烧结的

A method of production of a reduction resistant dielectric ceramic composition having a superior low frequency dielectric characteristic and further improved in accelerated lifetime of insulation resistance, specifically a method of production of a dielectric ceramic composition containing a main component including a dielectric oxide of a specific composition, a first subcomponent including a V oxide, a second subcomponent containing an Al oxide, a third subcomponent containing an Mn oxide, and a fourth subcomponent containing a specific sintering aid in a specific ratio, including a step of mixing at least part of the materials of the subcomponents excluding one or both of at least the material of the third subcomponent and material of the fourth subcomponent with the starting materials prepared for obtaining the material of the main component to prepare the pre-reaction material, a step of causing the prepared pre-reaction material to react to obtain a reacted material, and a step of mixing the materials of the subcomponents excluded when preparing the pre-reaction material with the obtained reacted material to obtain a dielectric ceramic composition.

本发明提供一种介电陶瓷组合物的制造方法，其中介电陶瓷组合物以特定的比例含有如下成分：含有特定组成的介电体氧化物的主成分，该主成分可以提供具有优异的低频率介电特性的、绝缘电阻的加速寿命进一步提高的耐还原性介电陶瓷组合物的制造方法，含有V氧化物的第1副成分，含有Al氧化物的第2副成分，含有Mn氧化物的第3副成分，以及含有特定的烧结助剂的第4副成分；该方法包含如下工序：将至少除去第3副成分的原料和第4副成分的原料的一种或两种的其它副成分原料的至少一部分，与为了得到主成分原料而准备的起始原料混合，准备反应前原料的工序；使准备的反应前原料反应而得到反应后原料的工序；以及在所得的反应后原料中，混合在准备反应前原料时除去的副成分原料，得到介电陶瓷组合物原料的工序。

Through designing of composition and structure of the bioactive graded coating,innerstress and its distribution in the coating were analyzed and calculated, the resultsshowed that when composition distribution coefficient n was 1.5, a reasonable stressdistribution could be got, that was at the beginning of deposition the suspension containingrichly BG granules was used so that a rich BG granules layer, a good transitional layerbetween BG layer at the bottom and the coating could be obtained at the titanium alloy side,the bottom of the coating; the stress value near the interface and surface and its character,pressure stress or tensile stress, were decided by the character of its composition itself.Changing composition distribution coefficient n could only change the variation tendency ofstress in the coating, but did not change the stress distribution rule in the coating. Thethinner the coating is, the sharper stress variation in the coating is, which does not mean thatthicker coating is better because the thicker the coating is, the little the permitteddeformation of coating is, so the coating thickness should be thinner, for example, about50μm for bending applications, but for applications only bearing pure shear stress, such asroot of tooth implant, the coating can be thicker little, for instance, about 80～100μm. The study on electrification characteristic and electrophoresis deposition of HAand BG granules in aqueous and non-aqueous solution system found that EPD almost didn'toccur in aqueous solution system. However, because HA granules take position charges inabsolute alcohol, a homogeneous EPD be carried out on the cathode titanium alloy slice, but taking negative charge in absolute alcohol the BG granules not be deposited on the cathode. A guided HA crystallizing, 100～300nm, on surface of the BG granules be realized by metathetical reaction, which cover BG granules with HA microcrystals and make the covered BG granules taking position charges in absolute alcohol, sequentially realize the EPCD of the BG and HA granules on the cathode, so it is feasible to make a titanium alloy/BG/HA bioactive graded coating by making use of EPCD technology. The corrosion experiment of rich boron bioglass coating and plasma spray coating showed that split phase, rich boron and rich silicon phase, occurred during its preparation. In basic medium the corrosion behavior of 〓 BG coating showed uniformity corrosion, the corrosion mostly occurred at rich boron phase area, therefore batch formula design of BGshould avoid the occurring of split phase. The corrosion appearance of plasma spray coatingappeared a non-uniform corrosion, mostly occurred at the edge of the laminated HA moltendrops, and emerged an accelerated corrosion tendency, which will easyly lead to corrosioncrackles extending to the interface and the happening of osmotic interfacial corrosion, thatmay be one of the major reasons leading to the coating cracking-off in the later period. Thetesting results of thermal expansion coefficient of 〓 and 〓BG showed the thermalexpansion coefficient of 〓 BG matched with that of titanium alloy better, and 〓 BG couldsinter with titanium alloy into densification enamel layer at low temperature (720℃).

