环甲的

The phytoplankton community was mainly composed of Cyanophyceae, Euglenophyceae, Bacillariophyceae, and Chlorophyceae, and the dominant species were Oscillatoria subtillissima, Dactylococcopsis irregularis, Euglena caudata, Melosira granulata, Cyclotella meneghiniana, Chlorella vulgaris, and Scenedesmus quadricauda. The main environmental factors affecting the distribution of phytoplankton species in July were ammonium-nitrogen, dissolved oxygen, water temperature, and total phosphorus, while those in September were pH, water temperature, dissolved oxygen, transparency, and total nitrogen. Water transparency and zooplankton were the main factors affecting the biomass of Cryptophyceae, Pyrrophyceae, and Bacillariophyceae; while nitrogen, phosphorous, and dissolved oxygen were the main factors affecting the biomass of Cyanophyceae, Euglenophyceae, and Chlorophyceae.

结果表明：调查期间共鉴定出浮游植物384种，隶属于8门，浮游植物密度范围为2.01×105～57.60×105 cells·L-1；群落组成以蓝藻、裸藻、硅藻和绿藻为主，主要优势种有细微颤藻、无常蓝纤维藻、尾裸藻、颗粒直链藻、梅尼小环藻、普通小球藻、四尾栅藻等；7月影响浮游植物分布的主要环境因子依次为铵态氮、溶解氧、水温和总磷，而9月的pH值、水温、溶解氧、透明度和总氮含量对浮游植物的分布产生影响较大；其中，透明度和浮游动物量是影响隐藻、甲藻和硅藻藻类生物量的主要环境因子，而蓝藻、裸藻、绿藻主要受水体氮磷营养盐浓度和溶解氧的影响。

Phenylenediamines, aminophenols, methoxyanil ines, and 1,4- hydroquinone, 1-naphthylamine were polymerized via the catalysis of horseradish peroxidase in mixed solvents of l,4-dioxane and water at amibient conditions by using hydrogen peroxide as the oxidant. Several factors influencing the polymer yield, such as the concentration of the substrate, pH value and oxidant amount were examined using a- phenylenediamine as substrate.

本文选择了苯二胺、氨基苯酚、甲氧基苯胺三个系列，以及对苯二酚、1-萘胺等单体，在二氧六环-水混合介质中以辣根过氧化物酶为催化剂，以双氧水为氧化剂进行了不同底物的室温酶促聚合，并以邻苯二胺为底物考察了溶剂用量、pH值、作为氧化剂的双氧水用量等条件对聚合物收率的影响。

None of them have been reported before. Some efforts were also made to find cupric ion as the right catayzer which could promote the cyclization of phenylhydrazine and a-bromoacetophenone efficiently.

为了扩展这一新的合成方法，我们用苯肼替代甲肼，发现在合适的催化剂存在下，苯肼也能够与α-溴代苯乙酮发生类似的环合反应，得到2，4-二苯基-1，2，3-三氮唑。

In thesecond chapter, eleven 1,3,4-oxadizoles bearing chiral pyrazolyl moieties(4a-k) andfive triazolotriazines bearing chiral pyrazolyl moieties(5a-e) were obtained from5-[(1"S)-1",2-diacetyl-oxyethyl]-1-phenylpyrazol-3-carboxaldehyde(1) with arylcar-bohydrazide or (5-aryl-1,2,4-triazin-3-yl)hydrazine through an intramolecular1,3-dipolar cycloaddition in the presence of the non-metal oxidant IBD.

其中第二章介绍了以D-葡萄糖为原料制得的5-[(1′S)-1′，2′-二乙酰氧基乙基]-1-苯基吡唑-3-醛(1)分别与芳基甲酰肼、(5-取代苯基-1，2，4-三嗪-3-基)肼反应，在无金属氧化剂—IBD引发下，发生分子内1，3-偶极环加成，采用&一锅煮&法合成了11种含手性吡唑基的1，3，4-噁二唑类化合物(4a-k)和5种含手性吡唑基的三唑并三嗪类化合物(5a-e)。

In this paper, 4-4-(trifluoromethoxy benzoyl cyclohexyl-3, 5-diaminobenzoate with a large branch chain, pyromellitic dianhydride and 4-(4-aminobenzyl) benzenamine were used to synthesize polyimides. The effect of monomer charge order on pretilt angle was investigated for the first time when PIs were used as LC alignment layer, and the effect of diamine mole ratio on pretilt angle was studied. The thermal stability of the pretilt angle was discussed.

