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Thus this method could be applied to monitor the process of producing dinitrogen pentoxide by electrochemical oxidation of dinitrogen tetroxide in nitric acid. The results from the two-step titration method of redox titration combined with acidity titration were well consistent with that from the method of redox titration combined with NMR.

氧化还原和酸度两步滴定与氧化还原滴定结合核磁共振光谱法的分析结果表明,两种方法的分析结果吻合良好,精确度良好,两种方法都可用于N_2O_4-N_2O_5-HNO_3体系各组分的全浓度分析。

Using EDTA as titratant,murexide as indicator,sodium tartrate ammonium fluoride and sodium thiosulfate as masking agent, nickle concentration was determined in ammonic medium.

以EDTA为滴定剂,紫脲酸铵为指示剂,NH4F、酒石酸钾钠、Na2S2O3为掩蔽剂,在氨性介质中测定镍的浓度;在pH值为8.0的氨-氯化铵缓冲液中,采用滴定比色法测得钴的浓度。

The accuracy and precision of the result accorded with the demand of titrating analysis. The selfmade microtitration was convenient and accurate, could be used to determining the contents of chlorphenamine maleate.

自制微型滴定装置具有较好的操作性能和精密度,符合滴定分析法的要求,可用于测定马来酸氯苯那敏的含量。

The accuracy and precision of the result accorded with the demand of titrating analysis. The self made microtitration was convenient and accurate, could be used to determining the contents of chlorphenamine maleate.

自制微型滴定装置具有较好的操作性能和精密度,符合滴定分析法的要求,可用于测定马来酸氯苯那敏的含量。

The accuracy and precision of the result accorded with the demand of titrating analysis.

自制微型滴定装置具有较好的操作性能和精密度,符合滴定分析法的要求,可用于测定马来酸氯苯那敏的含量。

The accuracy and precision of the result accorded with the demand of titrating analysis.

自制微型滴定装置具有较好的操作性能和精密度,符合滴定分析法的要求,可用於测定马来酸氯苯那敏的含量。

Methods Anhydrous acetic acid as solvent, 0.1 mol/L perchloric acid as titrant, crystal violet solution as indicator to establish non-aqueous titrations and ODS column as stationary phase, methanol and a mixture of 0.025 mol/L sodium phosphate monobasic and 0.02 mol/L sodium dedecyl sulfate (80:20) adjusted with phosphoric acid to a pH (4.8±0.1J as mobile phase, 220 nm as detective wavelength to establish HPLC-UV method for determination of piperazinylethylestrone drug substance; FMOC-CL as a derivatization reagent, FD as a detector to establish an HPLC method with derivatization and column switching for determination of piperazinylethylestrone in dog plasma.

分别采用无水冰醋酸为溶剂,0.1mol/L高氯酸为滴定液,结晶紫指示液指示终点的非水滴定法和HPLC-UV法测定哌嗪雌酚酮原料药含量;以FMOC-CL为衍生化试剂,采用柱切换柱前衍生化萤光检测的HPLC法测定狗血浆中哌嗪雌酚酮含量。

An automatic acidbase titrator using method of the color measurement to judge the end of titration is developed.

介绍了一种用测色法来判断滴定终点的全自动酸碱滴定仪。

Using methanol as solvent and sodium methanol standard solution as titrant,the certification of NTO standard substance was investigated by non-aqueous titration .

以甲醇为溶剂,采用甲醇钠溶液作为滴定剂,通过非水滴定法对NTO的定值方法进行研究,选择了最佳条件。

In the solution,low concentration sulfate ions was determined by a direct titration with barium perchlorate as titrant and thorin as the indicator;the concentration of calcium ions was determined by a direct EDTA titration using Calcon carboxylic acid sodium salt as the indicator.

先用高氯酸将固体混合物溶解形成水溶液,然后以钍试剂为指示剂,用高氯酸钡溶液滴定溶液中的微量硫酸根,并用EDTA法以钙红为指示剂滴定溶液中的钙离子,从而可以计算出钙基脱硫剂的固硫率(表示为脱硫后固体混合物中的钙硫化)。

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