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Better denitrification efficiency could be obtained with adding amylo and the removal ratios of ammonia nitrogen were at least 93%. The removal ratio of TN increased gradually with the increasing of C/N ratio. When C/N ratio was 10, the best removal ratio of TN could reach 80.81%. But when C/N ratio added on 12, the ratio removal of TN was not increased only keeping about 75%.

投加淀粉调整C/N比,系统能取得良好的脱氮效果,氨氮的去除均在93%以上,随着C/N比的增加,TN的去除也逐渐的增大,当C/N为10时,TN最高去除能达到80.81%,但当C/N增大到12时,TN的去除不再增大,只是稳定在75%左右。

Path analysis showed that N translocation rate of culm was higher for the high fresh ear yield varieties,while the N translocation rate of culm and tassel was higher for the high fresh kernel yield varieties,and the N translocation rate of leaf,bracteal leaf and ear axis was higher for the high kernel yield varieties.In addition,higher N translocation rate of leaf had a beneficial effect on N utilization efficiency as for fresh ear,fresh kernel or maturity kernel of the produce of waxy corn.

通径分析表明,鲜穗高产品种茎秆的氮素转移较高,鲜子粒高产品种茎秆和雄穗的氮素转移较高,成熟子粒高产品种叶片、苞叶及穗轴的氮素转移均较高;叶片的氮素转移高有利于品种鲜穗、鲜子粒及成熟子粒氮素利用效的提高。

The effect of zeolites ion-exchanged by transition metals on thermal catalytic cracking reaction is studied. The product distributions of the cracking reactions catalyzed by theβor ZSM-5 zeolites exchanged with transition metals are different from that catalyzed by corresponding Hzeolites, which means the mechanism of cracking reactions has varied. Group Ⅷ metals Fe, Co, Ni and Cu, Zn are shown to be of strong catalytic activity of oxidative dehydrogenation, while Ti and Cr are not of oxidative activity. Catalyzed by zeolites or catalyst containing Ag, conversion of thermal catalytic cracking reactions and the yield of ethylene increase while the yield of propylene does not decrease. Silver can not only promote the formation of carbonium ion, but also convert carbonium ion into free-radical via redox reaction. The weak adsorption of olefins on silver reduces the occurrence of hydrogen transfer and dehydrogenation. As a result, the yield of light olefins is favored by silver in the catalyst.

采用过渡金属交换的分子筛作为催化剂,进行催化热裂解制取乙烯的反应,研究发现,在β沸石分子筛和ZSM-5分子筛中引入过渡金属后,催化热裂解反应的产物分布与相应的氢型分子筛相比有了较大的变化,说明过渡金属的加入对于催化热裂解反应的机理具有影响,Ⅷ族金属如Fe、Co、Ni和第Ⅰ、Ⅱ副族Cu、Zn表现出较强的氧化脱氢活性,产物中氢气、焦炭的产很高,Ti、Cr则未表现出氧化作用:分子筛及催化剂中引入银后,催化热裂解反应的转化和乙烯的产有了提高,丙烯产没有很大的变化,说明银在催化热裂解反应中能够促进正碳离子的生成,又有可能通过氧化-还原作用部分改变反应机理,促进了自由基的生成,并且由于银对烯烃的吸附很弱,其氢转移反应和脱氢、加氢活性比较低,有利于烯烃产的提高。

The preliminary bioassary showed that at the concentration of 100μg/mL, the inhibitory rate of compounds Ⅴc to Fusarium graminearum was 81.3%;Ⅳe to Fusarium oxysporium was 83.4%;Ⅴe and Ⅴf to Cercospora sorghi were 79.7% and 72.4% respectively;Ⅳd to Fusarium graminearum and Fusarium oxysporium were 68.9% and 65.7% respectively.

