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Cyclohexane with Mn as a catalyst in Trial 3 gave a total conversion of cyclohexane of 73% and 28.8% of which were oxygenates which contained 15.2% of dimethyl succinate, 19.6% of dimethyl glutarate and 65.2% of dimethyl adipate.

环己烷锰作为催化剂在审判3了总转化环己烷的73 %和28.8 %,其中含氧化合物其中载有15.2 %的二甲基丁二酸, 19.6 %的二甲基戊二和65.2 %的二己二酸。

Methods: from prepation of crude drug as start, study the technology of extract and defat with L9 (3~4) orthogonal test. With EtOH extraction and water sed, alkali washing, EtOAC extraction as main methods of eliminate dopant. Finally with alky AlzO3 chromatographic column, rich and gain anticancer active site. The maximum response was achieved at a 40 min extracting time with 10 times volume 90% EtOH added to the sample for the first time and 30 min for the second time. Adding 10 times water will produce precipitation; Place the precipitation into 6 times petroleum benzin to de-fat at 60℃.

云南红豆杉中抗癌活性物制备工艺研究方法:利用正交设计试验L9(3~4)确定原料药提取工艺为:10倍量90%乙醇提取两次,第一次40分钟,第二次30分钟;醇提液用10倍量水沉;沉淀加6倍量石油醚40℃脱脂;用1mol/L的NaOH溶液碱洗,除去酸性杂质;以碱性氧化铝柱,以环己烷/丙酮为洗脱溶剂,在环己烷-丙酮(6:4)段富集到所需活性部位,洗脱剂用量为3VB。

Ophenyl phenol,ophenyl phenol sodium salt tetrahydrate,7ADCA,2ethyl phenyl hydrazine hydrochloride,2,3dihydrofuran,7ethyl3(2hydroxy ethyl)indole,methyl ester of etodolac; 1,8diethyl1,3,4,9tetrahydropyrano[3.4b] indole1acetic acid methyl ester,5chloro2methoxy benzoic acid,4(2aminoethyl)benzene sulfonamide,5cyano phthalide,phthalhydrazide,9thioxanthenone,n[(1,4benzodioxane2yl)carboxyl]piperazine HCL,2chloro4amino6,7dimethoxyquinazoline,2chloro benzimidazole,1(4fluorobenzyl)2chlorobenzimidazole,2methylthio4pyrimidone,5amino4imidazole carboxamide HCL,6chloro2hexanone,11oxo6.11hydrodibenzothiepin,6,11dihydrodibenzooxepin11one,10,11dihydrodibenzocyclohepten5one;dibenzosuberone,dibenzo cyclohepten5one;dibenzosuberenone,3,5dihydroxy benzoic acid,3,5dihydroxy benzyl alcohol,2mercapto benzimidazole,3,4dihydroxy benzaldehyde,3,4dihydroxy benzonitrile,2amino5chloro benzonitrile,2(4chlorophenoxy)ethyl chloride,2(4chloro phenoxy)tert,butane,ditrimethylol propane;DTMP,2,2bis(4hydroxyphenyl)butane; bisphenol B,1,1'bis(4hydroxyphenyl)cyclohexane;bisphenol Z,tetrabromobisphenolS,3,5ditertbutyl salicylic acid,3,4,5trihydroxy benzoic acid stearyl ester,1,2,4trimethoxybenzene.

华业公司产品:邻苯基苯酚,邻苯基苯酚钠盐,7氨基3去乙酰氧基头孢烷酸,邻乙基苯肼盐酸盐,2,3二氢呋喃,7乙基色氨醇,依托度酸甲酯,5氯2甲氧基苯甲酸,4(2氨乙基)苯磺酰胺,5氰基苯酞,双酮酞嗪,9噻吨酮,N〔(1,4苯并二恶烷2基)羰基〕哌嗪盐酸盐,2氯4氨基6,7一二甲氧基喹唑啉,2氯苯并咪唑,1(4氟苄基)2氯苯并咪唑,2甲硫基4嘧啶酮,5氨基咪唑4 甲酰胺盐酸盐,6氯2已酮,11氧6.11二氢苯并〔b.c〕虑平,11氧代6,11二氢二苯并氧杂卓,10,11二氢二苯并环庚烯5酮,二苯并环庚烯5酮,3,5二羟基苯甲酸,3,5二羟基苯甲醇,2巯基苯并咪唑,3,4二羟基苯甲醛,3,4二羟基苯腈,2氨基5氯苯腈,2(4氯苯氧基)1氯乙烷,2(4氯苯氧基)叔丁烷,双丙烷,2,2二(4羟基苯基)丁烷;双酚B,1,1'双(4羟基苯基)环己烷;双酚Z,2[3,5二溴4(2,3二溴丙氧基)]苯砜,3,5二叔丁基水杨酸,3,4,5三羟基苯甲酸十八烷基脂,1,2,4三甲基氧基苯。

Was obtained in Trial 8 where the total cyclohexane conversion was 78% with 74% of the starting cyclohexane converted to oxygenate.

