烯基

The method has been used to determine Phthalic esters in drinking water and seawater sample. 3. Single drop microextraction, followed by gas chromatography with flame ionization detection has been applied to determine Formaldehyde, Acetaldehyde and Acraldehyde in water based on 2,4-Dinitrophenylhydrazine derivatization. Extraction solvent, extraction time and stirrer speed were optimized. Optimal experimental conditions were as follows: 1.6μL toluene microdrop exposed for 30 min in a 3ml aqueous sample placed in 4ml vial and stirred at 600 rpm/min.

以2，4-二硝基苯肼衍生，单滴液相微萃取与气相色谱火焰光度检测器联用测定水样中的甲醛、乙醛、丙烯醛，考察了萃取溶剂、液滴大小、萃取时间、搅拌速度、盐效应等对该方法的影响，并对影响液相微萃取的各种因素进行了系统的阐述，确定了该体系的最佳实验条件，实现了甲醛、乙醛、丙烯醛的提取和富集。

Methacrylic acid-acraldehyde/ montmorillonite nanocomposites were prepared using Na+- montmorillonite via in-situ polymerization of methacrylic acid and acraldehyde in aqueous medium.

采用水溶性聚合单体甲基丙烯酸和丙烯醛在钠基蒙脱土层间直接原位插层聚合制备水溶性MAA-AL/MMT纳米复合材料，通过XRD和TEM对纳米复合材料的结构进行表征，采用TGA、DSC研究了纳米复合材料的热性能，同时考察了甲基丙烯酸与丙烯醛配比及体系pH值对纳米复合材料结构及应用性能的影响。

Anilido-imino nickel complex 1 {(C6H3Me2-2,6)N=CH-5-NO2-C6H3N (C6H3Me2-2,6)}NiBr was first synthesized, and its catalytic behavior toward polymerizations of norbornene and ethylene in the presense of methylaluminoxane were investigated in detail. The complex activated with methylaluminoxane exhibited high activities for norbornene polymerization.

首次合成了苯胺基亚胺镍配合物1{(C6H3Me2-2，6)N=CH-5-NO2-C6H3N(C6H3Me2-2，6)}NiBr，研究了其在助催化剂甲基铝氧烷的作用下对降冰片烯、乙烯的均聚以及对降冰片烯和乙烯的共聚的催化性能。

As we know, the algebraic sum of Hammett constants for thesubstituted donor and acceptor groups can be used to characterize the asymmetryin simple π-organic systems, to correlate the variation of NLO properties.

推拉多烯对取代基比较敏感，易于观察到结构上的变化，是一种很好的研究对象，对推拉多烯的量化计算研究可以给我们提供分子结构和非线性光学等性能之间的关系。

Allyl glycidyl ether was synthesized from allyl alcohol and epichlorohydrin by phase transfer catalysis.

以烯丙醇和环氧氯丙烷为原料，采用相转移催化法，合成了烯丙基缩水甘油醚。

At first,the intermediate of sodium 3-chloro-2-hydroxy propanesulfate was synthesized from epichlorohydrin and sodium bisulfite;And then,using NaOH as a catalyst,the title compound has been synthesized from intermediate and allyl alcohol to reach the yield of about 70%.

先由环氧氯丙烷和亚硫酸氢钠合成中间体3-氯-2-羟基丙磺酸钠，然后中间体再与丙烯醇在氢氧化钠催化下生成目标产物2-羟基-3-烯丙氧基丙磺酸钠。

The yield of allyl glycidyl ether can reach up to 96% at 30 ℃ for 3 h at a molar ratio of 1 to 1.5 of sodium allylate to epichlorohydrin.

醚化反应中固体烯丙醇钠与环氧氯丙烷摩尔比为1：1.5，在无水条件下于30℃反应3 h，烯丙基缩水甘油醚的收率达96%以上。

For most of the enones and allylic alcohols, the reaction could be completed within several hours with good yields.

反应无需有机溶剂，对于大部分的烯酮和烯丙基醇反应可以在数小时内完成，产率良好。

These substituents are either small groups such as phenoxy groups,aryls,cyclic secondary amines,cyano groups,and halogens or large functional moieties such as PDI,Phthalocyanines, porphyrins,BODIPY,cyclodextrin,Fullerene,calixarene,and so on.

这在过去的工作中，人们把一些小分子的，如酚氧基、仲胺基、苯基、氰基以及卤素氟、氯、引入到PDI中，同时也把一些较大功能团，如PDI本身、卟啉、酞菁、环糊精、BODIPY、杯芳烃、富勒烯等和PDI连接在一起。

UV-curable hyperbranched poly was synthesized via organosilicon polymer bearing silicon hydride end groups and vinyltriallylsilane at the presence of Pt/C catalyst.

通过含硅氢键的超支化聚合物和乙烯基三烯丙基硅烷在铂催化剂作用下反应制备了可紫外光固化的超支化聚硅氧基硅烷。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。