环

Bromo-2-sulfolene (2) reacted with substituted benzoic acid salt s 3a～3c or alizarin yellow (3d) to give four novel allylic substitution products 4a～4d by esterification reaction, respectively.

以3，4-二溴环戊砜(1)为原料，在无水吡啶作用下发生消除反应，得到反应中间体4-溴-2-环戊烯砜(2)，再分别与一系列取代苯甲酸盐3a～3c以及茜素黄GG(3d)发生酯化反应，合成出4种新环戊烯砜衍生物4a～4d，并用IR，1HNMR，MS，元素分析等表征了它们的结构。

In different conditions on fluidized state and stability of conical fluidized bed. The conlusions are: the conical angel of the conical fluidized bed is 20°, the fluidized state havesmall difference in conical distributor and distributor plate. The angle of conical bed increase,the fluidized state will have big difference. The angle is 60°and the conical as distributor, themass of fluidized is less, the most of material is the bottom of conical bed. The effect ofdistributor plate is much better than the conical distributor. Sawdust and rice hull can fluidize.The annular gap of conical distributor different, the angle of conical bed is same, the fluidizedquality of 10mm annular gap is better than the other conical distributors. The annular gap ismore wide, the conical bed have more slugging phenomenon and the pressure fluctuate is turnbig.In the experiment the flow of 2％and 4％distributor plates don\'t easy to control, becausethe pressure is very big and the pressure fluctuate of conical bed is too big.

在不同的条件下对锥形床的流化状态和稳定性进行了研究，结果得出：锥形床的锥角为20度时，分布锥和分布板的流化状态相差不明显，随着锥形床锥角的增大，分布锥和分布板的流化现象会出现明显的变化，锥形床锥角越大，分布锥的流化状态变化越明显，流化的的物料越少，大量物料都聚集在锥形床底部，而分布板在加料量少的情况下，能流化起来。10mm、15mm和20mm环隙分布锥在锥形床锥角相同条件下，10mm环隙分布锥的流化质量要好于其它两个分布锥，环隙越大越容易出现腾涌现象的产生，压降波动范围增大。2％、4％和6％开孔率分布板在本实验测定时，2％和4％开孔率分布板的流量不容易调节，同时产生的压降波动范围也很大，比较来说，6％开孔率分布板流化质量好些。

With the help of modern computational fluid dynamics tecnology, this thesis carries on a numerical simulation of annulus multiphase flow of the conventional auger drill stabilizer; it points out the deficiency of the annulus gas in cutting-carrying and lifting; and attempts to develop a drill stabilizer that are suitable for the gas drilling.

本文试图借助现代计算流体力学技术，对常规螺旋钻柱稳定器环空多相流动规律进行数值模拟研究，指出在环空气体携岩举升方面存在的不足，开发一套适合于气体钻井的新型钻柱稳定器，提出全井段环空流场改善方法，实现气体钻井防斜打快，减少冲蚀，提高井眼净化能力的目的。

First, we consider nonholonomic chained systems with modeling error, in this section,based on back-stepping , using the so-called adding a integrator , state-scaling technique , we design discontinuous feedback law,such that the trival solution of the closed-loop systems global strong stable; Second,we consider high-order nonholonomic chained systems with modeling errors and external disturbances, in this section,using input/state-scaling and integrator backstepping methods , we design discontinuous feedback law and give out the switching strategy, such that the closed-loop systems global /C-exponential stable; Finally, we consider a class of more general power chained form systems with particular drift-terms, in this section , using Lyapunov method, we design time-varying feedback law , such that the closed -loop systems p—exponential stable.

