烯

A method has been developed to determine residual stilbenes such as diethylstilbestrol, dienestrol and hexestrol in animal tissues using solid phase extraction and gas chromatography-mass spectrometry.

建立了动物组织中己烯雌酚、己二烯雌酚和己烷雌酚残留量的气相色谱-质谱分析方法。

In this paper, initiator is dissolved in 1-bromopropane which is solvent. Then the propene and hydrogen bromide that can be dissolved in 1-bromopropane are inlet in l-bromopropane when initiator is decomposing. The reaction occurs in fluid phase and high-purity 1-bromopropane is synthesized by one step method. In this paper, the material HBr is synthesized with NaBr and sulfuric acid at the presence of hydrobromic acid.

本论文以1-溴丙烷为溶剂，将引发剂溶于其中，加热到引发剂开始分解时再通入丙烯和HBr，使二者溶解于1-溴丙烷中，在液相中进行反应，实现丙烯&一步法&合成高纯1-溴丙烷利用NaBr与硫酸在氢溴酸存在下反应制备HBr气体，以作为合成1-溴丙烷的原料。

Firstly, Copolymerization of acrylamide and styrene was carried out in a microemulsion system, in which AM aqueous solution was the continue phase and St was the dispersed phase using ST-80 as surfactants respectively, then hydroxamic functions were prepared with hydroxylamine salt at temperatures of from 60℃ to 90℃.

首先以丙烯酰胺水溶液为连续相，以苯乙烯为分散相，ST-80为乳化剂制成微乳液，在15℃~35℃合成丙烯酰胺与苯乙烯的共聚物；然后采用程序控温方式，在60℃~90℃用硫酸羟胺将共聚物羟肟化合成了一种带有苯环结构的嵌段型氧肟酸类聚合物材料。

At 15-35℃, copolymerization of acrylamide and styene was carried out in a microemulsion system, in which AM aqueous solution was the continuous phase and St was the dispersed phase using ST-80 as surfactants, respectively. Hydroxamic functions were prepared with hydroxylamine salt at temperatures from 60℃ to 90℃.

以丙烯酰胺水溶液为连续相，苯乙烯为分散相，ST-80为乳化剂制成微乳液，在15~35℃下合成丙烯酰胺与苯乙烯的共聚物，采用程序控温方式，在60~90℃下使用硫酸羟胺将共聚物羟肟化得到产物。

In the synthesis of canthaxanthin by selective catalylitic oxidating of βcarotene,CO2 was used as acidifying or alkalizing agent,which controlled reacting system acidity and protected polyene.,producing less by-products and increasing catalylitic oxidation selectivity.In the addition reaction of isoprene with hypochloric acid,1-chloro-2-methyl-3-buten-2-ol and l-chloro-2-methyl-3-buten-4-ol were made by controlling of the acidity with carbon dioxide i...

CO2作为酸碱调节剂和惰性气体，在β-胡萝卜素催化氧化合成角黄素反应中，可以控制反应体系酸性，保护原料中的双键，减少副反应发生，提高催化氧化反应的选择性；异戊二烯氯醇化生成1-氯-2-甲基-3-丁烯-2-醇和1-氯-2-甲基-3-丁唏-4-醇反应中，CO2代替有机酸作酸碱调节剂，控制次氯酸的生成速度，达到调控反应的目的，反应条件温和，不副产固体。

In addition, ioding was found to be an efficient catalyst for the imino Diels-Alder reaction of N-arylimine and enol ethers and the reaction provided tertrahydroqinolines in good yields. One pot synthesis of tetrahydroqinolines from aldehyde, aniline and enol ethers was also achieved using iodine as the catalyst. The chemical yield of the"one pot"reaction was comparable with that obtained using preformed N-arylimine.

此外我们也发现碘能够有效地催化N-芳基亚胺与烯醇醚的Diels-Alder反应，以很高的化学收率得到了四氢喹啉衍生物，并且发现碘也能够直接催化芳香醛、苯胺、烯醇醚的三组分&一锅&反应，获得的化学产率与使用预制的N-芳基亚胺相当。

The palladium-catalyzed heteroannulations of C_(60) with a variety ofο-iodoanilines afforded the first synthesis of C_(60)-fused indoline derivatives.

通过在Pd的催化下，富勒烯和邻碘苯胺类化合物的杂环化反应，首次合成了一系列富勒烯并吲哚啉环衍生物。

The present invention relates to an ethylene/alpha-olefin interpolymer product comprising at least one alpha-olefin interpolymerized with ethylene and, characterized in at least one aspect, as having improved properties when utilized in a hot melt adhesive formulation.

本发明涉及包括至少一种与乙烯互聚的α-烯烃的乙烯/α-烯烃共聚体产物，其特征为在至少一方面，当用于热熔粘合剂配制剂时具有改进的性能。

Methods Twenty-four Sprague-Dawley rats were randomly divided into 4 groups (n=6):① control group (inhaled 0.9% normal saline for 3 hours, twice every day);② enalapril self-control group 〔intragastrically administrated enalapril 0.5 mg/only〕;③ model group (stimulated with 4 mg/L acrolein for 3 hours, twice every day);④ enalapril interventive group 〔inhaled acrolein and intragastrically administrated enalapril 0.5 mg/〕.

健康雄性SD大鼠24只，随机分为4组，每组6只。A组：空白对照组；B组：依拉普利自身对照组，依拉普利0.5mg/灌胃；C组：模型组，大鼠吸入4mg/L丙烯醛，每次3h，每天两次；D组：依拉普利干预组（吸入丙烯醛＋依拉普利灌胃），处理同模型组，并给予依拉普利0.5mg/灌胃。21d后处死大鼠，采集标本。

16 And 19 components are identified from three specimens,which accounted for 99.63%, 99.70% and 99.28% of volatile fraction, respectively. The major components are pulegone and menthone, which accounted for 89.02%, 83.51%and 87.11%(Horm rural Buerjin county of Xinjiang). Others are isomenthone, piperitenone,isopulegone and limonene et al.Key words Ziziphora clinopodioides Lam. essential oil gas chromatography-mass spectrometry

从3个样本中分别鉴定出10种、16种和19种挥发油成分，占各自挥发油总量的99.62%、99.71%和99.28%。3个采集地的芳香新塔花的主要成分相同，均为长叶薄荷酮和薄荷酮，两者总量分别达到了89.02%、83.51%和87.11%（新疆布尔津县禾木乡样品），其他主要成分为异薄荷酮、胡椒烯酮、异长叶薄荷酮、柠檬烯等。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