热化

The deuterium thermal desorption behavior of titanium deuteride with or without anodic oxide layer on the surface in a constant volume system has been investigated in the temperature range of 600℃ to 800℃.

应用反应速率分析方法，测定了氘化钛和表面有阳极氧化层的氘化钛在恒容体系和600-800℃范围内的热解吸反应速率常数，得到氘化钛和阳极氧化的氘化钛热解吸氘的活化能分别为24。

P-t curves of titanium hydride and titanium deuteride desorbing hydrogen and deuterium are investigated at 350～550 ℃ by using the method of reaction rate analysis in a constant volume system.

在高真空金属系统上测定了氢化钛和氘化钛在恒容体系中、350~550℃温度下热解吸氢和氘的P-t曲线；应用反应速率分析方法计算了各自在不同温度下的反应速率常数，得到氢化钛和氘化钛热解吸的表观活化能分别为27。

According to actual condition, a model of wall thickness of rotary kiln is established. The constant coefficients in the model, including thermal conductivity, heat transfer coefficient, Fourier coefficient and contact resistance, are closely calculated. A formula of contact resistance is draw from a great deal of data of surface and inner temperature of rotary kiln. The wall thickness of rotary kiln is simulated by MATLAB. The simulation result is transmitted from MATLAB to DELPHI through a group of interface functions compiled by VC++. The basic graphs-circle and line are analyzed by the means of the technique of Visualization in Scientific Computing and the Bresenham arithmetic, and are realized the visualization of the wall thickness. The contents of communication between master computer and slaver computer are designed and the error control technique, the idea of multi-thread and the embedded assembly language are applied to realize the temperature data transmission and graph transmission, which largely improved the speed of transmission and the reliability and stability of system.

建立了符合现场实际的回转窑壁厚数学模型；结合现场采用红外测温仪测量所得的温度数据和回转窑的实际结构数据，确定出适合该模型的定常系数(包括导热系数、换热系数、傅立叶系数、接触热阻等)，并得出与回转窑工况的相近的接触热阻公式ln=T~(0.5154)-36.7868；利用MATLAB软件仿真出回转窑壁厚，并将运算结果通过在VC++的编译环境下编译出MATLAB和DELPHI的接口函数传输到该监测系统中，实现了温度数据的转换和交换；运用科学计算可视化技术和Bresenham扫描转换算法对基本图形——圆和直线进行分析，从而实现了仿真后的壁厚数据可视化；在研究异步串行通信方式的基础上，设计了该系统上下位机功能和通信内容，并运用差错控制技术、多线程思想以及嵌入式汇编语言实现了温度数据和图形数据在上下位机之间的远程传输，提高了数据传输的速率和系统的可靠性、稳定性。

The experiment acquired pressure distribution and circulating rate under three fluidizing velocity (3.5m/s、4.5m/s、5.5m/s) and different media load. An experimental equation was acquired between circulating rate and the distribution of the pressure. And the relation between the circulating rate and the opening rate of the valve connecting the returner and the EHE was carefully discussed as well as the relation between the pressure of the EHE and the flow rate of the fluidizing air.

得到三种流化风速下（3.5m/s、4.5m/s、5.5m/s）不同装料量所对应的主床床体压力分布和物料循环量，得到循环量与压力的分布和流化风速的本实验台上的经验公式，并通过测量返料器通向外置换热器机械阀开度和返料量的关系，得到旋风分离器中下落物料进入换热器和直接进入主床的比例关系，同时测得换热器中压力和送风量的关系。

The ore-near hydrothermal alteration rocks in Pangushan tungsten deposit s incluted;silicification,greisenization muscovization,phyllitealteration,sericitization,biotization,chloritization, carbonatization and so on.

盘古山钨矿床的近矿热液蚀变作用包括硅化、云英岩化、白云母化、绢英岩化、绢云母化、黑云母化、绿泥石化和碳酸盐化等，与钨矿化关系密切的蚀变作用是云英岩化和白云母化，其次是硅化、绢英岩化和黑云母化。

Heat flux increases remarkably in spring, so layering comes into being gradually and concentrates on the central BS where tidal mixing is weak; whether the range or intensity culminates during the Summer Solstice; stratification is weakened in accompany with the decrease of heat flux in the fall, and is still apparent in BS strait; the gale enhances vertical stirring of sea water, so no obvious stratification exists in winter.