将Ti6Al4V合金在1000℃下进行真空热处理会降低其力学性能，且合金内的V元素会向表面富集，因此，钛合金真空热处理和表面涂层的烧结温度不能过高，即应低于其相转变点；通过对生物活性梯度涂层的组成和结构的设计，分析和计算了梯度涂层内的应力大小和分布，结果表明：对于本研究，当成分分布系数n=1.5时，可以获得较合理的涂层力学性能，即在沉积开始时，采用富含BG颗粒的悬浮液，以便在钛合金侧获得同底层BG有良好过渡的富BG涂层；梯度涂层界面和表面的应力大小、性质由材料组成本身的性质决定，改变成分分布系数，只能改变涂层内应力变化的趋势；涂层的厚薄不影响涂层内的应力分布规律，但涂层越薄，涂层内的应力变化越快，但这并不意味着涂层越厚越好，因为涂层越厚，涂层允许的变形越小，对于应用于弯曲受力部位的涂层而言，涂层应薄一点为好(50μm)；而对于仅纯受剪切应力的部位，如牙根种植体，涂层可适当加厚(80～100μm)；通过对HA和BG颗粒在水溶液体系和非水溶液体系中的带电特性和电泳沉积的研究发现，它们在水溶液体系中很难发生电沉积；在无水乙醇溶液中，HA颗粒带正电，可在阴极钛合金片上发生均匀的电泳沉积，而BG颗粒则带负电荷；利用复分解反应法，可以制得100～300nm的HA，通过诱导HA在BG颗粒表面结晶，可对BG颗粒进行表面包覆，获得了被HA包覆的BG颗粒，改变了BG颗粒表面的带电特性，使BG和HA颗粒在无水乙醇中均带上正电荷，从而实现了HA和BG颗粒在阴极上的共沉积。

A composite rigid shell, with an aerodynamic profile, elongated longitudinally along the span of the blade, one longitudinal end of which is turnable towards a hub of the rotor and includes a blade root, said shell including at least one layer of reinforcing fibres agglomerated by a matrix comprising a synthetic rigidifying resin and laminated upper-surface and lower-surface skins extending from a leading edge to a trailing edge of the blade, each of said laminated skins comprising, from an inside towards an outside of the shell, a film of polyetherimide resin, at least one layer of plies of long and unidirectional fibres oriented substantially along a longitudinal axis of the blade, and at least one layer of fibre fabric, in which the directions of weft and warp yarns are oriented substantially at 45.degree.

复合刚性外壳，与气动的个人资料，拉长纵向沿跨度刀片，一纵年底，这是对回转中心的转子和包括叶根表示，蚬壳，其中至少1层加固纤维烧结由一个矩阵组成的一个综合rigidifying树脂和复合材料层合上表面和低表面皮肤延长，从领先到尾缘的刀片，每个说，叠层皮组成，从内对外界的壳，一个电影聚醚酰亚胺树脂，至少有一个层的层长和单向纤维导向的大幅沿长轴的叶片，并至少有一个层的纤维织物，在该方向的纬纱和经纱是面向大幅在45.degree 。

Metal corrosion in sulfuric aeid edw point is a common and very serious harm go the corrosion forms, in a wide range of production in all aspects of life, especially in some specific process unit operation equipment middle.low-temperature corronsion dew point in the general industrial rurnace, boiler, fuel saving edvices, air preheater, heat exchangers, tower refrigeration systems, dust, garbage incineration furnace, sintering furnace flue and chimney acid plant and the wind tunnels of hypothermia sife, yes containing gurnace flue and chimney acid plant and wind tunnels of hypothermia site, yes containing acidic gases produced by the condensation of cold treatment from the local cold drinks along with the liquid in the device, lesding to a very serious material corrosion.

