滴定法

Objective: To establish the determination method of amygdalin in bitter almond by HPLC.

目的：建立苦杏仁中苦杏仁苷的HPLC测定方法；方法：通过单因素考察确定样品处理方法，建立 HPLC 测定方法并进行方法学考察，与药典法进行比较试验；结果：用HPLC法测定苦杏仁中苦杏仁苷含量高于药典的滴定法，方法学考察各项指标均符合要求；结论：用HPLC法测定苦杏仁中苦杏仁苷含量灵敏度高、重复性好，样品处理方法简便，可代替滴定法。

Free carboxyl group was determined by the wet chemical analysis method, acid-base titration, in this paper.

在几种测定方法—氢氧化钠直接滴定法、氢氧化钠反滴定法、醋酸钙法中，醋酸钙法较好。

Commonly used method is: EDTA titration method, atomic absorption spectrometry and potassium permanganate titration.

常用的方法有：EDTA滴定法、原子吸收分光光度法和高锰酸钾滴定法。

In this paper the mechanism of the EDTA titration method is expatiated and t.

对 EDTA滴定法的原理进行了阐述，并研究了影响 EDTA滴定法数据离散性的因素。

Degree of deacetylation of the three different chitosan are determined by acid -base titration or acid -base conductometric titration.The MW of chitosan I and II by viscometry is 1.0 X 106and 9.5 X 105,respectively.

分别采用酸碱指示剂滴定和电导滴定法测定了壳聚糖的脱乙酰度，后者测定结果大于前者；应用粘度法测定原料壳聚糖Ⅰ和Ⅱ的粘均分子量分别为：1.0×10~6、9.5×10~5。

The test method is to fetch the urea of the same quality and coated material of different quality first, make coating material parcel evenly the urea particle s surface, grant them into the soil, eluviate with the distilled water every 24 hours, collect the eluviationing solution, titrate the eluviationing solution with distillation titrimetric method, that is, add alkali distillation, make the ammonia release out, absorb with boric acid solution, then titrate it with standard acid.

试验方法是称取相同质量的尿素和不同质量的包膜材料，将包膜材料均匀地包裹在尿素颗粒的表面，将包裹后的包膜肥料施入模拟试验的土壤中，每隔24个小时用蒸馏水淋溶，收集淋溶液，用蒸馏滴定法滴定淋溶液，即加碱蒸馏，使氨释放出来，用硼酸溶液吸收，而后用标准酸滴定之。

Methods: Glass electrode,iodometric method,disodium EDTA titration,silver nitrate titration,fluoride ion selective electrode.

玻璃电极法、碘量法、乙二胺四乙酸二钠滴定法、硝酸银滴定法、氟离子选择电极法等。

There are three purity measuring methods of vulcanizing accelerator NOBS : potentiometric titration , indicator titration and liquid chromatography .

硫化促进剂 NOBS 纯度的测定方法有三种：电位滴定法，指示剂滴定法和液相色谱法。

As to the high polarity, high boiling point resultant—trimesic acid, the analysis methods of infrared spetrum, gas chromatography-mass spectroscopy, vapour-phase chromatography, acid number titration and so on are seperately used to characterize its property. Infrared spetrum and gas chromatography-mass spectroscopy are used to have a qualitative analysis on the resultant and are compared with the stand diagram. Sulfuric acid-methanol esterification and rapid esterification are used to prepare the trimesic acid trimethyl-ester and have a FID quantitative analysis. So that we make sure the purity of trimesic acid in the resultant and also we have an acid alkali titration on the resultant to get its acid number, in order to verify the purity of trimesic acid in the resultant.

对于高极性、高沸点的固体产物均苯三甲酸，分别采用红外光谱、气质联用、气相色谱、酸值滴定等分析手段进行了表征：利用红外光谱、气质联用的方法进行产物的定性分析，并与在同一仪器、同一条件下做出的标准谱图进行比对；采用硫酸-甲醇酯化法和快速酯化法制备出均苯三甲酸三甲酯，对其进行气相色谱FID定量分析，进而确定固体产物中均苯三甲酸的纯度；用酸碱滴定法确定固体产物的酸值，以对固体产物中均苯三甲酸的纯度进行验证。

The direct amperometric titration of amines with sodium tetraphenylborate solution based upon anodic depolarization at a dropping mercury electrode by the use of excess TPB titrant, was systematically investigated.

本文研究了用pH8的四苯硼酸钠水溶液对胺类的直接电流滴定法。滴汞为阳极，饱和甘汞为阴极，以3％琼脂的饱和NaCl溶液为盐桥组成电解池。适宜的滴定条件是：外加电压+0.18伏；底液为pH 2-3的HAc-NaAc介质，而以1％HAc更为方便；滴定体积为10-20毫升。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了