环己醇

Methods: from prepation of crude drug as start, study the technology of extract and defat with L9 (3~4) orthogonal test. With EtOH extraction and water sed, alkali washing, EtOAC extraction as main methods of eliminate dopant. Finally with alky AlzO3 chromatographic column, rich and gain anticancer active site. The maximum response was achieved at a 40 min extracting time with 10 times volume 90% EtOH added to the sample for the first time and 30 min for the second time. Adding 10 times water will produce precipitation; Place the precipitation into 6 times petroleum benzin to de-fat at 60℃.

云南红豆杉中抗癌活性物制备工艺研究方法：利用正交设计试验L9(3~4)确定原料药提取工艺为：10倍量90％乙醇提取两次，第一次40分钟，第二次30分钟；醇提液用10倍量水沉；沉淀加6倍量石油醚40℃脱脂；用1mol／L的NaOH溶液碱洗，除去酸性杂质；以碱性氧化铝柱，以环己烷／丙酮为洗脱溶剂，在环己烷-丙酮(6：4)段富集到所需活性部位，洗脱剂用量为3VB。

Water,Hydrogenated Polyisobutene,Cyclohexasiloxane,Glycerin,Alcohol Denat,Cetearyl Alcohol,PEG-20,Petrolatum,C13-14 Isoparaffin,Zea Mays Oil,Tocopheryl Acetate,Hydroxypropyl Tetrahydropyrantriol,Hydrolyzed Soy Protein,CI 14700/Red 4,Phenoxyethanol,Adenosine,PEG-100 Stearate,Ethylparaben,Triethanolamine,Polyacrylamide,Malus Domestica Stem Cell Culture,CI 19140/Yellow 5,Dimethyl Isosorbide,Dimethicone,Dimethiconol,Limonene,Xanthan Gum,Pentaerythrityl Tetra-Di-T-Butyl Hydroxyhydrocinnamate,Linalool,2-Oleamido-1,3-Octadecanediol,Capryloyl Salicylic Acid,Acrylates/C10-30 Alkyl Acrylate Crosspolymer,Passiflora Edulis Seed Oil,Disodium EDTA,Castanea Sativa Seed Extract,Butyrospermum Parkii· Cetyl Alcohol,Butylene Glycol,Octyldodecanol,Cetearyl Glucoside,Methylparaben,Citronellol,Prunus Armeniaca Kernel Oil,Laureth-7,Coumarin,Oryza Sativa Bran Oil,Glyceryl Stearate,Fragrance

水，甘油，氢化聚异丁烯，液体石蜡/矿油，丁二醇，环己硅氧烷，鲸蜡醇，甘油硬脂酸酯，棕榈油，玉米胚芽油，PEG-100硬脂酸酯，白蜂蜡/蜂蜡，肉豆蔻醇肉豆蔻酸酯，石蜡，香精，腺苷，苧烯，山梨醇，CI 14700，CI 19140，稻糠油，杏仁油，EDTA二钠，羟丙基四氢吡喃三醇，苯氧乙醇，聚乙二醇-14M，异十六烷，氢氧化钠，辛基十二醇，季戊四醇四（双-t-丁基羟基氢化肉桂酸）酯，山梨坦三硬脂酸酯，水解大豆蛋白，卡波姆，鸡蛋果籽油，苹果果实提取物，欧洲栗籽提取物，异山梨醇酐二甲醚，聚山梨醇酯-80，辛酰水杨酸，2-油酰胺基-1，3-十八烷二醇，氯苯甘醚，麦芽糖醇，香豆素，黄原胶，微晶蜡，丙烯酰胺/丙烯酰基二甲基牛磺酸钠共聚物，丙二醇，芳樟醇，香茅醇，玉米油，羟苯丙酯，羟苯甲酯

Chromatography peaks were obtained by GC-MS and 56 compounds were identified. The main components were linalyl butyrate (30.212%),(1α, 3α, 4β, 6α)-4,7,7-trimethyl-bicycloheptan-3-ol (10.940%),-4-carene (1.826%), 4-methylene-1-(1-methylethyl)-bicyclo [3.1.0] hexane (1.109%),β-myrcene (1.170%), limonene (5.784%), 3, 7-dimethyl-1, 6-octadien-3-ol (5.742%), n-hexadecanoic acid (0.914%) and-9, 12-octadecadienoic acid (2.952%), etc.

