环二酯

Their structures were confirmed by elemental analysis, 1H NMR, and IR spectral data. The preliminary bioassay results showed that α-phenyl-sul-fonylcyclododecanone oxime 2,4-dichlorophenoxy acetate (8p) had inhibition ratio 100% and 80.07% against Digitaria sanguinalis Scop., and 100% and 88.70% against Abutilon theophrasti Medic. at concentrations of 100 and 1 mg/L.

初步生物活性测定结果显示，部分化合物具有一定的除草活性，如α-苯磺酰基环十二酮肟-2，4-二氯苯氧乙酸酯(8p)在浓度为100和1 mg/L时对马唐的抑制率分别为100%和80.07%；对苘麻的抑制率分别为100%和88.70%。

The results of clinical assessment showed that levosimendan was safe and effective which could improve the prognosis of the patients and kept normal blood kinetics. By improving the reported synthetic route, levosimendan was synthesized from acetanilide via eight steps of reaction.

本论文探索了左西孟旦的合成路线，对文献报道的合成工艺进行了合理有效的改进，以乙酰苯胺为原料，最终经Friedel-Crafts反应，羰基α-位溴代，丙二酸二乙酯缩合，水解，脱羧，环合，拆分及重氮化加成等八步反应合成了左西孟旦。

Disodium petroleum cyclocarboxylic monoethanolamine sulfosuccinate was synthesized from petroleum cyclocarboxylic acid methyl ester via amidation,esterification and sulfonation.

利用石油环烷酸原料合成出石油环烷酸单乙醇酰胺磺基琥珀酸单酯二钠盐。

In addition to the multi-ring alkenyl ethers and alpha-fluorinated acrylates, additional monomers comprising one or more cyclic aliphatic and heterocyclic compounds, both unsubstituted and substituted, in particular dihydropyrans, may be incorporated into the photosensitive polymers.

除了多环烯基醚和α-氟化丙烯酸酯之外，可向所述光敏聚合物引入另外的单体，所述单体包括一种或多种未取代的和取代的环状脂肪族化合物和杂环化合物，特别是二氢吡喃。

The epoxidised cashew nut shell oil acrylate oligomer for UV curing materials was synthe- sized using epoxidised cashew nut shell oil and acrylic acid as main raw materials,N,N-dimethyl- benzylamine as catalyst and p-hydroxyanisole as inhibitor.

以N，N-二甲基苄胺作催化剂、对羟基苯甲醚作阻聚剂，环氧化腰果壳油和丙烯酸为主要原料合成了一种新型的紫外光固化预聚物——环氧化腰果壳油丙烯酸酯。

The molecule of taxol is an extremely complex diterpene with a taxane ring structure fused with a four-membered oxetane ring, an ester side-chain at position C-13 and a benzoyl side-chain at the C-2 position Fig.

紫杉醇分子是一个极其复杂的四环二萜类化合物：一个紫杉烷环加一个四个元素组成的氧烷环，在C-2和C-13上还分别有一个苯氧基和酯基侧链。

This protocol could also be used for the selective reduction of the endocyclic double bond of the 3-electron withdrawing group substituted coumarins. This method is clean, mild, and efficient.2 ZrCl_4 / HEH was found to be a selective and efficient reagent combination for the direct reductive amination of electron rich aldehydes and ketones with weakly basic amines after scanning various catalysts such as InCl_3, BiCl_3, CF_3COOH and so on.

图一 1。我们用汉斯酯作为有机还原剂，乙醇为溶剂，实现了4-甲叉基噁嗯唑酮和吡唑酮环外双键的高选择性还原；此外，我们还将这一还原体系用于3-吸电子集团取代-3，4-二氢香豆素环内双键的选择性还原。

By treatment of (4R)-carboxy-(2S)-phenylthiazolidine with isocyanic acid benzyl ester in CH_3COOH/(CH_3CO)_2O system,the reaction time is shortened from 17 h to 3 h,and the yield of (7aR)-3-phenyl-1H,3H-imidazo[1,5-c] thiazole-(6H, 7aH) 5,7-dione is raised from 75% to 93%.

改用异氰酸苄酯为关环试剂环化合成了(7aR) 3 苯基 6 苄基 1H，3H 咪唑并[1，5 c]噻唑 5，7 二酮，选用CH3COOH/(CH3CO)2O代替CH3COOH作溶剂，反应时间由17h缩短为3h，产率从75%提高到93%。

This dissertation focuses on the solid phase synthesis of several kinds of heterocyclic compounds from the resin bound cyclic malonic acid ester.

本论文从丙二酸环酯聚合物试剂出发，利用该试剂，完成了一系列的杂环化合物的固相合成研究，主要包括以下几个方面：一、制备了5-

In the first part of this thesis, a formal [4+2] cycloaddition of ketenes with N-benzoyldiazenes catalyzed by chiral NHCs was studied, which gave 1,3,4-oxadiazin-6-ones in very high yields and enantioselectivites.

论文的第一部分内容是在手性氮杂环卡宾的催化下，烯酮与N-苯甲酰偶氮化合物的环加成反应，合成各种手性的噁二嗪酮，它们还可以经过简单的两步一锅法制备手性氨基酯。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。