酸钠和十二烷基硫酸钠的结合能力及其影响因素。

The formation of microemulsion system containing emulsifier,acrylamide,2-ethyltrimethyl ammonium chloride,sodium-2-acrylamido-2-methyl-propane-sulfonate and hexamethylene was studied.

对复配乳化剂(span+tw een)、丙烯酰胺、(2-甲基丙烯酰氧乙基)三甲基氯化铵、2-丙烯酰胺基-2-甲基丙磺酸钠和环己烷组成的微乳液体系进行了研究，研究了单体总质量浓度、AM摩尔含量和阴阳离子单体配比改变对形成微乳液需要的适宜H LB值和最小乳化剂用量的影响。

Thirteen benzimidazole derivatives were synthesized by one-step oxidative cyclisation of 1, 2-phenylenediamine or 4-methyl-1, 2-phenylenediamine at room temperature and a series of aromatic aldehydes under imidazolium salt grafted iodobenzene diacetate assisted.

以水为溶剂，在咪唑盐二醋酸碘苯促进下，通过邻苯二胺或4-甲基邻苯二胺与各种芳醛室温氧化环合，一步合成了13种苯并咪唑类衍生物，反应时间25~45 min，反应产率92%~98%。

Based on B-trichloroborazine with boron-nitrogen ring structure, the monomer was synthesized by substitution reaction with different molar ratio of propylamine/isopropylamine, then the corresponding polyborazine was obtained through thermal polymerization.

以三氯环硼氮烷为原料，将其与正丙胺/异丙胺进行共取代反应，制得了不同结构的取代单体，再经热聚合反应获得了相应的聚硼氮烷先驱体。

Based on B-trichloroborazine with boron-nitrogen ring structure, the monomer was synthesized by substitution reaction with different molar ratio of propylamine/isopropylamine, then the corresponding polylyborazine was obtained through thermal polymerization.

以三氯环硼氮烷为原料，将其与正丙胺／异丙胺进行共取代反应，制得了不同结构的取代单体，再经热聚合反应获得了相应的聚硼氮烷先驱体。

The details and results are summarized below:(1)An ABC style three component cascade reaction of aromatic aldehydes, aromatic amines and diethyl malonic ester or cyclohexanone has been developed.

论文从苯炔和亚胺出发，设计并系统研究了4种新的多组分串联反应，主要内容和结果如下：(1)发展了一种芳醛、芳胺和丙二酸二乙酯或环己酮的ABC型三组分串联反应。

Bis-imidazoline was prepared from triethylene tetraamine and N,N-dimethylformamide dimethyl acetal at 85℃ for 2 h with toluene as solvent, with a yield of 90.4%. The reaction of bis-imidazoline with 1,2-dibromoethane and potassium carbonate in acetonitrile provided with a monobromide salt yield of 78.7%. Hydrolysis of monobromide salt under aqueous causic solution formed 1,4,7,10-tetraazzcyclododecane in a 74.2% yield.

用甲苯作溶剂，使三乙烯四胺和N，N-二甲基甲酰胺二甲基缩醛在85℃反应2 h，得到中间体双咪唑啉，产率90.4%，在乙腈溶剂中，碳酸钾存在下，双咪唑啉和1，2-二溴乙烷进行扩环反应，得到环状中间体一溴盐，产率78.7%，一溴盐经碱性水解2 h，得到1，4，7，10-四氮杂十二烷，产率74.2%。

A series of newl naphthalenic sulfonated polyimides were synthesized using 1,4,5,8-naphthalenetetracarboxylic dianhydride, 2,2'-benzidinedisulfonic acid by one-step high temperature polymerization method. The sulfonated degree of SPI-X membranes was controlled through adjusting the molar ratio of BDSA to the non-sulfonated diamines.

采用1，4，5，8-萘四酸二酐、2，2′-联苯二胺双磺酸和APBA为单体，通过高温一步聚合法合成了含有噁唑环的新型磺化聚酰亚胺，通过调节二胺单体的比例控制磺化程度。

In a DMF solution of CuCl〓-ethanolamine-acetic acid (1: 2: 2), 27 formed a highly oxidized heterocyclic compound 2-hydroxymethyl-naphtho [1, 2-a] oxazole (30) by the carbon-nitrogen coupling and carbon-oxygen coupling with the ligand of ethanolamine, which brings a chance to develop a novel approach to this heterocyclic compound via one-pot reaction of phenols under mild condition.

在氯化铜—乙醇胺—乙酸（1：2：2）的DMF溶液中，27与配体乙醇胺发生碳氮偶合与碳氧偶合，生成深度氧化的杂环化合物：2-羟甲基-萘并[1，2-a]〓唑（30）。这可望为酚类一锅化直接转化为30及其类似物提供一种简便的新合成路线。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失