环戊烯

Over the years, Masson's food additive brand -"Silver Valley" has been at the forefront of China Food Additive Industry forefront of the reform In 1984, the first in the domestic market development and production of soybean products for human consumption antifoamer; in 1988, took the lead in the domestic market development and production of edible spices - cyclopentyl enol methyl ketone; in 1989, took the lead in the domestic market to develop speed-fat cake oil; In 1992, the first in the domestic market development and production of ice cream and beverage emulsion stabilizer; in 1999, introduced the internationally advanced level molecular distillation Monoglyceride domestic exclusive CPP realize industrial production

多年来，美晨公司的食品添加剂品牌--"银谷"一直站在中国食品添加剂工业改革的潮头 1984年，率先在国内市场开发生产豆制品食用消泡剂；1988年，率先在国内市场开发生产食用香料--甲基环戊烯醇酮；1989年，率先在国内市场开发速发蛋糕油；1992年，率先在国内市场开发生产冰淇淋和饮料乳化稳定剂；1999年，推出具有国际先进水平的分子蒸馏单甘酯，在国内独家实现CPP工业化生产

In this paper, the synthesis ways and applications of 4,5-dimethyl-l,3-dioxolen -2-one were introduced. An appropriate way synthesizing DMDO from acetoin via acylation, cyclization and dehydrochlorination was selected. The influences of various process conditions on the reaction were studied in detail, and the optimum process conditions were obtained by single factor experiments.

本文介绍了医药中间体4，5-二甲基-1，3-二氧杂环戊烯-2-酮的应用情况和合成路线，选择了适于工业化生产的工艺路线，即采用羟基丁酮为原料，经酰化、环合和脱氯化氢等步骤合成DMDO，并采用单因素试验法详细研究了各项工艺条件对反应结果的影响规律，确定了优化工艺条件。

The method of one-step cyclopentene oxidation with hydrogen peroxide as oxidizer is the trend of research and development of glutaraldehyde in the future because its raw materials are cheap and easy obtainable.

指出吡喃法是目前国内外合成戊二醛普遍采用的方法，以过氧化氢为氧化剂的环戊烯一步氧化法具有原料价廉易得等特点，是今后研究开发的方向。

Glutaraldehyde was prepared by oxidation of cyclopentene with aqueous solution of hydrogen peroxide.

用过氧化氢水溶液氧化环戊烯制得戊二醛。

Under the optimized reaction conditions: n (H2O2)/n/n=2/0.04/1,V/V=8.75, reaction temperature 35℃, and reaction time 28 h, the highest yield of glutaraldehyde could reached 78% with a cyclopentene conversion of 99.99%.

在最佳工艺条件：n(H2O2)：n：n=2：0.04：1，V/V=8.75，反应温度35℃，反应时间28h下，环戊烯转化率达99.99%，戊二醛的收率最高可达78%。

Cyclopentene catalytic oxidation synthesis techniques which had good prospect were introduced with great emphasis,and positive significance of establishing large-scaled chemical plant of glutaraldehyde near the locality of raw material specially in north of China,was pointed out.

着重介绍了前景看好的环戊烯催化氧化合成工艺方法，指出在接近原料产地，特别是中国北方地区建立规模化戊二醛生产装置，具有积极的意义。

The heterogeneous W-HMS catalyst was in-situ prepared by immobilization of tungstic acid on hexagonal mesoporous silica. It was used to synthesize glutaraldehyde from cyclopentene.

采用原位合成法将W(上标 6+)引入六方介孔全硅分子筛骨架中，制备了应用于环戊烯催化氧化合成戊二醛反应的W-HMS催化剂。

A Michael addition of dimethyl malonate and 2-pentyl-cyclopentenone could conduct a precursor which used for preparing aim compound by a selective decarboxylation.

中间体化合物2-戊基环戊烯酮在一定条件下经Michael加成和选择性脱羧反应合成目标化合物。

The mechanism of the UV-induced photochemically photochromic process of 1,2-bis-(2',5'-bimethyl)-3'-thienyl-perfluoro-cyclopentene was investigated using two-dimensional(2D) FTIR spectroscopy.

利用二维相关红外光谱方法首次研究了1，2-二（2'，5'-二甲基-3'-噻吩）－全氟环戊烯在紫外光照引发下发生光化学闭环反应的历程。

Hydrogen peroxide(H_2O_2)was used as oxidant,oxalic acid as complexing agent and tungstic acid (H_2WO_4)as catalyst.

研究了以环戊烯为原料、草酸为有机络合剂、H2O2为氧化剂，在催化剂钨酸(H2WO4)的作用下一步合成戊二酸的绿色新过程，考察了氧化剂的含量、反应物配比、催化剂用量、反应温度、反应时间等对反应的影响。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失