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The invasion of drilling fluid is the main cause to the damage of fractured formation. The composite salt free-gel drilling fluid is got after analyzing the influence of different kinds of such soluble adulterant as organic salt and non organic salt on the performance of the solid-free drilling fluid and studying the condition to develop the free gel structure and the method to improve the fluid's high temperature stability and inhibitive property. The experiment shows that the apparent viscosity of this system is as high as 27000 mPas when the share rate is 0.3 r/min and the high temperature reaches at the stable level of 150℃ and the HTHP filtrate loss decreases to 15 ml at 150℃.

钻井液侵入是裂缝性储层损害的主要因素之一,实验分析了无机盐、有机盐等不同类型水溶性加重剂对无固相钻井液性能的影响,研究了无固相钻井液快速弱凝胶特性形成条件以及高温稳定性和抑制能力的提高方法,研制出的无固相复合盐弱凝胶功能性钻井液高温稳定性达到150℃,具有独特的流变性(0.3r/min黏度达到27000 mPas)和优良的抑制能力(150℃HTHP滤失量小于15 mL),成本远低于甲酸盐钻井完井液。

Per minute, the quenched trioxide is leached with hot water (between about 50°C. and about 100°C.) to leach the solubilized potassium and after liquid-solids separation the molybdenum trioxide is dissolved in ammonium hydroxide to form ammonium molybdates, which can be recovered from solution and then can be calcined to chemical grade molybdic oxide.

沥滤淬火的三氧化物,是为了浸出可溶性钾和液固体分离后三氧化钼溶解于氢氧化铵形成钼酸铵,这样形成的钼酸铵可以从溶液中得到,然后可以煅烧成化学级钼氧化物。

The subject has completed existing tail gas purification and recovery system from four aspects:(1) carbonation tail gas purification;(2) ammonia cleaning of soda ash filtering machine filtered tail gas;(3) NH3 and CO2 recovery and utilization of sodium carbonate producing tank;(4) distillation and recovery of furnace gas condensate.

本课题从四个方面完善现有纯碱尾气净化与回收系统:(1)碳化尾气净化;(2)滤碱机过滤尾气净氨;(3)出碱槽NH_3、CO_2的回收与利用;(4)炉气冷凝液的蒸馏与回收。

Through the processes of grinding bastnaesite ore concentrate, mixing the ore powder with NaCO3 in the ratio of 1 to 0.1-0.4, roasting the mixture at 400-800 deg.c for 1-6 hr, elution of the roasted sand with hot water to obtain NaF, drying filtered drag after eluting NaF and mixing the dried drag with ammonium chloride, roasting the mixture at 300-600 deg.c for 1-3 hr, hot water soaking to obtain rare earth chloride solution, extraction with 20% kerosine solution of naphthenic acid, and hydrochloric acid counter extraction to obtain rare earth chloride product.

本发明涉及一种氯化铵法从氟碳铈精矿提取氯化稀土的方法,首先将氟碳铈原精矿磨细,并与NaCO 3 混合,其比例为原矿∶NaCO 3 =1∶0.1~0.4,混合均匀后在400℃~800℃焙烧1~6小时,焙砂用热水洗出NaF,洗出NaF的滤渣干燥后与氯化铵混合,于300℃~600℃焙烧1~3小时,再用热水浸取得到氯化稀土溶液,用20%的环烷酸煤油液萃取,再采用盐酸反萃得到氯化稀土产品。

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