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The preparation method comprises monomer synthesis and polymer synthesis. The polymer synthesis is that cyclopentadienyl sodium monomer is added into metallic cobalt complex-triphenyl phosphorus cobalt chloride under strict oxygen-free and water-free conditions, and then double inner alkyne or outer alkyne conjugate monomer is added in, and after reaction, the precipitation, filtering, abstersion and vacuum-drying are carried out, the large molecules polymer containing cyclopentadienyl cobaltocenium organometallic cobalt is obtained.

制备方法,包括单体合成和聚合物的合成,聚合物的合成是在严格无氧无水条件下,在金属钴配合物三-三苯基磷氯化钴,加入环戊二钠单体,随后加入双内炔或双外炔共轭单体,反应后沉淀,过滤,洗涤,真空干燥,得到含环戊二茂钴有机金属钴的大分子聚合物。

In comparison with acetyl acetate method we found that in the reaction process the concentration of enol-like compound had some effect on the reaction rate.

通过与乙酰丙酮法的比较,认为在反应过程中,成环物质的醇型的化合物含量对反应速度有影响,醇型的化合物含量越高,反应温度越低。

Premise Liquefied petroleum gas is derived from oil gas, natural gas, the gas production of refinery and petrochemicals. The main components are dimethylmethane, propylene, butane, butylene and such low class hydrocarbon. It's a gas with achromaticity and transparence; LPG is hardly dissolved in water, but dissolved in ethanol and aether, it can dissolve gas production, propagation oil and caoutchouc.

液化石油气(liquefied petroleum gas,LPG)是石油伴生气、天然气、炼油厂及石油化工厂的气体产品,经分离精制而来,其主要成分为丙烷、丙、丁烷、丁等低分子烃;无色透明,带有微弱的臭味;难溶于水,溶于乙醇和乙醚等,并能溶解石油产品,动植物油和天然橡胶。

The production methods of glutaraldehyde,including those of addition reaction of acraldehyde , oxidation of 1,5-pentadiol,reduction of glutaryl chloride and oxidation of cyclopentene,are summarized.

综述了丙醛加成、 1,5 -戊二醇氧化、戊二酰氯还原和环戊氧化等戊二醛的合成路线和制备方法,考察了目前戊二醛的生产厂家及其在皮革鞣剂、油田注水杀菌剂和医药杀菌等领域的应用市

The main contamination in dining-room is acraldehyde.

学生食堂内主要污染物是丙醛,因此在学生食堂内对丙醛的浓度进行了检测。

Tetraallylsilane was synthesized by one-step approach through the reaction of silicon tetrachloride with the partially solvated Grignard reagents formed in situ from allyl bromide and magnesium in the mixed solvents of toluene and ether.

采用一步合成方式,将3-溴丙与金属镁在以甲苯和供电子溶剂构成的混合溶剂中进行反应,继而与四氯化硅反应,成功合成了四丙基硅烷,其产率在乙醚与3-溴丙的摩尔比为4(V甲苯/V乙醚=1·1)时达到极值,超过了91%。

When the reaction was finished, the ligand was extracted with CH2Cl2 and precipitated upon addition of diethyl ether followed by filtration.

2配体2在丙酮/水体系中催化/又种烃的AD反应,非链端烃的立体选择性(80一99%ee)明显优于链端烃(51一62%ee)。

The results of IR and DSC indicated that the curing reaction of BMI-modified phenolic resin mainly consists of two steps: the allyl groups in the Novolak resin react with maleimide group via"Ene"addition, and addition reactions of the C=C bonds formed thereby are followed.

IR与DSC方法研究表明:BMI改性酚醛树脂的固化反应主要是Novolak树脂上的丙基首先与酰亚胺基团的加成反应,然后加成反应所形成的C=C双键发生进一步加成。

Synthesis of tricyclopentadiene Two methods of polymerization were analyzed in the synthesis of TCPD: thermal polymerization of DCPD, Diels-Alder reaction of DCPD and cyclopentadiene.

三环戊二的合成采用两种方式对TCPD的合成进行了研究:DCPD直接热聚法、DCPD与环戊二加成法。

This dissertation is concerned with the approaches to a new high density liquid fuel, tetrahydrotricyclopentadiene, which can be synthesized with dicyclopentadiene as raw materials by three steps: Diels-Alder reaction, separation and hydrogenation. The main points of the paper are listed as follows.

本文以双环戊二为原料,通过双加成、分离、加氢反应得到目的产物——新型高密度液体燃料四氢三环戊二,主要研究内容包括: 1。

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The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意,我建议我们在价格上大家各让一半。

After an hour and no pup, look for continued contractions and arching of the back with no pup as a sign of trouble.

一个小时后,并没有任何的PUP ,寻找继续收缩和拱的背面没有任何的PUP作为一个注册的麻烦。