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The calcination of the catalysts at high temperature may easily result in theformation of tetrahedral structure Mo species before sulfidation,and decrease theamount of octahedral coordination Mo species.The sinter and loss of the activecomponents would take place during the calcination at overhigh temperature. Meanwhile,the active component could react with support,thus made the activecomponents entered into support bulk phase.

7催化剂在硫化前进行高温烧,容易形成四面体结构的钼物种,而八面体配位钼物种减少,且过高的烧温度易使活性组分发生烧结,同时可能发生活性组分的流失或与载体发生反应进入载体体相。

Using the Esterificational Reaction and the Pentane Isomerization Reaction as probes, catalytic activity of these superacids which were prepared by different process conditions such as different concentration of H2SO4, immersing time.

研究了不同的H_2SO_4浓度,H_2SO_4浸泡时间,烧温度,烧时间,包覆次数制备的催化剂催化酯化反应及正戊烷异构化反应的活性,并将其结果和表征结果进行了关联。

With the co-precipitation, using cross experiment, constitute of catalyst (include 2 equations), proportionment of precipitator, aged time, calcine temperature, had been discussed-how to influence the activity of catalyst. The activity will be primed if prepareing the catalyst with CuO:ZnO:CeO_2=6:9:10, using NaOH as precipitator, aged time 3h, calcining the calatyst at 450℃.

在共沉淀法中利用正交试验对催化剂中各种物质的配比量、沉淀剂类型、陈化时间和烧温度这4种因素进行了4水平分析,结果显示制备催化剂时使用的金属盐Cu(NO_3)_2、Zn(NO_3)_2和Ce(NO_3)_3的物质的量之比符合n_1∶n_2∶n_3=6∶9∶10、并且NaOH溶液作沉淀剂、3h陈化后在450℃烧,制得的催化剂催化效果最好,在130℃时CO转化率即达到99%以上。

In this paper,the selective reduction roasting experimental study is chiefly introduced,in which coal is used as reductant.

研究确定了最佳工艺条件为:采用烟煤做还原剂,还原剂加入量为矿量的10%;粒度在0~3mm,-0.074mm含量约占25%;烧时间20~30min;烧温度700~750℃。

On the basis of the Tin reverberator smelting thermodynamics process computer simulation model,the research was taken in what influences the smelting temperature,tin tenor in roasted product and reduction coal ca- pacity would do to the distribution of the main elements or components just like Pb,Zn,C,O in the grossly tin,slag and gas phase.

利用已建立的锡反射炉熔炼热力学过程计算机模型,首次研究了熔炼温度、砂锡品位及还原煤量对Sn、Fe、Pb、Zn、C等元素或组分分别在粗锡、炉渣及炉气相中分配行为的影响。模拟结果表明,熔炼反应最佳温度为1500K,当到达这一温度后,再提高炉温对反应过程的优化并无明显贡献,提高入炉砂的锡品位及还原煤量均对提高粗锡品位及锡回收率有利

The results show that the optimum preparation conditions of CuO/AC catalyst are as follows:the concentration of Cu(NO3)2 is 3%,soakage temperature 30 ℃,soaking time 6 h,calcinating temperature 300 ℃,and calcinating time 3 h.

研究结果表明,硝酸铜-AC制备CuO/AC催化剂的最佳条件为:硝酸铜质量分数为3%,浸渍温度为30 ℃,浸渍时间为6 h,烧温度为300 ℃,烧时间为3 h。

The optimal processing conditions are as follows: roasting temperature at 1 000℃, roasting time for 40 min, the ratio of NbH dosage to theoretic dosage at 1.1. The specific capacity of niobium suboxide of preparation by agate grind procedure is 69.50 mF·V·g-1, the loss is 11.25%, the leakage current is 1.8×10-4A·F-1·V-1, and the electrical properties are better than that of the national standard (GB/T 3136-1995) of FTa16-300 tantalum powder for capacitor.

用正交试验法及方差分析对玛瑙研磨工艺进行优化,得到制备低价铌氧化物最佳条件是:烧温度为1 000℃,烧时间为40 min, NbH用量与理论量之比为1.1,所制得的产物杂质含量低,比容为69.50mF·V·g-1,损耗为11.25%,漏电流为1.8×10-4A·F-1·V-1,其电性能指标高于FTa16—300电容器钽粉国家标准(GB/T 3136—1995)所规定的值。

The TCC technology was successfully applied to two of 160kA prebake cells in Pingguo Aluminum Company. It was shown that no tear-off of TCC was indicated after starting up of the cells. The operation of coating cells was improved to keep good shape of cell chamber, reduce the formation of sludge on the cell bottom, and gain more uniform current distribution.

将TIB:阴极涂层技术在160kA大型预槽进行了应用,并考核了涂层槽的指标,结果显示,烧启动后,TIB:阴极涂层不脱落,涂层槽的工作状态良好,炉膛规整,炉底干净,电流分布均匀;与对比槽比较,阴极内衬对钠的吸收减少,钠渗透速率减缓,炉底压降降低(平均降低39mv),电流效率提高(平均提高0.41%);涂层的寿命为38个月。

The TCC was still good and in integrity after 12h of electrolysis. The TCC technology was successfully applied to two of 160kA prebake cells in Pingguo Aluminum Company. It was shown that no tear-off of TCC was indicated after starting up of the cells. The operation of coating cells was improved to keep good shape of cell chamber, reduce the formation of sludge on the cell bottom, and gain more uniform current distribution.

将TiB〓阴极涂层技术在160kA大型预槽进行了应用,并考核了涂层槽的指标,结果显示,烧启动后,TiB〓阴极涂层不脱落,涂层槽的工作状态良好,炉膛规整,炉底干净,电流分布均匀;与对比槽比较,阴极内衬对钠的吸收减少,钠渗透速率减缓,炉底压降降低(平均降低39mV),电流效率提高(平均提高0.41%);涂层的寿命为38个月。

By calculating theoretically and testing, Topgallant void ratio of gas grid was determined.At high temperature,the charge material was suspending in gas bed,experiments of different magnetizing roasting temperature and roasting duration have been run by leading to reductive atmosphere containing CO.

在高温条件下,通入含CO还原气体,使物料处于悬浮状态,进行了不同磁化烧温度及时间试验,查明在650℃~760℃,烧时间10~60秒内,可以使菱铁矿(FeCO_3)、赤铁矿(Fe_2O_3)快速转变为磁铁矿(Fe_3O_4)。

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