春天海表热通量显著增强，层化结构也开始形成，主要分布在潮汐混合较弱的中央水域；夏至时节层化结构无论是发生范围还是层化强度都达到极致；进入秋季，层化强度伴随着海表热通量的减少而削弱，分布区域也逐步向渤海海峡转移；冬季大风进一步增强了海水的垂向混合，此时渤海不再有垂向分层。

An antibody binding to IGF-IR and inhibiting the binding of IGF-I and IGF-II to IGF-IR which is characterized in that said antibody is a is ofIgG1 isotype, b shows a ratio of IC50 values of inhibition of the binding of IGF-I to IGF-IR to the inhibition of binding of IG-II to IGF-IR of 1:3 to 3:1, c inhibits for at least 80% at a concentration of 5 nM IGF-IR phospohrylation in a cellular phosphorylation assay using 3T3 cells providing 400,000 to 600,000 molecules IGF-IR per cell in a medium containing 0.5% heat inactivated fetal calf serum when compared to such an assay without said antibody, and d shows no IGF-IR stimulating activity measured as IGF-IR phophorylation at a concentration of 10 M in a cellular phosphorylation assay using 3T3 providing 400,000 to 600,000 molecules IGF-IR per cell in a medium containing 0,5% heat inactivated fetal calf serum when compared to such an assay without said antibody has improved properties in antitumor therapy.

一种已经提高了抗肿瘤治疗的特性的抗体，所述抗体结合IGF-IR并且抑制IGF-I和IGF-II与IGF-IR结合，其特征在于所述抗体a是IgG1同种型，b显示其对IGF-I与IGF-IR结合的抑制的IC 50 值与其对IGF-II与IGF-IR结合的抑制的IC 50 值的比率为1∶3-3∶1，c当与没有所述抗体的这种测定比较时，其在5nM的浓度上，在包含0.5％的热灭活胎牛血清的培养基中，使用3T3细胞的细胞磷酸化测定中，抑制至少80％的IGF-IR磷酸化，所述3T3细胞提供400，000-600，000分子IGF-IR/细胞，和d当与没有所述抗体的这种测定相比，在包含0.5％的热灭活胎牛血清的培养基中，使用3T3的细胞磷酸化测定中，其在10μM的浓度上没有显示作为IGF-IR磷酸化所测量的IGF-IR刺激活性，所述3T3提供400，000-600，000分子IGF-IR/细胞。

Transition metal borides and inorganic boron-containing compounds, such as TiB〓, BN, B〓C and BP, are one of the most important groups for application in high-temperature performance, electronics and catalysts. Traditionally, they were prepared by high-temperature reactions; however, the products were beyond nanometer scale.

中文题名溶剂热合成硼化物及非金属含硼化合物纳米材料副题名外文题名论文作者谷云乐导师钱逸泰学科专业无机化学研究领域\研究方向学位级别博士学位授予单位中国科学技术大学学位授予日期2003 论文页码总数70页关键词纳米材料硼化物溶剂热合成馆藏号BSLW /2003 /O613 /6 硼化物、非金属含硼化合物功能材料（如硼化钛、氮化硼、碳化硼和磷化硼等）通常具有高硬度、高熔点、机械强度大、高温化学稳定性好等一系列优良性能，有些还具有奇异的光、电、磁、热学性能和催化活性，是一类最富潜力的非氧化物高温结构材料、电子材料和催化材料。

The millimetersized tubular crystal selenium was first prepared. By studying the process of treating selenium in ethylenediamine, we proposed the mechanism of the preparation of selenides under solvothermal condition. The selenides came into being from the reaction of metal ions with Se〓, which was obtained by the amine attacking selenium. Moreover, a new precursor to prepare nanocrystalline selenides at room temperature was obtained. From this precursor, we have prepared nanocrystalline silver selenides, copper selenides, lead selenides and cadmium selenides nanorods.

首次报道了采用溶剂热处理的方法制备出厘米尺度的管状结构硒晶体；通过对硒粉在乙二胺中的溶剂热研究，初步探讨了以单质硒为硒源的溶剂热合成硒化物的反应机理应是硒受胺类的亲核进攻变成Se〓而进一步形成相应的硒化物；获得了合成硒化物纳米晶的前驱物，并在室温条件下合成了硒化银、硒化铜、硒化铅纳米晶和硒化镉纳米棒等。

For the quality of ferroalloy, a series of ferroalloys have been researched by differential thermal analysis and thermal gravimetric analysis .

利用差热技术对不同的铁合金产品进行差热分析，结果表明，不同的铁合金产品具有不同的差热曲线，而且对于同种铁合金，易粉化的与不粉化的铁合金产品的差热曲线也不相同，这就为铁合金的质量评价提供了一种新方法。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。