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The pyrrole, oxazoles, pyridinones, quinolines, dibenzodiazepines, tetrahydrobenzoxazines and tetronic acids have been prepared from enaminones.

吡咯、唑烷、嘧啶酮、喹啉、二苯并二氮杂环类、四氢苯并噁嗪酮和特窗酸等都可以由烯胺酮类化合物制得。

Diamines are performed. An new and effective atom economy, domino reaction is developed, and 5, 6dihydro-4H-thieno [2, 3-b] thiopyran are synthesized by 4-(4-methyl-1, 3-dithiol-2-ylidene)-1, 7-diaryl-1, 6-diene-3, 5-dione

然后以4-[(4-甲基-1,3-二噻烷-2-亚甲基)-1,7-二芳基]-1,6-二烯-3,5-二酮类化合物为合成子探索稠杂环合成方法,并发现一个高效的,具有原子经济性的多米诺效应合成方法,并成功的利用其合成了一系列噻喃并噻吩衍生物。

Objective To investigate the change of plasma prostaglamdin I 2(PGI 2 ),endothelinand thromboxane B 2 (TXB 2 )in thrombogenic disease and its clinical significance.

目的 探讨血栓性疾病血浆前列环素(PGI 2 )、内皮素(ET-1)、血栓烷B 2 (TXB 2 )水平的改变及其临床意义。

Hydroxy-N,N-bis(2-aminoethyl)ethylamine was synthesized by addition alkylation of diethyl triamine with epoxyethane for the first time.

以二乙烯三胺和环氧乙烷为原料,通过加成烷化反应一步合成标题化合物,经多种谱学手段表征确证。

Two types of P Br N contained flame retardant,O (2,4,6 1 trioxo 1 oxyphosphabiscyclooctane 4 methylene) O (2,3 dibromopropyl)phosphoric melamine salt and O (2,4,6 tribromophenyl)phosphoric melamine salt,were synthesized from phosphorus oxychloride,pentaerythritol,2,3 dibromopropanol,2,4,6 tribromophenol and melamine,etc.

以三氯氧磷、季戊四醇、2 ,3 二溴丙醇、2 ,4,6 三溴苯酚及三聚氰胺等为原料合成了两种含磷溴氮阻燃剂,即O (2 ,4,6 三氧杂 1 氧基磷杂双环 [2 。2 。2 ]辛烷 4 亚甲基) O 2 ,3磷酸三聚氰胺盐和O (2 ,4,6 三溴苯基)磷酸三聚氰胺盐。

Hydroesterification of tert-butyl alcohol with ethanol catalyzed by transition metal triphenylphosphine complexes were investigated in room temperature ionic liquids as reaction medium at 100-140℃ and 3-6MPa of CO.

首次在超强酸氯铝酸离子液体中实现了饱和烷烃的羰化反应。发现2,2,4-三甲基戊烷可直接与CO反应,产物叔丁基异丁基酮,叔丁基异丁烯基酮和3,3,5-三甲基环己酮。

The compound 3, 9-bis (2', 4', 6'-tribromophoxy)-2, 4, 8, 10-traoxa -3, 9-dip- hosphospiro [5.5] undecane -3, 9-dioxide (HFR-1) was prepared with pentaeryth- ritol, phosphorus oxychloride and 2, 4, 6-tribromophenoxy soldium by esterifica- tion and condensation reaction.

以三溴苯酚钠、三氯氧磷、季戊四醇为原料,通过酯化和缩合两步反应合成了阻燃剂3,9-双(2',4',6'三溴苯氧基)-2,4,8,10-四氧代-3,9-二磷螺环-3,9-二氧[5.5]十一烷。

Based on above conditions, the prepared resin can absorb deionizing water over 600 times of its own weight and NaCl aqueous solution (9g/L) over 60 times.

在上述条件下制得的树脂的吸水率≥600g/g,吸盐率≥60 g/g,环己烷回收率为97.3%。

The effects of different of categories surfactants, the proportion of surfactant and cosurfactant , the chain lengths of alcohol and alkane, temperatures and pH values on the W/O microemulsion phase areas are systematically studied in the dissertation. SEM and laser scatting techniques are used to verify particles'sizes of W/O microemulsion. Consequently, a system TritonX-100/n-C〓H〓OH (weight ratio 1: 1)/C〓H〓/H〓O is obtained which is a stable system with relatively large W/O microemulsion phase area.

本文系统研究了表面活性剂种类、助表面活性剂的链长、表面活性剂和醇的配比、烷烃的链长以及温度、pH值等对W/O微乳液相区域的影响,并用SEM、激光光散射等对微乳液粒度进行了表征,从而获得一种稳定的、W/O微乳液区域较大的体系:壬基苯酚聚氧乙烯醚(TritonX-100)/正戊醇(质量比1:1)/环己烷/水体系。

In order to study the aldol condensation of 2,15-hexadecanedione on the surface of aluminium, the intermolecular condensationmechanism of acetone occurring on aluminum was simulated by usingsemi-empirical AM1 method embodied in MOPAC 6.0 program package.

为了研究2,15-十六烷二酮在氧化铝表面的环合机理,选择小分子丙酮为模型化合物,用量子化学半经验AM1方法研究双分子丙酮在氧化铝表面的醛醇缩合机理。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。