初步生物测试结果表明:在质量浓度为100μgmL下,化合物Ⅴc对小麦赤霉病菌的抑制达到了81.3%;化合物Ⅳe对马铃薯干腐病菌的抑制达到了83.4%;化合物Ⅴe,Ⅴf对玉米弯孢病菌的抑制也分别达到了79.7%和72.4%;化合物Ⅳd对小麦赤霉病菌和马铃薯干腐病菌的抑制分别达到了68.9%和65.7%。

The results showed that N6+TDZ0.05 mgL^(-1)+NAA0.01 mgL^(-1)+KT0.50 mgL^(-1) was most suitable for Platanthera mandarinorum with an induction rate of 92.5%; N6+TTDZ0.05 mgL^(-1)+KT0.50 mgL^(-1) was most suitable for Coeloglossum viride with an induction rate of 98%; N6+IAA0.01 mgL^(-1) was most suitable for Platanthera mandarinorum with a germination rate of 96%; N6+IAA0.01 mgL^(-1)+GA30.01 mgL^(-1) was most suitable for Coeloglossum viride with a germination rate of 94.5%.

结果表明,最适合长白舌唇兰原球茎和类原球茎诱导的培养基为N6+TDZ0.05mgL^(-1)+NAA0.01 mgL^(-1)+KT0.50 mgL^(-1),诱导为92.5%;最适合凹舌兰原球茎和类原球茎诱导的培养基为N6+TDZ0.05 mgL^(-1)+KT0.50 mgL^(-1),诱导为98%;长白舌唇兰类原球茎萌发为完整植株的最佳培养基为N6+IAA0.01 mgL^(-1),萌发为96%;凹舌兰类原球茎萌发为完整植株的最佳培养基为N6+IAA0.01 mgL^(-1)+GA30.01 mgL^(-1),萌发为94.5%。

Theory; the spatial meshing theory includes comparative motion, comparative differential and conjugative curved surface; and the application of meshing theory includes gear drive and worm drive. The spatial meshing theory is the main part of the course.

课程的重点讲解内容有曲线的参数方程、切线、法面、弧长、曲、空间曲线的基本公式、挠及平面曲线的基本公式等;曲面第一和第二基本公式,法曲、主方向和主曲、欧拉公式、短程挠、欧拉公式和贝特朗公式推广、相对法曲和相对短程挠等;刚体的绝对和相对运动速度、相对微分和绝对微分、相对速度和相对微分、轨迹曲面的法曲和短程挠等;空间共轭曲面的啮合条件、诱导法曲、两类界限点、等距共轭曲面、空间啮合的二次接触原理等;蜗杆传动的数学模型建立及啮合特性分析方法等。

A synthesis of 2-pentylidene cyclopentanone starting from cyclopentanone and n-valeraldehyde through aldol condensation, followed by dehydration, was studied, and the yield reached 85.6%. 2-Pentenyl cyclopentanone was prepared in a yield of 95.0% from 2-pentylidene cyclopentanone with a hydrogenation methodology. Through Baeyer-villiger oxidation,δ-decalactone was synthesized in a yield of 63.9% from 2-pentenyl cyclopentanone with hydrogen peroxide.

研究了以正戊醛和环戊酮为起始原料,经羟醛缩合、脱水反应合成2-戊叉环戊酮,产达到85.6%,2-戊叉环戊酮加氢制备2-戊基环戊酮,产为95.0%,2-戊基环戊酮在双氧水作用下经Baeyer-villiger氧化重排反应合成δ-癸内酯,反应产为63.9%,合成δ-癸内酯的总产为52.0%,气相色谱分析纯度为98.7%。

Results The DNA was obtained from PPJ through a nasopancreatic tube. Aberrant p16 methylation and K- ras gene mutation were detected in the same samples of PPJ. Sensitivity,specificity,positive predictive values,negative predictive values and accuracy of HE staining for pancreatic cancer were 40%,100%,100%,45.4% and 60.0%,respectively. Of the 20 cases of pancreatic cancer,K- ras gene mutation was detected in 14 (70%) and the p16 gene was shown to be methylated in 7 (35%). Of the 8 cases of chronic pancreatitis,K-ras gene mutation was detected in 2 (25%). Of the 2 cases of mucinous cystoadenoma of pancreas,K-ras gene mutation was detected in 1 (50%). Aberrant methylation of p16 was not detected in pancreatic juice samples from patients with chronic pancreatitis and mucinous cystoadenoma of pancreas.

