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Exposed argentite could be dissolved in thiourea acidified by sulphuric acid ,since native Ag is not dissolved in non-oxidizing inorganic acids , hydrochloric acid was used to dissolve the sphalerite and to soak out the argentite which was enveloped in sphalerite .

继以硫酸酸化的硫脲溶剂溶解裸露的辉银矿,然后根据自然银在非氧化性的无机酸中不溶的特性,采用盐酸溶解闪锌矿并浸

The preparation process includes the following steps: dissolving activator and RE oxide in the molar ratio of 0.01-0.02 in concentrated nitric acid and heating to dry, dissolving the obtain RE nitrate in deionized water to obtain solution of RE nitrate; dissolving soluble tungstate and surfactant in deionized water to obtain tungstate solution; mixing the RE nitrate solution and the tungstate solution through stirring to reaction for 25-60 min to obtain white precipitate; hydrothermal reaction of the precipitate in a reaction kettle at 100-260 deg.c for 24-72 hr; centrifugally separating, washing and drying to obtain the product.

浓硝酸的加入量保证稀土氧化物溶解就可以,过量的硝酸可以加热除去;将可溶性钨酸盐和表面活性剂溶解于去离子水中,得到钨酸盐溶液,表面活剂性的加入量为反应原料重量的0-30wt%;将稀土硝酸盐溶液加入到钨酸盐溶液中搅拌,发生沉淀反应,磁力搅拌时间为25-60分钟,得到白色沉淀;将含有沉淀物的溶液作为前驱物加入到反应釜中,发生水热反应,反应温度为100-260℃,反应时间为24~72小时;离心分离,洗涤,干燥,即得所需产物。

They had suppressed the cathodic process of carbon steel electrode. Their inhibition performance was also related with their molecule stereo conformation and electron configuration. Four of bis-(1, 1'-benzotriazoly)-α,β-diamide compounds linked via-CO 〓CO-chain were synthesized and certified by IR and 〓H-NMR. The minimum energy conformations of these compounds were obtained by MM2 forcefield program. The two benzotriazole moiety in BBT1 was more planar than in other compounds. This was beneficial in increasing the inhibition effects of BBT1. In 0.5M H〓SO〓 solution, BBT1 suppressed anodic corrosion reaction. In 3%NaCl solution, BBT1 suppressed both cathodic and anodic corrosion reactions. 1- [ (1'-imidazolly)-methyl] benzotriazole was synthesized by Mannich reaction.

合成了四个通过-CO〓CO-连接的双(1,1'-苯并三唑)-α,ω-二酰胺化合物,采用MM2分子力学程序优化了它们的分子结构,双(1,1'-苯并三唑)-α,ω-二酰胺化合物的缓蚀作用与其分子内两个苯并三唑单元的空间取向有关系,良好的平面性有利于苯并三唑二聚体的吸附和缓蚀作用,苯并三唑二聚体BBT1分子内两个苯并三唑单元近似平行,所以显示出较好的缓蚀效果。0.5M硫酸中BBT1主要抑制铜的阳极溶解的电化学反应;3%NaCl溶液中,BBT1对铜的阳极溶解和氧的阴极还原过程均有抑制作用,相比较而言对阴极过程的抑制作用更大一些。

The renaturation methods of inclusion body proteins dissolved by HAC or urea are explored.

分别对乙酸溶解的包涵体蛋白和尿素溶解的包涵体蛋白的复性方法进行了摸索。

KIR bind corresponding HLA-Ⅰmay hame four results followed:1、When inhibitory KIR bind HLA-Ⅰand there has no activatory KIR bind it,cell isn\'t dissolve because inhibitory signal access was done;2、When activatory KIR bind corresponding HLA-Ⅰand there has no inhibitory KIR bind it,form activate signal,lead cell dissolve.3、If activatory or inhibitory receptor both bind HLA-Ⅰ,both signal access is make done,when activatory signal play the main role,NK cell still actived,lead target cell dissolve.4、If activatory or inhibitory receptor both bind HLA-Ⅰ,both signal access is make done,when inhibitory signal play the main role,or both signal access don\'t play,NK cell do not make effect.this is NK cell recognice nomal tissue.

