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HPLC was coupled with both mass spectroscopy and ultraviolet absorption spectroscopy for simultaneous separation and characterization of the products from glow plasma reaction of chloroform.(3) Phosphorus pentachloride has been used to perchlorinate acenaphthene under moderate pressure and temperature in sealed reaction vessels.

在此基础上,以反相C〓柱为固定相,甲醇/乙醇/环己烷为流动相,采用梯度洗脱的方法,对氯仿辉光放电合成产物进行高效液相色谱-紫外光谱-质谱联用分离分析,成功的分离得到包括富勒烯C〓和全氯代碳簇在内的数十种产物,并得到了相应的质谱和光谱数据。

The kinds of compounds with AIE, AIEE and CIEE are summarized, mainly including siloles, substituted ethenes (mainly including fulvene and DPDSB style), CN-MBE, pyran, biphenyl compounds and polymers.

侧重总结了silole型、取代乙烯型(主要包括亚甲基环戊二烯型和DPDSB型)、腈取代二苯乙烯型、吡喃型、联苯型等小分子化合物和少数高分子的结构与AIE性质之间的关系,以及为解释AIE现象所提出的限制分子内的转动、避免非辐射去活、构象扭曲避免形成excimer、J-聚集态以及形成分子间的C-H/π键等理论。

In this paper, chiral molybdenum or tungsten 2'-pyridinyl alcoholate complex catalyzed asymmetric epoxidation of cis-1-propenylphosphonic acid in H2O was reported.

目前磷霉素的生产是通过以Na2WO4为催化剂、在乙醇中以30%的H2O2将顺丙烯膦酸环氧化得到消旋产物,再利用α-苯乙胺进行拆分而得到[2,3]。

The result indicates that those four resuscitation-inducing aromatic herbs mainly contain volatile oil ,and all contain alicyclic compounds; the volatile oil of Borneolum Syntheticum and Styrax both contain Sesquiterpenes of caryophyllene; as resin herbs , Styrax and Benzoinum both contain vanillin, resin ester and balsamic acid .

结果表明,四味芳香开窍药主含挥发油,均含有脂环化合物,并存在一些共有成分,如龙脑冰片与苏合香挥发油中均含有倍半萜类成分石竹烯;苏合香和安息香皆为树脂类中药,两者均含有香荚兰醛成分,尚含树脂酯,香脂酸等。

by summarizing and analysing the progress on studies of pharmacodynamic material basis of resuscitation-inducing aromatic herbs such as moschus,borneolum syntheticum,styrax,benzoinum, and exploring the generality of those herbs,to provide scientific reference for further studies on the relevance of common substance ,nature and the efficiency of restoring consciousness and inducing resuscitation of those herbs.the result indicates that those four resuscitation-inducing aromatic herbs mainly contain volatile oil ,and all contain alicyclic compounds; the volatile oil of borneolum syntheticum and styrax both contain sesquiterpenes of caryophyllene; as resin herbs , styrax and benzoinum both contain vanillin, resin ester and balsamic acid .

通过对芳香开窍药麝香、冰片、苏合香、安息香的药效物质基础研究进展的整理、分析,探索其共性,拟为深入研究该类药的共性物质—药性—开窍醒神效应之间的关联性提供科学参考。结果表明,四味芳香开窍药主含挥发油,均含有脂环化合物,并存在一些共有成分,如龙脑冰片与苏合香挥发油中均含有倍半萜类成分石竹烯;苏合香和安息香皆为树脂类中药,两者均含有香荚兰醛成分,尚含树脂酯,香脂酸等。

The catalyst Ti-MCM-41 is used in epoxidation of propylene, in which cumenen hydroperoxide is used as oxidant, alkalescence of solution, reaction temperature and solvent are tested.

将所合成的Ti-MCM-41催化剂用于CHP氧化丙烯的环氧化反应中,对反应液的酸碱性、反应温度及溶剂进行了考察。

One of them can efficient catalysed the alkene in the absence of dear additives by introducing an imidazole in the salen ligand.

其中分子内含咪唑的手性吡咯烷Mn催化剂成功实现了不加昂贵添加剂的情况下高效催化取代色烯环氧化反应。

The recent development about applications of ionic liquids to transition metal -catalyzed cyclization of alkyne and enyne compounds was introduced.

概述了离子液体在过渡金属催化炔及烯炔类化合物环合反应中应用研究进展。

As is well-known,the buckminsterfullerene〓was discovered by means ofmass spectrum with laser-evaporation pr...

富勒烯是三连接的笼形分子,其多面体的表面由五元环和六元环构成。

Ethane> toluene>1, 3, 5-trimethylbenzene>methyl isobutyl ketone>1, 4-Dioxane>isoprene> 1, 2, 4-trimethylbenzene>cyclohexane>1, 3-Butadiene>methyl butyl ketone were the most reactive VOC species in PRD.

化学活性排名前十位的化合物为:乙烯>甲苯>1,3,5-三甲苯>甲基异丁基酮>1,4-环氧乙烷>异戊二烯>1,2,4-三甲苯>环己烷>1,3-丁二烯>甲基丁基酮。

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I didn't watch TV last night, because it .

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Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

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