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The constituents were extracted by some solvents. 18 constituents were isolated from Chloroform fraction by different chromatography. 15 constituents were identified by IR ,MS and NMR as follows: 3-sitosterol, P-sitosterylpalm itate,succinate acids, 1, 4-benzenediol, 1, 2-benzenediol, p-hydroxybenzaldehyde, syringaresinol, oleanolic acid, usolic acid, ethyl caffeate , Rosmarinic acid ethylster and etc. In such constituents ,nine compounds were isolated for first time from Origanum vulgare L..

牛至药材经水煮醇沉法所得浸膏,利用溶剂法和色谱法从中分离得到18个单体成分,通过IR、MS、NMR等波谱技术鉴定了其中的15个化合物,分别为β-谷甾醇(1)、β-胡萝卜苷(2)、琥珀酸(3)、对-二苯酚(4)、邻-二苯酚(5)、对羟基苯甲醛(6)、1.2-二羟基-4-异丙基-5-甲基苯(7)、新木脂素(8)、丁香脂素(9)、齐墩果酸(10)、乌苏酸(11)、4-二十六烯(12)、正二十六醇(13)、咖啡酸乙酯(14)、迷迭香酸乙酯(15)等,其中化合物3、4、5、6、7、8、9、14、15等9种化合物均为首次从该属植物中分离得到。

To observe effect of receptor ligand on subcelluar distribution of liposome was found that alprenolol liposomes was increased in mitochondria and sarcolemma,especially in nuclei(8 fold increased), as compared with blank liposome.

观察受体配基对脂质体在心肌亚细胞器中分布的影响,结果发现,烯丙洛尔掺入脂质体,使脂质体在细胞核、线粒体和肌膜的分布增加,尤其在细胞核增加最明显,较空白脂质体增多了8倍。

Polygonatum odoratum Agglutinin from Amaryllidaceae species is a mannose-binding protein with various biological activities.

丙烯酰胺对PML中Trp淬灭程度达到83%,KI能淬灭PML分子中49%的Trp残基的荧光。

The detailed mechanisms of the electron transfer reactions of common coenzyme NADH model compounds were systematically investigated using o-allyloxy benzenediazonium salt as the probe.

应用邻位烯丙氧基取代的芳基重氮盐作为探针,对辅酶NADH几种最常用的模型化合物电子转移反应的过程和机理进行了比较系统的考察。

In the final step of the synthetic pathway leading to cabergoline, an allylic acid intermediate of Formula is reacted with N-(3-dimethylaminopropyl)-N-ethyl carbodiimide to produce cabergoline, i.e.

在卡麦角林合成路径的最后一步,分子式中的一个烯丙酸基中间体同碳二亚胺耦联剂反应生成卡麦角林,如

Hydrogels based on n -alkyl methacrylate esters,acrylic acid and acrylamide cross-linked with 4,4′-diazobenzene were preparared.

合成了带不同疏水侧基的甲基丙烯酸酯、甲基丙烯酰胺及丙烯酸与 4,4′二偶氮苯交联共聚的凝胶。

The coating composition comprises, in a specific proportion, a vehicle ingredient comprising in a specific proportion an oligomer having at least twoacrylate groups and an ethylenic monomer copolymerizable with the oligomer, aacrylic-modified chlorinated polyolefin having a specific chlorine content, an organic peroxide polymerization initiator, and a polyisocyanate compound.

该涂料组合物含有特定比例的由至少具有两个丙烯酸酯基的低聚物和可与该低聚物共聚的乙烯性不饱和单体形成的媒介物成分、特定氯含率的丙烯酰基改性氯化聚烯烃、有机过氧化物聚合引发剂、和聚异氰酸酯化合物。

A reversed-phase high performance liquid chromatographic method was established for determination of isothiocyanates in human urine , which used the reaction of propyl isothiocyanate with 1,2-benzenedithiol as reference instead of the synthesis of 1,3-benzodithiole-2-thione.

省去合成1,3 苯二硫杂环五烯 2 硫酮这一步骤,直接用异硫氰酸丙基酯与1,2 苯二硫酚反应作标准,建立了尿液中异硫氰酸酯的反相高效液相色谱测定方法。

The new olefination methods of alkyl substituted propargylic dithioacetals are described in this thesis.

中文摘要本篇论文围绕在烷基取代炔丙基硫缩醛的新型态烯化反应,可分为两部分进行探讨。

Aiming at the shortcomings of high formaldehyde content and low soaping and crocking fastnesses of currently used pigment printing binder,by60Co-γ radiation polymerization process,the waterborne polyacrylate emulsion containing active keto groups was synthesized from acrylate monomers and diacetone acrylamide.

针对目前所用涂料印花黏合剂存在的色牢度低和甲醛含量高的缺陷,采用钴60-γ辐射法聚合工艺,利用丙烯酸酯单体、双丙酮丙烯酰胺合成出含活性酮羰基的丙烯酸酯乳液;然后同含端酰肼基聚氨酯乳液按一定的比例混合,制备出酮肼交联型丙烯酸酯聚氨酯复合乳液。

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