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热量测定

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The combustion heat of three alkane homologue s were measured in the oxygen bomb calorimeter in this paper.

采用氧弹热量计测定了几种同系物的燃烧热值,并分析了烷烃同系物的燃烧热随碳链的增长的变化规

The heat capacity Cp of EDTA solution used as activator in the Buna- S manufac-ture was measured by using a precision automated adiabatic calorimeter in the temperaturerange of 278K to 324K as fundamental data for the construction of large compositive appara-tus.

丁苯橡胶合成用活化剂乙二胺四乙酸盐溶液比热容的测定赵小明,刘志刚,陈钟颀(西安交通大学热工教研室西安710049)关键词EDTA溶液,比热容,绝热量热法比热容是物质重要参数,与物质结构密切相关。

The sample was measured with the DSC method and compared with the calorimetric method.

采用DSC法对试样进行了测定,并与绝热量热法进行了比较。

The standard molar special heat capacity of 1,1-diamino-2,2-dinitroethylene (FOX-7) was determined with two continuous Cp modes of a mircocalorimeter to be 176.56 and 176.02 J·mol-1·K-1 at 298.15 K, respectively.

应用Micro-DSCⅢ微热量仪的两种连续比热容测定模式对1,1-二氨基-2,2-二硝基乙烯(FOX-7)比热容进行了测定。

The photosynthesis is determined by photosynthesis meterThe results showed that the net photosynthesis rate of Carex lasiocarpa(47.41 μ mol/m/s)is faster than those of other plants in Carex lasiocarpa wetland, Based on the overall sunlight radiation and the efficient photosynthesis radiation, energy utilization rate in radicula was the highest(1.3945% and 3.1879%)While those in spike was the lowest(0.0020% and 0.0046%).

毛果苔草湿地的物理过程观测设在中国科学院三江平原沼泽湿地生态实验站内,用美国CID公司出品的光合仪对典型湿地中几种优势植物的光合能力进行测定;在80℃干燥的植物样品,粉碎后,分别称量约1g左右,用美国公司Parr型氧弹式热量计测定;研究发现毛果苔草湿地建群种中毛果苔草的净光合速率最大,为47.41μmol/m/s。

The power-time curves of E.coli reacting with Co-SG at different temperature has been determined by microcalorimtric method The multiplication rate constant k, generation time G,bacterial growth inhibition ratio I,total thermogenetic quantity Q, the heat quantity of a single bacterium Q_(0) and the heat quantity of a single bacterium per minute have also been calculated according to the power-time curves.

用微量热法测定了大肠杆菌及其在Co -SG配合物作用下的热谱曲线,计算了速率常数k ,传代时间G、抑制I、总产热量Q、单个细菌的产热量Q0 和每分钟单个细菌的产热量 Q0 ,建立了部分代谢参数之间的关系,探讨了大肠杆菌在不同温度和Co -SG作用下的代谢抑制,发现可用t、tr、tg和 Q0 定量表征在不同温度下大肠杆菌的生长代谢和药物的抗菌活性。

The research on the energy needs of the canines is often a research of the basic metabolizing rate.

对于犬的能量需要研究一般是研究基础代谢率,近年来研究能量需要较多,比如热量测定法或保持体重恒定法。

The computer oxygen bomb calorimeter is designed as per the requirements in national standard of PRC GB/T213 Measurement Method of Calorific Value of Coal, GB/T384 Determination of Calorific Value of Petroleum Products and JJG672 Oxygen Bomb Calorimeter.

用途微机氧弹热量计是依据中华人民共和国国家标准GB/T213《煤的发热量测定方法》、GB/T384《石油产品热值测定法》和中华人民共和国国家计量检定规程JJG672《氧弹热量计》的要求设计。

The compositions of complexes were determined as, by chemical and elemental analyses, Mn2CI2, Mn2Cl2, Cu2Cl2-2H2O, Cu(NO3)2-H2O, Cu(CH3COO)2, Zn2Cl2, Zn2(NO3)2-4H2O,ZnSO4 and Zn4(NO3)2, respectively. These complexes were characterized by IR,'H NMR and XPS. The crystal structures of these complexes were determined by single crystal X-ray diffraction techniques. The thermstability of the complexes was investigated by TG-DTG and the processes of their thermal decomposition were speculated. The constant-volume combustion energies of complexes, cU, were determined by a precision rotating bomb calorimeter at 298.15 K. Their standard enthalpies of formation, Hm, were calculated respectively. Finally, their biological activity was researched after the bactericidal activity was determined by selection of 1-2 bacteria.

通过化学分析、元素分析确定化合物分子组成分别为Mn_2Cl_2,Mn_2Cl_2,Cu_2Cl_2·2H_2O,Cu(NO_3)_2·H_2O,Cu(CH_3COO)_2,Zn_2Cl_2,Zn_2(NO_3)_2·4H_2O,ZnSO_4和Zn_4(NO_3)_2;借助IR、~1H NMR和XPS对化合物的键型特征进行了表征,运用X-射线单晶衍射分析法测定了个别化合物的晶体结构;以TG-DTG技术研究了化合物的热稳定性,阐明了它们的热分解机理;用精密转动弹热量计测定了化合物在298.15 K的恒容燃烧能,并计算了它们的标准燃烧焓和标准生成焓;选取1~2种病菌,初步测定了化合物的杀菌活性,进而研究了它们的生物活性。

In this study, we used poly L-latcide, poly DL-latcide-co-glycolide 75:25 (PLGA7525) and poly DL-latcide-co-glycolide 50:50 (PLGA5050) during citric acid inducing ammonium bicarbonate gas forming process to form porous polymer film, and rolled the porous polymer film to make nerve conduits with pores and multi-layered. Electron Spectroscopy for Chemical Analyzer and Attenuated Total Reflectance – Fourier-Transform Infrared Spectrometer were employed for determining elements' functionabilities and chemical compounds. Charge Coupled Device camera and Scanning Electron Microscope were employed for macroscopic and microscopic morphologies and structural observation. Differential Scanning Calorimetry was employed for measuring glass-transition temperature. Nano-indentation system was employed for measuring elastic modulus and hardness. Biodegradation and water absorption ratios were measured to analyze their chemical properties and SEM was employed for microscopic morphology of the tested nerve conduit.

本研究将以聚乳酸、聚乳酸-聚甘醇酸共聚合物(75:25)、聚乳酸-聚甘醇酸共聚合物(50:50)做为研究材料,以柠檬酸诱发碳酸氢铵发泡之气泡成型法制作具有相连通孔隙之高分子薄膜,再将高分子薄膜卷制成特殊多层的导管,制作具有多层孔隙之新型神经再生导管,以电子能谱化学分析及减弱式全反射-傅立叶转换红外线光谱分析进行成份分析及化学元素测定;以电荷耦合元件摄影机、扫瞄式电子显微镜进行多层孔隙型神经导管巨观及微观形态结构观察;以示差扫瞄热量量测分析玻璃转换温度、奈米三维量测弹性模数及硬度;以及进行降解性质测定,并以扫瞄式电子显微镜进行降解后之导管微观结构形态观察。

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