获得了审判8的总环己烷转化率78 %与74 %的转换开始环己烷氧化。

Using benzophenone as a probe, the energytransfer mechanism was studied by pulse radiolysis experiments on TOP-BP-CH andTBPO-BP-CH system. The results showed that organo phosphoryl compounds canaccept energy from excited CH and capture a proton from geminate pair .

结果表明含磷酰基有机化合物在能量转移过程中有双重作用:一方面从环己烷激发态接受激发能,另一方面从环己烷偕离子对〓夺取质子,发生质子转移过程。

The result was compared with oxidations of cyclohexene without irradiation and at irradiation without catalyst.

另外,本文还研究了各种类型的催化剂在中压汞灯下光催化环己烯的氧化反应,结果表明,无论上述的哪种催化剂,在中压汞灯下光催化环己烯氧化反应,都得不到环氧环己烷,生成的产物主要为水和二氧化碳。

The method ensures safety and enhances heat transfer, and can remarkably improve the oxidizing reaction speed of cyclohexane and the total selectivity of cyclohexanone, cyclohexanol and cyclohexyl hydrogen peroxide.

该方法具有安全性,强化了热量的传递,可显著地提高环己烷氧化反应速度,提高环己酮、环己醇和环己基过氧化氢的总选择性。

When a solution of cis-1-t-butyl-4-chlorocyclohexane in ethanol is refluxed for several hours, the major product is found to be trans-1-t-buty1-4-ethoxycyclohexane.

答:顺-1-t-丁基-4-氯环己烷在ethanol中回流几小时主要产物得到反-1-t-丁基-4-乙氧基环己烷

In this paper we study the biodegradation of petroleum wastewater by microorganisms with a new way.For the chain alkyl hydrocarbon in crude oil, strains were isolated by screening and acclimatizing at the existence of diesel oil and kerosene. For the aroma hydrocarbon in crude oil, strains were isolated by screening and acclimatizing at the existence of phenol.

本试验我们针对石油中的链烷烃,分别以柴油和煤油为代表物进行筛选得到以降解链烷烃为主的菌种:针对石油中的芳香烃,以苯酚为代表物进行筛选得到以降解芳香烃为主的菌种:针对石油中的环烷烃,以环己烷为代表物进行筛选得到以降解环己烷为主的菌种。

ASpheric FeNi nanoparticles with average diameter of about 70 nm were obtained in the system of cetyltrimethyl ammonium bromide/H_2O,while most of the products were nanofilms/rods with the addition of cyclohexane; nearly monodisperse FeNi nanoparticles with average diameter of about 25 nm were prepared in the system of PEG/cyclohexane/H_2O.With the assistance of ultrasonic,a no-surfactant method to 8.5 nm FeCo nanocrystals with high Ms(>200.5 emu/g)has been developed with economical FeCl_3·6H_2O as iron sources.

a以水合肼为还原剂在十六烷基三甲基溴化铵/H_2O体系中得到了平均粒径约70 nm的FeNi合金球形颗粒,当在此体系中加入环己烷时样品主要形态为纳米膜/棒;于PEG/环己烷/H_2O体系中制备了单分散性较好的平均粒径约25 nm的FeNi合金纳米颗粒,合金纳米颗粒粒径随金属离子浓度减小而减小。

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Finally, according to market conditions and market products this article paper analyzes the trends in the development of camera technology, and designs a color night vision camera.

最后根据市场情况和市面上产品的情况分析了摄像机技术的发展趋势,并设计了一款彩色夜视摄像机。

Only person height weeds and the fierce looks stone idles were there.

只有半人深的荒草和龇牙咧嘴的神像。

This dramatic range, steeper than the Himalayas, is the upturned rim of the eastern edge of Tibet, a plateau that has risen to 5 km in response to the slow but un stoppable collision of India with Asia that began about 55 million years ago and which continues unabated today.

这一引人注目的地域范围,比喜马拉雅山更加陡峭,是处于西藏东部边缘的朝上翻的边框地带。响应启始于约5500万年前的、缓慢的但却不可阻挡的印度与亚洲地壳板块碰撞,高原已上升至五千米,这种碰撞持续至今,毫无衰退。