猪去氧胆酸

The taurohyodeoxycholic acid was synthesized by aminolysis of sodium taurine with carboxy-carbonate mixed anhydride prepared by reacting hyodeoxycholic acid with ethyl chloroformate at the present of triethylamine.

猪去氧胆酸与氯甲酸乙酯在三乙胺存在下反应生成羟酸－碳酸乙酯混合酐，而后将其与牛磺酸钠进行氨解反应，合成猪磺去氧胆酸。

Results Both bile arisaema and hyodeoxycholic aicd had the same main spot and color on the plate which was separated well with other spots.

结果 胆南星药材和猪去氧胆酸对照品在薄层板上主斑点位置及颜色一致；且斑点集中，分离度好。

OBJECTIVE To investigate the impurities of the hyodeoxycholic acid and its purification.

目的 研究猪去氧胆酸中的杂质成分和纯化方法。

RESULTS AND CONCLUSION Hyodeoxycholic acid was purified by recrystallization and column chromatography.

结果与结论从猪去氧胆酸中分离出一种主要杂质，建立了纯化猪去氧胆酸的方法。

Hyodeoxycholic acid ; pig bile ; TLC scanning

猪去氧胆酸；猪胆汁；薄层扫描法

Methods Hyodeoxycholic acid and bilirubin in Calculus Bovis were separately identified by TLC, and the cholic acid content was determined by TLCS with the scan wavelength of λ=380 nm,λ=650 nm.

①用薄层色谱法分别鉴别猪去氧胆酸和胆红素；②用薄层扫描法测定胆酸含量，扫描波长：λ=380nm，λ=650nm。结果薄层色谱法可以区分体外培育牛黄和人工牛黄。

Results TLC can be used for the identification in-vitro cultured Calculus Bovis and artificial Calulus Bovis, the samples containing cultured Calulus Bovis showed the specific spots of bilirubin but no hyodeoxycholic acid spot while the samples containing artifical Calulus Bovis showed the hyodeoxycholic acid spot but no bilirubin spot.

含人工牛黄的样品有猪去氧胆酸斑点，含体外培育牛黄的样品未检出有与猪去氧胆酸对照品相对应的斑点；含人工牛黄的样品不显胆红素斑点，含体外培育牛黄的样品显示与胆红素对照品相对应的斑点。

Eleven molecular tweezer artificial receptors based on hyodeoxycholic acid have been synthesized by using solid K2CO3 as supporter through the reaction of methyl hyodeoxycholate with aroyl chloride in solvent-free conditions under microwave irradiation.

吴秀明；赵志刚*；刘兴利；陈宇；赵潇湘摘要：在微波辐射无溶剂条件下，以固体K2CO3为载体，猪去氧胆酸甲酯与芳酰氯反应合成了11个猪去氧胆酸分子钳人工受体。

Chenodeoxycholic acid ,cholic acid,ursodeoxycholic acid ,hyodeoxycholic acid,deoxycholic acid,Dehydrocholic acid

熊去氧胆酸，鹅去氧胆酸，猪去氧胆酸，胆酸，去氧胆酸，去氢胆酸，胆酸钠，去氧胆酸钠，猪去氧胆酸钠，猪胆盐，牛胆盐，禽胆盐，猪胆粉，牛胆粉，三号胆盐

The intermediates of manufacturing process include the hydrolyzed solution, the aqueous solution of Radix Isatidis extraction, the aqueous solution of Fructus Gardeniae extraction, the aqueous solution of Flos Lonicerae Japonicae extraction, the aqueous solution of baicalin, the alcohol solution of mixteure composed by cholic acid and hyodeoxycholic acid, 4-blended solution, 6-blended solution, the blended solution of baicalin and ASFLJE and 8-blended solution.

清开灵注射剂处方由胆酸、猪去氧胆酸、水牛角、黄芩苷、板蓝根、栀子、金银花和珍珠母组成，其生产过程中间体包括水解液、板蓝根液、栀子液、金银花液、黄芩液、四混液、胆酸混合液、六混液、银黄液和八混液。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！