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A new method is used for the rapid determination of SOn^2- in laboratory waste water by benzidine hydrochloride separate and acid-base titration.

中文摘要:提出了利用盐酸联苯胺沉淀分离,酸碱滴定法快速测定实验室废水中SO4^2-含量的新方法。

Lipase mediates esterification between caproic acid (0.6mol/L) and ethanol (0.6mol/L) in n-heptane at 40℃. The decrease in caproic acid is measured by titration and 1 unit of lipase synthetic activity is defined as 1 μmol caproic acid consumed per min.

在40℃下,脂肪酶催化己酸(0.6mol/L)与乙醇(0.6mol/L)在正庚烷中进行酯合成反应,通过滴定法测定剩余的己酸,1个脂肪酶有机相合成酶活单位定义为:在测定条件下每分钟消耗1μmol己酸的酶量。

Ultrasonic conductometric titration is an easy, quick and reliable method for determining surface acidity of zeolites.

对影响超声振荡电导滴定法测定分子筛表面酸性质的因素进行了考察。

So the conductometric titration method can be used for measuring the composition of water-soluble copolymer containing ion monomer through complex reaction between polyelectrolyte and surfactant.

利用电导率的这一转折性变化,建立起了复合作用电导滴定法测定共聚物P(AM- co -NaAMPS)分子链中磺酸盐单体NaAMPS含量的新方法。

Accuracy of determination of deacetylation degree of chitosan by two abrupt change conductometric titration was studied, and effects of chitosan solution concentration, viscosity and deacetylation degree on the result of equivalence point were also investigated.

结果表明:壳聚糖样品质量浓度控制在2~6g/L,利用双突跃电位滴定法可以测定壳聚糖的脱乙酰度,不同样品脱乙酰度测定结果RSD小于0.61%(n=3),该方法具有较高地准确性,可以用于壳聚糖生产和加工过程中的质量控制与检测

In this investigation,the composition of copolymer P(AM- co -NaAMPS) of acrylamide and 2-acrylamido-2-methyl-propanesulfonate sodium has been determined with the aqueous solution of cetyl trimethyl ammonium bromide as titrant at a concentration of 0.001 mol·L-1 by conductometric titration method.

与元素分析进行比较的结果表明,上述复合作用电导滴定法可作为测定水溶性大分子链中磺酸盐单体含量的方便而又准确的方法,而且预计还可用作为测定水溶性大分子链中其它离子性基团含量的简捷方法。

The factors affect on the degree of substitution of product, yield and apparent viscosity, such as the mol rates of EPTAC with -NH2, reaction temperature, reaction time and the content of water in system have been discussed in detail. FTIR spectrometer and UV spectrometer are used to characterize the structure of the derivative and it is proved that substitution reaction mainly occurs on the -N element .The particle size and morphology of chitosan and quantemary ammonium salt of chitosan are analysised by comparing photos of their scanning electron microscope. The degree of substitution of HACC is determined by acid -base conductometric titration. An error in current formula of DS has pointed out and a correct formula has presented.On the base of experience of above experiment, the reaction conditions of HACC were systematically investigated through orthogonal design, and then the best conditions are found. Water-solubility and dependence of pH are studied.

壳聚糖和环氧丙基三甲基氯化铵在异相条件下发生反应,通过单因素实验,制备了一系列不同性能的壳聚糖季铵盐,本文首次详细讨论了反应条件(反应摩尔比、反应时间、反应温度、水含量)对产率及产物性能的影响;用红外光谱和核磁共振对结构进行表征分析时,发现季铵盐阳离子基以N位上取代为主;通过电镜图片对壳聚糖和季铵盐衍生物外观形貌进行对比,采用酸碱电导滴定法测定产物的取代度,并对常用取代度公式做了修正。

Zeta potential,density of surface carboxyl groups,the interaction between carboxyl groups and component in copolymerization emulsion,mechanical properties of films,state of water,particle diameter and distribution of particle diameter and theological behavior of emulsion were investigated by Zeta meter,the conductometric titration, particle size apparatus,dynamic mechanics analysis,differential scanning calorimmetry,scanning electron microscope,rheological apparatus,respectively, to study the mechanism on the water resistance of modified PVAc emulsion.

利用Zeta电位仪、电导滴定法、激光粒度仪、DMA、DSC、SEM、流变仪等手段从Zeta电位、表面羧基密度、羧基和乳液组分中的相互作用、羧酸改性后胶膜的力学性能、水的存在状态、粒径分布、流变性能和微观形貌方面探索了羧基提高乳液耐水性的机理。

The components of the hydrochloric acid and the fire_retardant - an organic diacid in the waste water produced by production of the fire_retardant were analysed rapidly by acid base potentiometer.

采用酸碱电位滴定法快速简便地测定了阻燃剂生产中产生的含有盐酸和阻燃剂———一种有机二元酸的含量。

Quantum chemical calculations were performed based on these conformations to explain the experimental data. 4. The molecular recognition of the chiral Salen Fe complexes towards imidazole derivatives and the measure of the equilibrium constants of host-guest system of the Salen Fe and EMIm a.

用紫外-可见光谱滴定法考察了不同主体Salen-Fe对咪唑及其衍生物的分子识别行为,测定了识别过程的平衡常数和热力学参数,讨论了影响主客体配位能力的有关因素;系统地考察了主客体缔合反应的圆二色光谱性质。

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