文章用均苯四酸二酐、4，4'-二胺基二苯甲烷和具有较大支链的4-（4-苯甲酰基）环己基－3，5-二胺基苯甲酸酯等单体制备聚酰亚胺，首次研究了单体加料顺序对液晶预倾角的影响，同时也研究了二胺配比对液晶预倾角的影响问题，并探讨了预倾角的热稳定性等问题。

Synthesis of PPA are intermediate ester methoxy-pyrimidine main raw material; for quinoline acid synthesis; are prepared quinolones (such as: Pipemidic, Ciprofloxacin quinolinic acid, such as containing the quinolone drugs) of raw materials; also are manufacturing and other chemical products dyes intermediates.

是合成PPA的中间体甲氧基嘧啶酯的主要原料；用于喹啉酮酸的合成；是制备喹诺酮类药物(如：吡哌酸、环丙氟哌酸等含喹啉酮酸的喹诺类药物)的原料；亦是制造染料及其他化工产品的中间体。

Three types of dyes derived from crown ether benzotellurazole (including telluracarbocyanine, polymethine styryl dye and merocyanine dye) are formed by the methods analogous to non-crown ether dyes.

本文系统研究了冠醚苯并碲唑的各种合成方法，探讨了杂环的季铵化反应，并进一步制备了对称冠醚碲碳菁及冠醚苯并碲唑衍生的多甲川苯乙烯菁、部花青染料。

The glycyrrhizic acid antigen is prepared through the process including following steps: dissolving glycyrrhizic acid in N, N-dimethyl formamide, dioxane or dimethyl sulfoxide, heliophobically adding N-hydroxy succinimide, reacting with dicyclohexylcarbodiimide at 0-10 deg.c for 2-5 hr; and reacting with carrier protein at normal temperature for 4-6 hr to obtain glycyrrhizic acid antigen.

本发明所提供的甘草酸抗体，是用甘草酸抗原免疫动物，然后从被免疫动物的血清中分离得到的；所述甘草酸抗原按如下过程制备：先将甘草酸溶解在N，N-二甲基甲酰胺、二氧六环或二甲基亚砜中，避光加入N-羟基琥珀酰亚胺，然后在0-10℃条件下与二环己基碳二亚胺反应2-5小时；接着与载体蛋白常温反应4-6小时，得到甘草酸抗原。

Therefore, in the laboratory, a 2L gasliquid equilibrium measurement device was used to measure the equilibrium solubility of H2S, CO2, CH3SH and COS in the mixed solutions of Methyldiethanolamine, Tetramethylene sulfone respectively under different temperatures and different proportions. With the relevant parameters being correlated from the measured data, a corresponding thermodynamic calculation model was set up, based on the gasliquid two phase state equilibrium equation, and in combination with the overseas research results.

为此，在实验室利用容积为2 L的气液平衡测定装置，测定了不同温度和溶液配比条件下硫化氢、二氧化碳、甲硫醇、硫氧碳在甲基二乙醇胺（Methyldiethanolamine，MDEA）、环丁砜（Tetramethylene sulfone，TMS）水溶液中的平衡溶解度，并根据气液两相平衡状态方程，结合国外研究成果，利用测定的平衡溶解度数据关联出相关参数，建立了相应的热力学计算模型，用于预测该复杂体系中酸气分压与溶液负荷的气液平衡关系。

At the same time, we carried on to observe the pathogenic plant disease symptom characteristic in detail. 3. In lab,experimental result expressed that Difenoconazole 10% WP and Propiconazol 25% EC have the highest control effect, wheras Carbendazim 98％ WP and metalaxyl 25% WP almost can not repress development of cotton leaf spot pathogens.

室内药剂筛选试验研究表明，25%丙环唑乳油、10%世高可湿性粉剂对棉花叶斑病致病菌具有很好的抑菌效果，这两种杀菌剂的作用效果普遍高于其它药剂，是较为理想的化学防治药剂；98％多菌灵可湿性粉剂和25%甲霜灵可湿性粉剂，抑菌效果不理想，对病原菌生长的抑制作用普遍不明显。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。