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Allow sufficient time for the reaction to reach completion, and titrate the unconsumed Reagent with standardized Water Solution to the electrometric or visual endpoint.

给与足够的时间达到反应完全,用标准水溶液去滴定未反应的的卡尔试剂,以永停法或视觉观察终点。

According to articles published in domestic periodicals from 1992 to 1996,the application of titration in analyzing the ferroalloy and its related minerals is summarized in this paper.

根据 1992~ 1996年 5年间国内刊物上所发表的文章,概述了滴定分析法在铁合金及其相关矿物分析中的应用。

This method is fast,accurate,simple and is used to the routine check of the metallic iron in sponge iron with satisfactory result.

介绍了用三氯化铁-重铬酸钾容量法测定海绵铁中金属铁的方法,试样用三氯化铁溶液选择性地使金属铁溶解,过滤分离不溶物,移取部分滤液,用重铬酸钾容量法直接滴定,方法快速准确,操作简便,用于海绵铁中金属铁的日常检测,可获得满意结果。

A series of cholesterol-bearing O-carboxylmethyl chitosan conjugates with different degrees of substitution of the cholesterol moieties and cholesterol-bearing chitosan were synthesized by the succinyl linkages and characterized by Fourier transform infrared, Proton Nuclear Magnetic Resonance (~1H NMR) and elemental analysis. These hydrophobized chitosan derivatives were amphiphilic in nature and their self-aggregation behavior in aqueous media was evaluated by the fluorescence probe technique.

课题的主要研究内容如下:采用化学的方法合成了不同分子结构、不同取代度的系列胆甾醇基壳聚糖衍生物—胆甾醇基壳聚糖和胆甾醇基-羧甲基壳聚糖,并应用先进的分析手段电位滴定、红外光谱法(IR、核磁共振波谱法等对原料、中间产物以及产物进行了结构表征,衍生物分子中的胆甾醇基取代度(3.2%~12.5%)采用元素分析的方法进行检测。

With the acid and alkali titrate method,we got the mean molecular weight and discussed the monomer density,the initiator amount used, chain transfer agent factor as well as reaction temperature to molecular weight influence tendency and d.

聚丙烯酸钠在很多领域的广泛应用,我们采用水溶液聚合法中的中和法合成低分子量聚丙烯酸钠,用酸碱滴定的方法测得聚丙烯酸的平均分子量,并探讨了单体浓度、引发剂用量、链转移剂用量以及反应温度等因素对聚丙烯酸钠分子量的影响趋势和程度。

GC-MS is used to determine content of free TDI, reaction kinetics is analysed by chlorhydric acid/n-dibutyl amine titration -NCO method and DSC, so the system activation energy is calculated.

采用气相色谱-质谱法测定其游离TDI含量,用盐酸-正二丁胺滴定-NCO法和DSC法相结合,分析反应动力学规律,计算体系表观活化能。

Secretion was measured by determining changes in gastric volumes, titratable acidity, acid concentration and total bicarbonate.

用幽门结扎法和灌流法收集胃液,分别测定胃液总量、可滴定H~+量、氢离子浓度和碳酸氢盐的量。

Methods WHO bioassay and microplate method were used for the tests.

采用WHO生物测试法和微量滴定板法。

To determine the content of ascorbic acid in vegetables with the constant current coulometry method, dead-stop method was used for the detection of end point of the coulometric titration.

以恒电流库仑分析法测定了蔬菜中抗坏血酸的含量,以死停终点法指示库仑滴定终点,测定结果与国标规定方法相吻合。

We collected Leishmania promastigotes,washed its with 0.01mol/LpH7.2 buffers ,smashed its,and then measured protein content and titrated work concentration.2.We tested Kala-azar patients"serum and healthy persons"serum of epidemic area by ELISA. The results of three antigensmethods were the same, work concentration of serum was the same(l :100).Results:The protein content of three antigens is, 901 strain with 1000ug/ml,801 strain with 960ug/ml and 951 strain with 1100ug/ml. Suitable work concentration is, 901 strain with 10ug/ml ,801 strain with 12ug/ml and 951 strain with 11ug/ml.

1、抗原的提取:收集新疆不同地区分离得到的利什曼原虫前鞭毛体,经培养,用0.01mol/L pH7.2的磷酸盐缓冲液漂洗,超声粉碎,比色法测定其蛋白质含量,间接ELISA法滴定出抗原的工作稀释度。2、检测:用提取的三株抗原,分别进行间接ELISA法测定黑热病病人血清和疫区健康人血清抗体,并以肺结核病人血清、非疫区健康人血清做对照,三株抗原所用检测方法一致,血清工作稀释度均为1∶100。

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