结果 所有胰液标本均成功抽提出DNA,30例胰腺疾病病人胰液标本同时进行了K-ras基因突变和p16基因启动子区5′CpG岛甲基化检测,其中20例胰腺癌病人胰液中K-ras基因突变为70%(14/20),p16基因甲基化为35%(7/20),8例慢性胰腺炎中K-ras基因突变为25%(2/8),2例胰腺囊腺瘤病人中K-ras基因突变为50%(1/2),慢性胰腺炎和胰腺囊腺瘤病人胰液中无p16基因甲基化。

Results l.Serum concentrations of VCAM-1 in PIH (93.39 + 57.3)ug/ml were higher than that in normal pregnant group. Serum concentrations of VCAM-1 in moderate(97.89 + 34.07)ug/ml and severe PIH(132.24 + 60.97)ug/ml were significantly higher than that in normal group.(P.05, P.01). There was no difference between serum levels of VCAM-1 mild PIH and normal pregnant group. 2.Serum levels of IL-6 in PIH group(102.17 ?48. 31)pg/ml were significantly higher than that in normal group(49.16 + 12.9)pg/ml.Serum levels of IL-6 in moderate(95.79+31.19)pg/ml and severe PIH( 127.27+11.3 8)pg,ml were significantly higher than that in normal group. There was no difference between serum levels of PIH in mild PIH (52.13 + 12.90)pg/ml and normal pregnant group. 3. In PIH group, serum concentrations of VCAM-1 correlate with the levels of IL-6,r=0.63. 4.The expression of VCAM-1 in cytotrophoblast of spiral arteries in normal pregnant group(100%) were significantly higher than that in PIH group.Theexpression of VCAM-1 in moderate PIH(37.50%) and sever PIH were lower than that in normal group.There was no difference between the mild PIH and normal group.Conclusions The increased levels of serum of VCAM-1 may participate in the process of vascular endothelium damages in PIH.

结果 1、妊高征组血清VCAM-1浓度为(93.39±57.3)μg/ml明显高于正常妊娠组(44.87±15.60)μg/ml,差别有显著性(P<0.05);中、重度妊高征组VCAM-1浓度分别为(97.89±34.07)μg/ml和(132.24±60.97)μg/ml,与正常妊娠组比较,差异有显著性(p<0.05)和非常显著性(P<0.01);轻度妊高征组VCAH-1为(48.46±15.60)μg/ml与正常妊娠组比较,差异无显著性(P>0.05)。2、妊高征组血清IL-6含量为(102.17±48.31)pg/ml,明显高于正常妊娠组(49.16+12.9)pg/ml,差异有非常显著性(P<0.01);中、重度妊高征组IL-6含量分别(95.79±31.19)pg/ml和(127.27±11.38)pg/ml,与正常妊娠组比较,差异有显著性(P<0.05)和非常显著性(P<0.01);轻度妊高征组IL-6含量为(52.13±12.90)pg/ml与正常妊娠组比较,差异无显著性(P>0.05)。3、VCAM-1与IL-6水平呈明显正相关,r=0.63(P<0.01)。4、子宫胎盘床螺旋动脉滋养细胞VCAM-1表达,正常妊娠组都存在阳性表达(阳性表达100%),妊高征组有10例阳性表达阳性表达为叩们,差别有非常显著性河<0.01L 中、重度妊高征组阳性表达分别为37、50%和0,与正常妊娠组比较,差别有显著性河<0.05)和非常显著性汀<0.01太轻度妊高征组阳性表达为83.33凡与正常妊娠组差别无显著性问>0.05)。

The results showed that, with the increase of reaction temperature, the catalytic deacidifcation and non-catalytic deacidification ability of MgO were basically decreased at lower space velocity and gradually increased at higher space velocity.

结果表明,随着反应温度的升高,MgO的催化脱酸和非催化脱酸在较低空速下降低,在较高空速下逐渐增加;MgO的催化脱酸和非催化脱酸在335~365 ℃范围内均随空速的增加而降低;在反应过程中降低反应系统的压力有利于MgO的催化脱酸反应。

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