第一部分考虑的模型为带有模型误差的高阶非完整链系统，我们运用加幂积分器、State-scaling技巧以及基于Back-stepping方法构造出不连续反馈律，从而使得所讨论系统的闭环系统的平凡解全局强稳定；第二部分考虑的模型为带有模型误差的不确定高阶非完整链系统，这一部分我们运用input／state scaling和integrator backstepping方法构造出不连续反馈律，并给出切换策略，使得所对应的闭环系统全局κ-指数稳定；第三部分考虑的系统是形式更为一般的且带有特殊形式漂移项的幂链系统，利用Lyapunov函数方法，设计出时变反馈律，从而使得相应的闭环系统ρ-指数稳定。

By the balance of communication link power, SNR balance guidelines and BER balance, under the base to meet the requirements of systems and not affecting thequality of call. Finally, the open-loop/closed-loop variable step length reverse power control is introduced, its principle is under the original open-loop power control to select suitable power control step by the new power control bit, and achieves a balanced system fastest and most effective.Keywords: Step, Power-control, Brethren interference, Proximity effect

依据通信链路的功率平衡准则、信噪比平衡准则和误码率平衡准则，在满足系统要求和不影响通话质量的基础上，最后提出了开环/闭环可变步长的反向功率控制，其原理是在原有的开环功率控制的基础上，依据新的功率控制比特，来选取合适的功率控制步长，以最快、最有效的方法使系统达到平衡。

First, the ring based load balance data storage method divides the sensor networks into a lot of rings and stores data among all nodes within a ring.

首先，负载平衡数据存储协议将传感器网络划分为多个环，在网络工作的某个时间段内，数据被分散存储在某个环内的多个节点上；其次，该存储结构的最大特点是，在不同时间段内，各环轮换工作进一步消除热点。

The vapor phase Beckmann rearrangement of cyclohexanone oximeover RBS-1 catalyst was carried out in a continuous flow fixed bed reactor under atmosphere pressure.

在常压连续流动固定床反应装置上，考察了反应温度、环己酮肟质量空速、溶剂种类、环己酮肟浓度、载气流量、水的质量分数等反应条件或反应氛围对环己酮肟气相Beckmann 重排反应的影响。

Through taken the measurements of pH, TOC, UV-Vis spectra and high-performance liquid chromatograph in the degrading process of solution ,it was found that the COD of dye solution increased, pH continuing declined and TOC reduced gradually. The UV-Vis spectra and high-performance shown that though dye molecules had been destroyed, Strong Chromophore Azo Double Bond of dye was certainly under attack, the big conjugated system was vandalized and dye molecules were decolorized degradation, but they were not completely changed into carbon dioxide and other inorganic matter by mineralization, it appeared accumulation of aromatic ring and double benzene nucleus, so it is thus evident that complete destruction of aromatic ring is more difficult than the double benzene.

通过测定直接大红染料脱色过程中的溶液pH、TOC、紫外可见光谱图和高效液相色谱图可知，在脱色处理时间(6h)范围内，染料溶液的COD值增大， pH值持续下降，TOC值逐渐降低，结合紫外可见光谱图和高效液相色谱图，说明染料分子虽然已经遭到破坏，染料分子内强生色基团偶氮双键确实遭到攻击，大的共轭体系被破坏，染料分子被脱色，却没有完全被彻底矿化成二氧化碳等无机物，出现了芳环和萘环结构的累积现象，可见完全破坏芳环比破坏偶氮双键发色团更困难。

Pressure sensor and pressure switch controller can be used in tathode ring machine to check the pressure on real time and warn automatically.

介绍了压力传感器在碱性锌锰电池制环机上的应用，在粉环成型机上利用压力传感器和压力转换控制器对粉环重量进行实时监控，实现自动报警功能，提高产品稳定性。

Based on finite element method,stiffness characteristics were investigated under different whirling angle, pedestal parameters ,and fit clearance,to present guidance for design of elastic ring.

本文针对两种弹性环刚度的计算方法——解析法和有限元法进行了对比，分析了各自的适用条件，并基于有限元法分析了涡动角、凸台参数和配合间隙对弹性环刚度的影响，为弹性环的结构设计提供了参考。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。