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Calcining seed of rutile titanium dioxide was prepared at low temperature using metatitanic acid as raw material through alkaline hydrolysis,hydrolysis reaction,first washing,neutralization reaction,second washing and acid dissolution.

以偏钛酸为原料,经碱解反应、水解反应、一次洗涤、中和反应、二次洗涤、酸溶反应,低温下制备了高活性金红石型TiO2煅晶种,并将其用于盐处理过程,考察了晶种添加量和煅温度对TiO2晶型转化的影响。

As confirmed by XRD and XPS determinations, the crystalline pattern of immobilized TiO2 was still anatase-form after calcination, and the micrographic structure and surface properties of ACF have not been damaged by the deposition process and calcination at different temperatures.

从XRD 以及XPS图可以看出;煅后的TiO2仍保持了锐钛矿相;而且经过负载以及不同温度下的煅后; ACF的形貌以及特性并没有被破坏。

Through micropolariscope study on normal clinker ,overburning clinker and underburnt clinker from vertical kiln of a Shaanxi's cement factory,this paper disclosures the relationship between clinker's fine texture and technological conditions.

以陕西某水泥厂立窑熟料为研究对象,利用偏光显微镜对水泥正常熟料、过和欠熟料进行了显微结构分析,揭示了水泥熟料显微结构与结过程中室内温度、通风、氧分布等结工艺的关系。

The method comprises the steps that the molybdenum bearing spent catalyst is roasted and comminuted, then the molybdenum bearing spent catalyst is leach and filter by adopting alkaline solution bearing ammonia, ammonium bicarbonate and oxyful, and the secondary roasting and leaching are performed to the solids after filtration, the twice leaching solution is acidified and the aluminum is precipitated out, then is acidified continuously to precipitate out the molybdenum in the form of molybdic acid, the molybdic acid is dissolved by using ammonia water further, the pH value is adjusted again to obtain ammonium molybdate deposition, and the ammonium molybdate product is obtained after dryness.

将含钼废催化剂进行焙、粉碎,然后采用含氨、碳酸氢铵和双氧水的碱性溶液浸取并过滤,过滤后的固体物进行二次焙和浸取,两次浸取液酸化沉淀出铝,然后继续酸化将钼以钼酸形式沉淀出来,钼酸进一步用氨水溶解,再次调节pH值获得钼酸铵沉淀,干燥后得到钼酸铵产品。

The process of selective reduction roasting-ammonia leaching-solvent extraction-electrowinning is adopted to extract nickel,cobalt and recover iron from low grade nickeliferous laterite ore.

本研究采用选择性还原焙-氨浸-溶剂萃取-电积工艺从低品位红土镍矿中综合提取镍、钴、铁,重点介绍了采用煤作还原剂,选择性还原焙的试验研究。

But the grain growth, grain semiconduction and grain boundary insulation were influenced by many factors, such as the type and contents of dopants, sintering temperature and so on. Therefore, in this thesis the effect of the restore sintering temperature, the oxygenize temperature, the donor and acceptor dopant on the dielectric and varistor properties of devices were studied. With SEM, the microstructure of SrTiO3-based double function ceramic was analyzed.

而晶粒生长、晶粒半导化和晶界绝缘化受到多种因素的影响,诸如杂质的种类和含量、成温度等,因此本论文研究了还原成温度、中温氧化温度、施主和受主掺杂等对SrTiO_3基陶瓷的压敏和介电性能的影响,并借助于SEM分析对SrTiO_3基双功能陶瓷的微观结构进行了分析。

Ammonium paratungstate has a great effect on the properties of the blue tungsten oxide , and blue tungsten oxide has a great effect on tungsten and tungsten carbide powder also; The tungsten carbide powder of good quality can be made from APT or blue tungsten oxide treated by a special process.

仲钨酸铵对蓝钨性能影响较大,而蓝钨物理性能对钨粉和碳化钨粉的性能影响也较大,通过对APT煅前或煅后进行特殊处理优选蓝钨原料,可以制取优质碳化钨粉。

The occurrence of deleterious alkali-carbonate reaction and performance of certain aggregates were determined by detailed petrographic examination of the aggregates in destructive concrete'structures.

在对材料制备过程的研究中,通过对溶胶—凝胶过程及干凝胶不同成温度的物相变化的研究,结合热力学函数方法的计算结果,提出了多组份溶胶的形成过程、溶胶的干燥过程、凝胶的成过程中的主要物相的生成反应。

The photoactive TiO2 was deposited on the surface of magnetic particles using sol-gel coating technique to prepare a novel nanometer-sized magnetic photocatalyst TiO2/SiO2/Fe3O4,and were characterized by means of XRD and TEM,with analysis of effects of calcining temperature and time,catalyst amount as well as radiant time on papermaking wastewater degradation.

采用溶胶-凝胶法,在磁性颗粒表面包覆TiO2,制备了易于固液分离的磁载光催化剂TiO2/SiO2/Fe3O4,通过XRD和TEM对产物的晶体结构、晶粒大小、形貌进行了表征,讨论了焙温度、焙时间、催化剂用量和光照时间等对TiO2光催化剂处理造纸废水的影响。

The results indicate that the pillaring process and crystal growing of anatase can be more easily realized by increasing the acid-base ratio of pillaring agents, raising the pillaring temperature and adding proper quantities of alkali. The calcination of Ti-pillared precursor brings the growth of TiO2 grain, at the same time the layer distance is declined. In order to obtain ideal products, the right pillaring conditions are: the acid-base ratio of pillaring agents of 13, pillaring temperature of 65 ℃ and the volume of alkali (2 mol/L) in pillaring liquid of 6 mL.

结果表明:在一定范围内增大柱撑剂酸碱比、提高柱撑温度以及加入适量碱,有利于插层复合反应的进行和锐钛晶型的生长;柱撑前驱物焙后TiO2晶粒长大,同时焙引起的脱水导致膨润土层间距的下降;为获得较理想的产物,合适的柱化条件为:柱撑剂酸碱比 n n (HNO3)为13、柱撑温度65 ℃和柱撑液加碱量为(2 mol/L NaOH) 6 mL。

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