物

New contributions of this work are as follows:(1). Preparation of Spherical MgCl_2-Supported Late-Transition Metal Catalysts for Ethylene PolymerizationFacile and effective immobilization of late-transition metal catalysts. 2,3-bis-(2,6-diisopropylphenyl) butane diimine nickel dibromide (1) and 2,6-bis-[1-(2,4,6-trimethylphenylimino)ethyl]pyridine iron dichloride (2), for ethylene polymerization has been achieved, using spherical MgCl_2 supports obtained by thermal dealcoholization of MgCl_2·2.56C_2H_5OH, and the effects of dealcoholization temperature on supported late-transition metal catalysts and the properties of resultant polymers were studied, the results indicated that:1.Supports with appropriate mechanical strength, high surface area and high porosity could be prepared by thermal dealcoholization of spherical MgCl_2·2.56C_2H_5OH supports; 2.BET, XRD, IR, SEM, GPC and DSC analyses indicate that the activities of the supported late-transition metal catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature.

本工作的新贡献如下：(1)、球形氯化镁负载后过渡金属催化荆催化乙烯聚合本文将配合物2，3-双(2，6-二异丙基苯亚胺)丁烷二溴化镍(1)和配合物2，6-二[1-(2，4，6-三甲基苯亚胺)乙基]吡啶二氯化铁(2)分别直接负载于经不同热脱醇温度处理的球形氯化镁载体上，研究了氯化镁载体的脱醇温度对负载化后过渡金属催化剂及其聚合物的影响，研究表明：1、通过对球形MgCl_2·2.56C_2H_5OH载体进行热脱醇处理，可以获得合适机械强度、较高比表面积和较高孔隙度的球形氯化镁载体；2、BET，XRD，IR，SEM，GPC和DSC研究表明，脱醇温度极大地影响负载后过渡金属催化剂的活性和聚合物的性能。

New contributions of this work are as follows:(1). Preparation of Spherical MgCl_2-Supported Late-Transition Metal Catalysts for Ethylene Polymerization Facile and effective immobilization of late-transition metal catalysts. 2,3-bis-(2,6-diisopropylphenyl) butane diimine nickel dibromide (1) and 2,6-bis-[1-(2,4,6-trimethylphenylimino)ethyl]pyridine iron dichloride (2), for ethylene polymerization has been achieved, using spherical MgCl_2 supports obtained by thermal dealcoholization of MgCl_2·2.56C_2H_5OH, and the effects of dealcoholization temperature on supported late-transition metal catalysts and the properties of resultant polymers were studied, the results indicated that: 1.Supports with appropriate mechanical strength, high surface area and high porosity could be prepared by thermal dealcoholization of spherical MgCl_2·2.56C_2H_5OH supports; 2.BET, XRD, IR, SEM, GPC and DSC analyses indicate that the activities of the supported late-transition metal catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature.

本工作的新贡献如下：(1)、球形氯化镁负载后过渡金属催化荆催化乙烯聚合本文将配合物2，3-双(2，6-二异丙基苯亚胺)丁烷二溴化镍(1)和配合物2，6-二[1-(2，4，6-三甲基苯亚胺)乙基]吡啶二氯化铁(2)分别直接负载于经不同热脱醇温度处理的球形氯化镁载体上，研究了氯化镁载体的脱醇温度对负载化后过渡金属催化剂及其聚合物的影响，研究表明： 1、通过对球形MgCl_2·2.56C_2H_5OH载体进行热脱醇处理，可以获得合适机械强度、较高比表面积和较高孔隙度的球形氯化镁载体； 2、BET，XRD，IR，SEM，GPC和DSC研究表明，脱醇温度极大地影响负载后过渡金属催化剂的活性和聚合物的性能。

Three Texas drovers met on the highway and proceeded to dicker as follows: Says Hank to Jim:"I'll give you six pigs for a hoss; then you'll have twice as many critters in your drove as I will have in mine."

