烯

These novel reagents were treated with base to produce polystyrene-supported a-seleno carbanions, which reacted with alkyl halides, followed by stereospecific selenoxide syn-elimination to give 2i-vinylphosphonates and is-vinylsulfones respectively.

它们在碱的作用下形成α—硒基碳负离子，然后与卤代烃发生烷基化反应，烷基化后的树脂可以通过温和条件下的氧化消除以良好产率和较高纯度分别合成了烯基磷酸酯和烯基砜。

This novel reagent was treated with LDA to produce polystyrene-supported a-seleno carbanions, which reacted with alkyl halides and epoxides, followed by stereospecific selenoxide syn-elimination to give olefins and allylic alcohols respectively.

它与LDA反应形成α—硒基稳定的碳负离子，再与卤代烃或环氧化合物发生α—烷基化反应，烷基化后的树脂可以在30%的双氧水中进行氧化-消除，以良好产率和较高纯度合成了取代烯烃或烯丙基醇。

A new monomer,4-hexanoxyl-4′-undecylene-[10]-acyloxyazobenzene was synthesized using the main materials:phenol,underlenic acid,1-bromo- n -hexane, p -nitrophenol,thionyl chloride,by the substitution,reduction,couping and diazotization methods.A new polymer was prepared by hydrosilation reaction of poly (methylhy-drosiloxane) with the monomer.

以苯酚、十一烯酸、正溴己烷、对硝基苯酚和二氯亚砜为主要原料，通过取代、还原、重氮化和偶合等反应，合成了一种新的液晶单体 4-己氧基-4′-十一烯-[10]-酰氧基偶氮苯，并与聚通过硅氢加成生成一种新的高分子液晶。

Zinc diamyl dithiocarbamate antioxidant showed good synergism with antimony diakyl dithiocarbamate antiwear additive in improving the oxidation stability of modified soybean oils. The incipient oxidation temperature and induction period time of genetically modified soybean oils were improved significantly by adding polyalphaolefin and additives, and they were even better than that of the synthetic base oil PAO with the same additive formulation.

结果表明，改性大豆油的不饱和脂肪酸含量越高，其氧化安定性越差；抗氧剂二戊基二硫代氨基甲酸锌和抗磨剂二烷基二硫代氨基甲酸锑在改性大豆油中均表现出了良好的抗氧协同性能，尤其在基因改性大豆油中，聚-α-烯烃和添加剂的复配使其起始氧化温度和氧化诱导时间均超过了相同配方的聚-α-烯烃油样。

The influence factors such as amount of catalyst,molar ratio of maleic anhydride to n-butanol,and reaction time on the yield of dibutyl maleate were discussed.

以La2(SO4)3/SiO2为催化剂，顺丁烯二酸酐和丁醇为原料，合成内增塑剂顺丁烯二酸二丁酯，探讨了催化剂用量，酐醇物质的量比以及反应时间等对收率的影响。

The C2 to C5 and heavier acetylenes and dienes in a thermally cracked feed stream are hydrogenated without significantly hydrogenating the C2 and C3 olefins.

使经过热裂解的进料物流中的C2－C5及更重的炔烃和二烯烃加氢，而不使C2和C3烯烃发生显著的加氢。

This makes Ni-W-P powder more suitable for partial hydrogenation of dienes. The kinetic results suggest there are some different between the active sites of Ni-P and Ni-W-P powder. DSC, XRD and EXAFS results suggest that the tungsten codeposition makes Ni-W-P powder more amorphous than Ni-P powder.

动力学结果表明在两种合金微粒上，不仅环戊二烯与环戊烯的相对配位能力不同，而且它们各自的反应速率常数也不一样，表明非晶态Ni-P、Ni-W-P合金微粒的催化活性中心存在着一定的差异。

Phytochemical investigation on the acetone extract of the stems of K.oblongifolia led to the isolation of 49 compounds and 31 of them were identified.They were 20 lignans,(including 11 dibenzocyclooctadienes,8 spirobenzofuranoid dibenzocycloocta -dienes,1 other lignan),9 flavones,and 1 nortriterpenoid.Among them,4 were new compounds,1 was new natural products,and 8 compounds were isolated from this family for the first time.

通过对冷饭藤的藤茎化学成分的研究，从丙酮提取物中分离得到49个化合物，鉴定了31个化合物，包括木脂素类化合物20个(联苯环辛烯类木脂素11个，螺苯骈联苯环辛烯类木脂素8个，其他类型木脂素1个)，黄酮类化合物9个，降三萜类化合物1个，其中。4个为新化合物，1个新的天然产物，8个为本科首次报道。

The technological scheme is that under the conditions one reaction temperature 40-200 deg.c, reaction pressure from normal pressure to 6.0 MPa and reaction velocity of 0.5-3/hr, C4 mixture as the main material is made to contact with catalyst to produce isooctene. The production process may be used in industrial production of selective C4 mixture dimerizing process to prepare isooctene.

本发明通过采用以混合碳四为原料，在反应温度为40～200℃，反应压力为常压～6.0MPa，反应液体体积空速为0.5～3小时-1条件下，反应原料与催化剂接触生成异辛烯的该技术方案较好地解决了上述问题，可用于混合碳四选择性二聚制异辛烯的工业生产中。

Anion exchange resin was not suitable for the separation as stationary phase due to the strong adsorption toward catechol.The chemicals of eluates were measured by UV and IR.Terpene-catechol resin can be used for preparing copolymeric coating from terpene-catechol resin with raw lacquer.

通过对洗脱液进行紫外光谱分析，表明用中性氧化铝作固定相，分别用汽油、乙醇和NaOH-乙醇溶液洗脱，能较好地分离萜烯树脂和萜烯-邻苯二酚树脂。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新