环戊烷

Three alicyclic dianhydrides, 1,2,3,4-cyclobutanetetracarboxylic dianhydride, 1,2,4,5-cyclopentanetetracarboxylic dianhydride, and 1,2, 4, 5-cydohexane tetracarboxylic dianhydride were polymerized with two aromatic diamines, 1,4-bis (4-amino-2-trifluoromethylphenoxy) benzene (6FAPB, a) and 4, 4'-bis(4-amino-2-trifluoromethyl phenoxy) biphenyl (6FBAB, b) respectively, via a two-step polycondensation procedure to afford two series of fluorinated semi-alicyclic polyimides.

分别将脂环族二酐单体1，2，3，4-环丁烷四酸二酐、1，2，4，5-环戊烷四酸二酐和1，2，4，5-环己烷四酸二酐与芳香族含氟二胺1，4-双（4-胺基-2-三氟甲基苯氧基）苯(6FAPB， a)和4，4'-双（4-胺基-2-三氟甲基苯氧基）联苯(6FBAB， b)反应制备两个系列的含氟半脂环族聚酰亚胺，研究了PI薄膜的热性能和光学性能。

Using mordern physical chemistry techniques (such as XRD、 TG-DTA、 IR、 XPS and 〓Xe-NMR)、 chemical adsorption techniques (NH〓-TPD、 H〓-TPD、 TPO、 TPR etc.) and pulse flow microreaction of n-hexane、 methylcyclopentene and n-hexane containing 0.2ppm thiophene, we studied mainly the following three points:(1). the changes occured during the calcination pretreatment of Pt ammine complex supported on β and L zeolites;(2). the effect of structure and acidity-basicity of zeolite on the dispersion and electron state of Pt particles; and (3). the influence of second metal component on the reactivity of nhexane aromatization and sulphur-resistance of Pt/L zeolite catalyst. Several interesting and valuable results are obtained and summerized as follows

本论文运用各种近代物理表征方法(XRD、BET、TG-DTA、IR、XPS和〓Xe-NMR)、化学吸附技术(NH〓-TPD、H〓-TPD、TPO、TPR等)和正己烷、甲基环戊烷及含噻吩正己烷的脉冲微反等方法，着重研究了(1)载Pt的β和L沸石在分解预处理过程中发生的变化；(2)沸石载体结构及酸碱性对Pt粒子分散及电子状态的影响；(3)第二金属组份对载Pt沸石催化剂上正己烷芳构化及抗硫性能的影响等，得到了某些有意义的结果。

Also made of polyether and cyclopentane Yingpao Xiangrong of the good.

另外制成的硬泡聚醚与环戊烷的相溶性较好。

In China an eight-step approach to the cis-bicyclic amine was adopted, including five-step route to cyclopentane-...

国内工业生产方法是以环己酮为原料经五步反应合成中间体1，2-环戊烷二甲酸，再经过三步反应完成顺式构型的建立和氮杂五元环的合成。

3 Recently, we reported an efficient tin-free version of this reaction involving thiophenol for the preparation of cyclopentane derivatives through a 1,5-hydrogen transfer/cyclization sequence [Eq.(1); AIBN=azobisisobutyronitrile].

最近，我们报道了高效的、不使用锡试剂而使用苯硫酚的反应，这个反应是通过1，5-氢转移/环化步骤制备环戊烷衍生物的[化学反应式(1)；AIBN=偶氮二异丁腈][4]。

The effects of reaction parameters such as temperature, pressure, and hydrogen to hydrocarbon ratio (H2/HC) on the hydroconversion of methylcyclopentane over Pt/HZSM-5 have been investigated in a fixedbed downflow reactor.

在连续流固定床反应装置上，考察了反应温度、压力及氢烃摩尔比等条件对甲基环戊烷临氢转化反应活性及扩环反应选择性的影响；结合反应评价结果和热力学分析，探讨了Pt/HZSM-5催化作用下MCP的扩环反应规律。

0 G of cyclopentyl bromide and 19.4 g of magnesium are reacted in ether or THF to give a cyclopentyl Grignard reagent.

一百十九点零克的环戊基溴或溴环戊烷和十九点四克的镁在乙醚或四氢呋喃中产生反应，形成一个环戊格氏试剂。

The additional activity of the mechanical mixture can be ascribed to the acid sites on dealuminated Y zeolite, where the activated hydrogen spilt over from the neighboring Pt sites could hydrogenate the adsorbed benzene with the formation of cyclohexane and methylcycloheptane.

发现虽然Y沸石本身没有加氢活性，但它的加入可以显著提高Pt/Al2O3的活性，因为在Pt中心上得到活化的氢可以快速溢流到邻近的沸石颗粒表面的酸中心上，并和吸附在其上的苯发生加氢反应生成环己烷和甲基环戊烷。

CH3OH could attack the phosphor atom in 1,3,2-dioxaphopholane of compiound (1) to give O-methyl O-hydroxyethyl-O-phthalimidoethyl thiophosphate in 85% yield; in the presence of potassium hydroxide aryl selenol could attack the carbon atom in 1,3,2-diox-aphopholane of the cyclic phospholipid conjugate of N^1-(2-furanidyl)-N^3--5-fluorouracil to give the corresponding product of ring-opening in high yields.

在室温下，以异丙醇作溶剂，苯硒酚与化合物2不反应。在氢氧化钾存在下，以异丙醇／水作溶剂（体积比20：1，在室温下，硒酚可以有效地进攻中化合物2中1，3，2-二氧磷杂环戊烷中的碳原子生成相应的开环产物。按照这一反应条件，顺利实现了硒酚对N^1-（2-呋喃基）-N^3-羟烷基-5-氟脲嘧啶硫代环甘油磷脂缀合物的亲核开环，生成甘油骨架的端碳原子上带有芳硒基新颖的磷脂核苷缀合物。

Dihydro-5H-cyclopentanopyridine, a key intermediate of Cefpirome, was synthesized from cyclopentanone and propargylamine under autoclave prompted by copper chloride.

以环戊酮和丙炔胺为原料，在高压釜中用氯化亚铜催化合成头孢匹罗关键中间体6，7-二氢-5H-环戊烷并吡啶。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。