用GC-MS分离出69个峰，鉴定出56种物质，主要成分为：芳樟丁酸酯(30.212%)、(1α， 3α， 4β， 6α)-4，7，7-三甲基－双环[4.1.0]庚烷－3-醇(10.940%)、-4-蒈烯(1.826%)、4-亚甲基－1-（1-甲基乙基）－双环[3.1.0]环己烷(1.109%)、β-月桂烯(1.170%)、柠檬烯(5.784%)、3，7-二甲基－1，6-辛二烯－3-醇(5.742%)、n-棕榈酸(0.914%)、-9，12-十八碳烯酸(2.952%)等。

Aiming at demand of national economy and linking the actual condition of domestic refinery chemical , a routine with cyclohexene as main raw material was developed in the thesis.

本文针对国民经济发展的需求，结合我国精细化工行业的实际，进行了以环己烯为主要原料，合成1，2-环己二醇的研究。

Silicasulfuric acid was used as the catalyst for synthesis of Cyclohexanone 1, 2-propylene ketal from cyclohexanone and 1, 2-propylene glycol. The effect of catalyst dosage, molar ratio and reflux time to reaction were investigated.

以磺化硅胶为催化剂，以环己酮和1，2-丙二醇为原料合成环己酮1，2-丙二醇缩酮，考察了催化剂的用量、原料配比和回流时间对反应的影响。

The ketalization of cyclohexanone and 1,4-butanediol catalyzed by the Hβ zeolite was studied.Effects of reaction time,mole ratio of reactants and amount of catalyst on the yield of ketal were studied.Results showed that the Hβ zeolite was an efficient catalyst for the synthesis of ketal.

研究了Hβ分子筛催化1，4-丁二醇与环己酮的缩合生成新型七元环缩酮的反应，考察了反应时间、酮与醇的配比、催化剂用量、催化剂重复使用等因素对醛与醇缩合反应的影响。

The paper take the Ce (SO4)2/PAn as catalyst and cyclohexanone, 1,2-propylene glycol as raw materialr to synthesize cyclohexanonel 1,2-propylene glycol ketal.

以硫酸高铈[Ce (SO4)2]掺杂聚苯胺为催化剂，环己酮和1，2-丙二醇为原料，催化合成环己酮1，2-丙二醇缩酮。

A series of 3 - aryl - 3 -( 5,5 - dimethyl - 3 - hydroxy - 2 - cyclohexene - 1 - one - 2 - yl) propanoic ester s were synthesized by reaction between aromatic aldehydes ,5,5- dimethyl -1,3-cyclohexanedione and isopropylidene malonate catalyzed by KF - Al2O3 in alcohols.

在KF-Al_2O_3催化下，将芳香醛3，5-二甲基-1，3-环己二酮及丙二酸亚异丙酯在醇中反应，一锅式合成了一系列的3-芳基-3-(5，5-二甲基-3-羟基-2-环己烯-1-酮-2-基)丙酸酯。

Condensation of cyclohexanone and pentaerythritol catalyzed by iodine supported on activated carbon was investigated.

为了研究活性炭负载单质碘催化合成季戊四醇双缩酮催化活性，以季戊四醇和环己酮为原料，合成环己酮季戊四醇双缩酮。

The Company perennial operating a variety of organic chemical raw materials, varieties include: methanol, ethanol, ethylene glycol, n-butyl alcohol, isobutyl alcohol, isopropyl alcohol, acetic acid, vinyl acetate, acetic acid acetate, acetic acid small lipid , styrene, toluene, phthalic anhydride, xylene, acetone, butanone, cyclohexanone, DMF, sulfuric acid, methyl isobutyl ketone, glycol ether, three toluene, octyl resin, melamine, etc. and so on.

本公司常年经营各种有机化工原料，品种有：甲醇、乙醇、乙二醇、正丁醇、异丁醇、异丙醇、冰醋酸、醋酸乙烯、醋酸乙脂、醋酸丁脂、苯乙烯、甲苯、苯酐、二甲苯、丙酮、丁酮、环己酮、DMF、硫酸、甲基异丁基酮、乙二醇丁醚、三甲苯、二辛脂、三聚氰胺，等等。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。