得克萨斯州的三个贩子在公路上碰头，打算进行下述的物物交换。汉克对吉姆说："我用6 头猪换你1 匹马，那么你的牲口数将是我所有牲口数的2 倍。"

The rubber composition for covering a carcass cord of the present invention comprises 25 to 80 parts by mass of silica, 1 to 15 parts by mass of a silane coupling agent and 3 to 30 parts by mass of an organic vulcanizing agent represented by the following general formula (1):- n - wherein R is -(CH 2 -CH 2 -O) m -CH 2 -CH 2 -; x is an integer of 2 to 6; n is an integer of 10 to 400; and m is an integer of 2 to 5, based on 100 parts by weight of a diene rubber, and a tire prepared by using the rubber composition.

以100重量份的二烯橡胶为基准，本发明的用于包覆胎体帘线的该橡胶组合物包含25～80质量份的二氧化硅、1～15质量份的硅烷偶联剂和3～30质量份的由如下化学式(1)表示的有机硫化剂：- n -，其中R是-(CH 2 -CH 2 -O) m -CH 2 -CH 2 -；x是2～6的整数；n是10～400的整数；并且m是2～5的整数，以及使用该橡胶组合物制备的轮胎。

Furthermore, two kinds of oligonucleotides with same size and difference sequence were successfully separated.

建立了分析2个丫SNP的单碱基引物延伸反应，掌握了单碱基引物延伸反应的规律。

The crystallization of the blends were investigated by wide angle X-ray diffraction and polar light microscope . The results show that PPEKK in the blends deforms the crystallization of PPS but don't change its crystal structure.

用广角X射线衍射和偏光显微镜对共混物的结晶性能进行了研究，结果表明PPEKK对共混物中PPS的结晶作用有阻碍作用，但没有改变PPS的晶相结构。

All PSI complexes could be solubilized by high concentration of Digitonin. Different area of thylakoid membrane could be separated by Tween-20 and PSI complex could be found in them solubilized by Digitonin.

高浓度的毛地黄皂苷能够获得全部的PSI复合物；Tween-20能够分离不同区域的类囊体膜，结合毛地黄皂苷处理均能够获得PSI复合物。

Recent progress for β-diketone derivatives were reviewed based on reading a great deal of related literature including Photoluminescence and Electroluminescence of rear earth metal complexes and the photoelectric properties of multi-pyridine Ru complexes.

本论文在大量文献调研的基础上，对β-二酮的结构特点和研究状况、稀土配合物发光材料和多吡啶钌配合物光电性质研究进展进行了较详细的综述。

The fluorescence properties of complexes of europium with β-diketone and terbium with benzoic acid and its derivatives were analyzed and the synergic effect of the second ligand was illustrated from the energy matching of the minimum triplet state of ligands and the resonance energy level of rare earth ions.

提出了掺杂离子荧光增强效应的机理。 4。首次采用ab initio CIS方法，在劈裂价层基组3—21G水平上对各配体进行了量化计算，系统分析了前线分子轨道特征和激发态的能级，从配体最低激发三重态能级与稀土离子共振能级的能级匹配，分析了铕与β-二酮的配合物的荧光性能和铽与苯甲酸系列衍生物的配合物的荧光性能，解释了第二配体的协同效应。

The complexes of disk - like crown ether liquid crystal with Eu have theproperties of liquid crystals and havn't the properties of fluorescence. The complexes of disk -like crown ether liquid crystal with Eu and β-diketone have the properties of fluorescence and electroluminescence.

盘状冠醚液晶Eu配合物具有液晶性质而无荧光特性；盘状冠醚液晶与EuⅢ）和β-二酮形成的配合物具有荧光特性，和电致发光性质。

Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

I am coming just now,' and went on perfuming himself with Hunut, then he came and sat.

我来只是现在，'歼灭战perfuming自己与胡努特，那麼，他来到和SAT 。