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The present doctoral dissertation was carried out to study the chemical constituents isolated from stems of two medicinal schisandraceous plants.34 compounds were isolated from the ethanol extracts of the stems S.henryi collected in the Jiangxi province by various column chromatographies.27 of them were identified on the basis of spectral analysis.There are 18 lignans,(including 5 dibenzocyclooctadienes,6 aryltetralins,2 tetrahydrofurans,3 diarylbutanes,2 other lignans),3 flavanols,2 glyceroesters,1 naphthoquinone,1 xanthine and 2 steroids,of which 6 compounds were new compounds,and 7 compounds were isolated from this family for the first time.

采用多种色谱技术进行分离纯化,从翼梗五味子藤茎的乙醇提取物中分离到34个化合物,综合运用现代波谱学技术鉴定了27个化合物,包括木脂素类化合物18个(其中联苯环辛烯类木脂素5个,芳基四氢萘类木脂素6个,四氢呋喃类木脂素2个,二芳基丁烷类3个,其他类型木脂素2个),黄烷醇类化合物3个,甘油酯类化合物2个,萘醌类化合物1个,黄嘌呤类化合物1个,甾体类化合物2个,其中,5个为新化合物,7个为本科首次报道。

A new method for the synthesis of 1 methyl 3 propyl pyrazol e 5 carboxlic acid from 2 pentanone and diethyl oxalate is reported.

以 2 -戊酮和草酸二乙酯为起始原料,经缩合、与甲基肼环合、水解等三个步骤合成了 1 -甲基-3-丙基吡唑-5 -羧酸。

As one of aliphatic polyether-ester, poly (p-dioxanone) shows not only excellent biodegradability, biocompatibility and bio-absorbability, but also good flexility, tensile strength and knot strength. The PPDO has already been used in some biomedical materials such as suture, bone repair device and may have potential application in peroral or parenteral drug delivery systems.

聚对二氧环己酮是脂肪族聚醚酯的一种,不仅具有优良的生物降解性、生物相容性和生物可吸收性,而且具有出色的柔韧性、抗拉强度和结节强度,可应用于生物医用材料,例如手术缝合线、骨科修复材料等,并在口腔和非肠道给药系统中具有潜在的应用前景。

A series of mono-, sesqui-, di- and tri-terpenoids with various structural types, which produced by bio- oxidation, hydrogenation, hydrolyzation, esterification and cyclic cleavage toward-limenone, were analyed by GC-MS.

经GC-MS分析发现该两细菌对-柠檬烯有显著的生物催化转化作用,能对底物进行不同程度的氧化、还原、水解、酯化、开环等反应,并产生丰富的系列结构不同的其它萜类化合物:包括单萜、倍半萜、二萜、以及三萜等。

Starting from tetrafuran, 2_(4_Aminosulfonylphenyl)_4H_1,2_thiazine_1_dioxide, an antiepileptic drug with special structure, was obtained via esterification, sulphonation, chloridization, condensation and cyclization.

以四氢呋喃为原料,经酯化、磺化、酰氯化、缩合、环化等步骤,合成了化学名为 4_(四氢_2H_1,2_噻嗪基_2 )苯磺酰胺_S_S_二氧化物的抗癫痫药舒噻嗪,通过IR、1HNMR和元素分析对其结构进行了表

Synthesis of the antiepileptic tiagabine hydrochloride;2. Starting from tetrafuran, 2_(4_Aminosulfonylphenyl)_4H_1,2_thiazine_1_dioxide, an antiepileptic drug with special structure, was obtained via esterification, sulphonation, chloridization, condensation and cyclization.

以四氢呋喃为原料,经酯化、磺化、酰氯化、缩合、环化等步骤,合成了化学名为 4_(四氢_2H_1,2_噻嗪基_2 )苯磺酰胺_S_S_二氧化物的抗癫痫药舒噻嗪,通过IR、1HNMR和元素分析对其结构进行了表

Ingredients:shea butter extract, cetearyl alcohol, hexadecyl trimethyl ammonium bromide, methylcyclohexyldimethoxy silane, poly dimethyl siloxane, tetradecanoic acid isopropyl ester, glycerol, amino silicone oil.

成分:,乳木果提取液,十六,十八混合醇,十六烷基三甲基氯化铵,环甲基硅氧烷,聚二甲基硅氧烷,肉豆蔻酸异丙酯,甘油,氨基硅油。

To improve water resistance of starch adhesives, tolylene diisocyanate and epichlorohydrin were used as cross linking agents.

以甲苯二异氰酸酯和环氧氯丙烷为交联剂,对氧化淀粉进行两步交联改性,提高了淀粉胶黏剂的耐水性。

This paper reviews the recent progress on the Chinese syntheic research of marine natural products according to type classifications: marine cyclopeptides, cembranes, cembrenss, cembranolides, quinolone derivativcs, triacetonamine and subergorgic acid analogues.

本文综述中国海洋天然产物合成研究的最新进展,包括海洋环肽、西松烷和西松烷型二萜内酯、喹啉酮衍生物和三丙酮胺以及柳珊瑚酸类似物等。

In this work,the non\|aqueous carbonyl nickel slips were prepared by ball\|milling using Cyclohexanone\|butyl alcohol,Glycerol trioleate,Poly\|vinyl\|butyl and polyethylene glycol as the solvent,dispersant,binder and plasticizer,respectively.

本文以环己酮丁醇为溶剂,三油酸甘油酯为分散剂,以聚乙烯醇缩丁醛为粘结剂,聚乙烯乙二醇为增塑剂,通过球磨工艺制备了非水基羰基镍粉浆料。

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