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Starting with commercial available tosylmethyl isocyanide and but-2-enoic methyl ester, pyrrolo[2,1-f][1,2,4]triazine derivatives was prepared by twelve-steps process in total yiled of 5.0%~8% via pyrrole and pyrrolo [2,1-f] [1,2,4] triazine ring formation, substitution and amination reactions etc.

本文以简单的对甲基苯磺酰甲基乙腈和反-2-丁烯酸为原料,经过形成吡咯,吡咯并[2,1-f][1,2,4] 三嗪环,取代,酰胺化等等12步反应,合成了结构新颖的吡咯并[2,1-f][1,2,4] 三嗪衍生物,总收率达5%~8%。

A reversed-phase high performance liquid chromatographic method was established for determination of isothiocyanates in human urine , which used the reaction of propyl isothiocyanate with 1,2-benzenedithiol as reference instead of the synthesis of 1,3-benzodithiole-2-thione.

省去合成1,3 苯二硫杂环五烯 2 硫酮这一步骤,直接用异硫氰酸丙基酯与1,2 苯二硫酚反应作标准,建立了尿液中异硫氰酸酯的反相高效液相色谱测定方法。

From Leontopodium nanum (collected from Zhang County, Gansu Province), 12 compounds were isolated, of which 9 compounds have been identified. Among them, a derivative of coumarin is new.

从采自甘肃漳县的矮火绒草全草的甲醇提取物中,采用同样方法共分离纯化得到12个化合物,鉴定了9个化合物的结构,其中有1个新化合物,命名为6,7-并二氧六环[2-(1-甲酯基-1-甲基)-甲烯基]-香豆素(1)。

A Michael addition of dimethyl malonate and 2-pentyl-cyclopentenone could conduct a precursor which used for preparing aim compound by a selective decarboxylation.

中间体化合物2-戊基环戊烯酮在一定条件下经Michael加成和选择性脱羧反应合成目标化合物。

Diverse products including monocyclic, tricyclic, and different tetracyclic products were isolated from the S.

为了更进一步的了解在不同的氨基酸改变下对於氧化鲨烯环化酵素酪氨酸-510所造成突变效应,我们继而利用&定点饱和突变&的方式来进行探讨。

Besides, the Tyr710Arg mutant produced two monocyclic products, achilleol A and camelliol C, and only the Tyr710Pro mutant lost the cyclase activity.

此外,在Tyr710Arg的突变株中也产生了两个单环的产物, achilleol A和camelliol C。而所有突变点中只有Tyr710Pro使氧化鲨烯环化酵素失去活性,且没有任何产物产生。

In this dissertation, polyethylene glycol monomethyl ether of 2000 molecular weight as soluble support, an array of soluble polymer-supported tartrate esters were designed, synthesized, and applied in asymmetric epoxidation of allylic alcohols.

本论文以平均分子量为2000的聚乙二醇单甲醚为可溶性支载体设计和合成了一系列可溶性聚合物支载的酒石酸酯配体,并将它们用于烯丙基醇的不对称环氧化反应。

The chemical analysis result of modified lignin by alkaline-oxygen treatment is as following:The chemical analysis result of modified lignin by alkaline-oxygen treatment showed that the carboxyl group of modified lignin increased, since muconic acid type structure were generated from phenolic structure by ring-open reaction during alkaline-oxygen treatment.

氧碱处理改性木素的化学分析结果见下表;┌────┬────┬─────┬────────────────┬────┐│改性本素│OCH_3│总糖│C_9单元式│COOH │├────┼────┼─────┼────────────────┼────┤│O_4 │8.49 │0.07 │C_9H_(10.45)O_(3.7)(OCH_3)_(053)│10.82 │└────┴────┴─────┴────────────────┴────┘氧碱处理改性木素的化学分析结果表明,改性木素的羧基含量明显增加,在氧碱处理的过程中,由于芳环的开裂,(来源:ABCe6论6d文网www.abclunwen.com)形成了己二烯二酸结构,因此改性木素具有较高的反应活性,易与Al~(3+)形成络合。

The present invention provides a multinuclear half metallocene compound in which two or more of transition metals of groups 3 to 10 on periodic table are connected through bridge ligand simultaneously containing Pi-ligand cycloalkandienyl group and Alpha-ligand functional group and its preparation, and a process for preparing styrene polymer using the compound as a catalyst.

本发明提供了一种其中的两个或更多元素周期表第3-10族过渡金属通过同时包含π-配体环烷基二烯基团和α-配体功能基团的桥配体连接的多核半金属茂络合化合物及其制备方法,及使用本化合物为催化剂的苯乙烯聚合体的制备工艺。

Reactor Construction: Multitube reactor systems for chemical industry ( all technical heat transfer fluids,particularly mkoltensalt 50 years experience) for production of:phthalic anhydride,maleic anhydride,acrolein,methyl methacrylate,methanol,ethylene oxide and other endothermic and exothermic catalytic gasphase processes.

反应器制造部:列管反应器系统,用于化学工业(所有工业用热交换流体,特别是熔盐传热)中生产苯酐,顺酐,丙烯醛,丙烯酸,甲基丙烯酸甲酯,甲醇,环氧乙烷及其他放热与吸热气相催化生产工艺。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。