金属材料的硫酸露点腐蚀是一种常见的，危害十分严重的腐蚀形式，广泛的发生在生产生活的各个方面，尤其发生在一些特定的过程单元操作设备中间。低温露点腐蚀一般发生在在工业加热炉、锅炉、燃料节省器、空气预热器、热交换器、塔顶冷凝系统、除尘器、垃圾焚烧炉、烧结炉、烟道，烟囱及酸厂的引风管道等的低温部位，是含酸性的气体经由该产遇冷冷凝下来的冷饮液局部地随着于设备上，从而造成对材料极严重的腐蚀。

Metal corrosion in sulfuric aeid edw point is a common and very serious harm go the corrosion forms, in a wide range of production in all aspects of life, especially in some specific process unit operation equipment middle.low-temperature corronsion dew point in the general industrial rurnace, boiler, fuel saving edvices, air preheater, heat exchangers, tower refrigeration systems, dust, garbage incineration furnace, sintering furnace flue and chimney acid plant and the wind tunnels of hypothermia sife, yes containing gurnace flue and chimney acid plant and wind tunnels of hypothermia site, yes containing acidic gases produced by the condensation of cold treatment from the local cold drinks along with the liquid in the device, lesding to a very serious material corrosion.

该下载资料由本站会员上传，如果侵犯了您的权力，请通知我们，将立即删除！摘要金属材料的硫酸露点腐蚀是一种常见的，危害十分严重的腐蚀形式，广泛的发生在生产生活的各个方面，尤其发生在一些特定的过程单元操作设备中间。低温露点腐蚀一般发生在在工业加热炉、锅炉、燃料节省器、空气预热器、热交换器、塔顶冷凝系统、除尘器、垃圾焚烧炉、烧结炉、烟道，烟囱及酸厂的引风管道等的低温部位，是含酸性的气体经由该产遇冷冷凝下来的冷饮液局部地随着于设备上，从而造成对材料极严重的腐蚀。

In order to make these silver paste successfully used in commercial, a clear understanding is required for the complex relation between different parameters such as particles size, solid volume fraction, packing density on suspension printing and deformation and the mechanism of silver powder sintering shrinkage and the inorganic adhesive effect under the batch manufacture condition.The main emphasis of our researches was to improve the silver paste properties by developing a reliable, screen-printing paste suitable for fine lines and lower sintering porosity and good interface between thick film and glass substrate.

为开发电学性能稳定、高导电率、具有良好细线印刷性能及优良附着性的高性能电子浆料，本研究着眼于对影响参数进行详细剖析，找到关键控制参数，通过研究微观结构与粉末参数的对应关系，找到如何能制备出具有致密的厚膜结构与较低的孔隙率，并且其浆体与有机载体的界面区也要有明显的改善的电子浆体；同时对批量生产的银粉的形态与粉末烧结反应的收缩现象，无铅玻璃体系对银膜致密化等过程进行研究，获得致密高导的无铅银浆料。

Blade according to claim 1, characterised in that the portion of the spar received in the shell (44) is a single longitudinal bundle (50), solid and substantially flat, connecting to one another the pressure and suction face coverings that each comprise an outer skin (4a, 4b) internally reinforced, from the leading edge (45) and to a point beyond the spar (50), in the direction of the trailing edge (46), by a sole (53a, 53b) for rigidifying the blade in flapping, each sole being laminated and constituted by longitudinal mats or sheets of unidirectional fibres of carbon agglomerated by a polymerised synthetic impregnation resin ensuring the connection by adherence of the pressure and suction face surfaces of the spar (50) directly to the inner faces of the corresponding soles (53a, 53b).

刀片根据权利要求1 ，特色是在该部分的SPAR公司收到的蚬壳（ 44 ）是一个单纵束（ 50 ），固体和大幅的单位，连接到另一个的压力和吸力面对覆盖，每个包括一外皮肤（第4 A ， 4b ）的内部钢筋，从领导力（ 45岁）和一个点，超越了SPAR公司（ 50 ），在方向，尾随的优势（ 46分），由一个唯一的（ 53A条， 53b ） rigidifying刀片在扑，每个唯一被叠层和所构成的纵向垫或床单单向碳纤维烧结由polymerised合成树脂浸渍确保连接坚持的压力和吸力面对表面的SPAR公司（ 50 ）直接向党内的脸相应的鞋底（ 53A条， 53b ）。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。