滴定分析法

The methods determing the groups in the modified starch have been developed, that is acidimetry for the basicity of acidified starch, complexing titration for the substitution degree of carboxymethyl starch, and heat paste titration and carbonyl process respectively for the carboxyl and nitrogen of oxidized starch.

建立了以酸碱滴定测定酸化淀粉的碱量、络合滴定法测定羧甲基淀粉的取代度、热糊滴定和羟胺法测定氧化淀粉中羧基及羰基、消化定氮测定阳离子淀粉等几种变性淀粉的基团分析方法。

The carbohydrate,fats,protein and amino acid content before and after leather corrosion was analyzed with the following methods:the anthrone color method and the potassium ferricyanide law,the benzine,the Kjeldahl nitrogen determination and the salicylic acid color method,the sole indicator formol titration method.

为了弄清楚霉菌对皮革侵蚀前后，皮革成分变化及其霉菌产生危害的机理，利用蒽酮比色法、石油醚萃取法、凯氏定氮法与水杨酸比色法、甲醛滴定法，分别对侵蚀前后的皮革样品中糖、脂肪、蛋白质和游离氨基酸含量进行了分析。

The instrument is designed according to Chinese Pharmacopoeia 2005 edition of the capacity analysis requirements of the end-point titration.

概述 本仪器是根据中国药典2005版对容量分析永停滴定法的要求而设计的一款新颖微电脑控制的自动永停滴定仪。

In accordance with the method of silver nitrate titration of chloride in water,the sources of the uncertainty of measurement of chloride in water were analyzed and the uncertainty was evaluated.

根据硝酸银滴定法测定水中氯化物的含量，分析了该方法测量不确定度的来源，评定了水中氯化物的测量不确定度，在各不确定度中，以标准溶液配制与样品分析时滴定消耗的硝酸银体积引入的不确定度较大。

Thus this method could be applied to monitor the process of producing dinitrogen pentoxide by electrochemical oxidation of dinitrogen tetroxide in nitric acid. The results from the two-step titration method of redox titration combined with acidity titration were well consistent with that from the method of redox titration combined with NMR.

氧化还原和酸度两步滴定与氧化还原滴定结合核磁共振光谱法的分析结果表明，两种方法的分析结果吻合良好，精确度良好，两种方法都可用于N_2O_4-N_2O_5-HNO_3体系各组分的全浓度分析。

For moisture meters based on Karl Fisher capacitance titrimetry, the accuracy of measurement is dependent on capturing correct end point.

用卡尔。费休容量滴定法测定水分，滴定终点的捕捉正确与否决定着分析的精确度。

GC-MS is used to determine content of free TDI, reaction kinetics is analysed by chlorhydric acid/n-dibutyl amine titration -NCO method and DSC, so the system activation energy is calculated.

采用气相色谱-质谱法测定其游离TDI含量，用盐酸-正二丁胺滴定-NCO法和DSC法相结合，分析反应动力学规律，计算体系表观活化能。

When hydrochloric acid was added into saccharin sodium solution,chemical reaction happened,whose product was glucide,which cannot be dissolved in water,however,it can be dissolved by ethyl acetate,therefore glucide can be extracted from other components,then can be determined by titration with sodium hydroxide.

利用糖精钠与盐酸反应生成不溶于水而溶于乙酸乙酯的物质，将其萃取出来，然后再利用氢氧化钠对其进行滴定分析，采用二分试差法准确测定了某镀光亮镍添加剂中糖精钠及某镀光亮镍液中糖精钠的含量，分别为88。

As to the high polarity, high boiling point resultant—trimesic acid, the analysis methods of infrared spetrum, gas chromatography-mass spectroscopy, vapour-phase chromatography, acid number titration and so on are seperately used to characterize its property. Infrared spetrum and gas chromatography-mass spectroscopy are used to have a qualitative analysis on the resultant and are compared with the stand diagram. Sulfuric acid-methanol esterification and rapid esterification are used to prepare the trimesic acid trimethyl-ester and have a FID quantitative analysis. So that we make sure the purity of trimesic acid in the resultant and also we have an acid alkali titration on the resultant to get its acid number, in order to verify the purity of trimesic acid in the resultant.

对于高极性、高沸点的固体产物均苯三甲酸，分别采用红外光谱、气质联用、气相色谱、酸值滴定等分析手段进行了表征：利用红外光谱、气质联用的方法进行产物的定性分析，并与在同一仪器、同一条件下做出的标准谱图进行比对；采用硫酸-甲醇酯化法和快速酯化法制备出均苯三甲酸三甲酯，对其进行气相色谱FID定量分析，进而确定固体产物中均苯三甲酸的纯度；用酸碱滴定法确定固体产物的酸值，以对固体产物中均苯三甲酸的纯度进行验证。

The composition of obtained PMN-PT have been analyzed by means of macro-quantity chemical analysis. The analyzed results of the Pb2+ concentration indicated that PbO in the PMN-PT seldom volatilized at 850℃. The PbO volatility loss could be up to 3.9% when sintered at 1200℃.

采用定量化学分析法对PMN-PT中的阳离子进行滴定分析。pb~(2+)的化学分析结果表明：在850℃下合成PMN-PT钙钛矿相时，氧化铅的挥发量极少。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了