与活化型KIR受体相比,抑制型KIR受体与HLA-Ⅰ类抗原结合的亲和性更强,当抑制型和活化型KIR受体识别和结合同一HLA-Ⅰ类抗原分子时,以抑制作用为主。KIR与相应HLA-Ⅰ结合后可能产生以下4种情况:①当抑制型KIR与HLA-Ⅰ结合而无活化型KIR与HLA-Ⅰ相互作用时,因抑制信号通路启动而不产生细胞溶解;②当活化型KIR与靶细胞表面的相应HLA-Ⅰ结合同时无抑制型KIR与HLA-Ⅰ的相互作用时,形成刺激信号通路,导致靶细胞溶解。

The location and severeness of osteolysis around aseptically loosened hip prostheses have certain relation with the migration pathway and collection site of wear particles originated from articular surface.Cement and cementless prostheses have some different roentgenographic feature of osteolysis around the components.

无菌性松动假体周围骨溶解的发生部位及严重程度与磨损颗粒迁移和聚集的部位有关,固定方式不同骨溶解的X线表现亦有差异。

Pulp mills can use partial borate autocausticizing to increase their causticizing capacity or reduce energy intensity by adding sodium metaborate to the liquor cycle which drives autocausticizing reactions in the recovery boiler and forms sodium hydroxide in the smelt dissolving tank without the use of lime or additional causticizing processes.

纸浆厂可以利用硼酸盐自动苛性微粒来提高他们的苛性化能力或是通过在循环液中增加驱动回收炉中的自动苛性化反应和在冶炼溶解池中形成氢氧化钠而不使用石灰和额外的苛性处理的硼酸钠来减少能源的强度。

Base on core observation and grain size analysis, and under associated consideration of logging trace characteristics, Chang8 reservoir in study area is classified into three sedimentatal microfacies, subsea river, mouth bar and river flank.3.The mian diagenesis in study area are: mechanical compaction, cementation, metasomasis and denudation in late diagenetic phase.4. In allocation of reservoir macroscopic heterogeneity, more heterogeneticer reservoir, class 1 and class 2, mainly locate in the center of subsea river or crook and divaricate of the river; class 3 and class 4 mainly locate in river flank, and the physical property of these locality are better.5. Diagenesis of reservoir have influence on the pore structure which influences the reservoir microscopic heterogeneity. The better the pore structure is, the slighter the reservoir microscopic heterogeneity is; on the contrary, the reservoir microscopic heterogeneity is serious.

本次研究所取得的主要成果及熟悉有:1、将合水地区长8储层细分为6个小层:长8_1~1、长8_1~2、长8_1~3、长8_2~1、长8_2~2和长8_2~3.2、依据岩心观察和粒度分析,并结合测井曲线特征,研究区长8储层分为水下分流河道、河口坝和河道侧翼四种沉积微相。3、研究区主要经历的成岩作用有:机械压实和压溶作用、胶结作用、交代作用、晚成岩期溶解作用。4、从宏观非均质性平面展布特征来看研究区宏观非均质较强的1类和2类区主要分布于水下分流河道中间或河道拐弯和分又处。3类和4类往则主要分布于水下分流河道侧翼,这些地方储层均质性相对较好。5、储层成岩作用影响储层的孔隙结构,储层的孔隙结构又对储层的微观非均质性有不同程度的影响,孔隙结构越好,则储层的均质性越好,储层的孔隙结构差,则非均质性强。

The inclusion bodies were washed with Deoxycholic acid Sodium Salt for several times, and then dissolved in N-Lauroyl Sarcosine Sodium for denaturant.

以脱氧胆酸钠洗涤包涵体,然后用N—十二烷基肌氨酸钠溶解,将溶解包涵体进行透析复性。

The results were shown as following:(1)Compared with unsubstituted Pc, the introduction of carboxyphenoxy improves the solubility of four Pc derivates, and can be attributed to amphiphilic phthalocyanine. This property is most important for photosensitizer to transmit in vivo and enrich on the surface of tumors.

研究结果表明:(1)合成的四种酞菁与其它酞菁类衍生物相比,由于用羧基苯氧基对酞菁周边环进行了修饰,其溶解性能得到明显地改善,属于两亲性酞菁化合物,这种溶解特性适合其作为光敏剂在体内的传输和在肿瘤组织中的富集。

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